Quantitative understanding of thermal stability of α′′-Fe16N2Electronic supplementary information (ESI) available: Details of experiments; XRD patterns of the pristine α′′-Fe16N2 nanoparticles and an empty borosilicate capillary (Fig. S1); typical examples of the Rietveld analyses (Fig. S2); XRD patterns of the samples heat-treated at 473, 493, 503 and 513 K under N2 (Fig. S3); plots of wFe, wFe4N, and wamorvs. t/t1/2 (Fig. S4); experimental data collected under an Ar atmosphere (Fig. S5 and S6)
The thermal stability of α′′-Fe 16 N 2 , which attracts much interest because of its superior magnetic properties featuring a large magnetocrystalline anisotropy ( K u ∼ 1 × 10 7 erg cm −3 ) and a large saturation magnetization ( M s ∼ 234 emu g −1 ), though unfortunately thermally unstable, has bee...
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| Main Authors | , , , , , , , , , |
|---|---|
| Format | Journal Article |
| Language | English |
| Published |
06.08.2013
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| Online Access | Get full text |
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| Abstract | The thermal stability of α′′-Fe
16
N
2
, which attracts much interest because of its superior magnetic properties featuring a large magnetocrystalline anisotropy (
K
u
∼ 1 × 10
7
erg cm
−3
) and a large saturation magnetization (
M
s
∼ 234 emu g
−1
), though unfortunately thermally unstable, has been
quantitatively
studied.
The thermal stability of α′′-Fe
16
N
2
, which has a large magnetocrystalline anisotropy (
K
u
∼ 1 × 10
7
erg cm
−3
) and a large saturation magnetization (
M
s
∼ 234 emu g
−1
), though unfortunately thermally unstable, has been
quantitatively
studied. |
|---|---|
| AbstractList | The thermal stability of α′′-Fe
16
N
2
, which attracts much interest because of its superior magnetic properties featuring a large magnetocrystalline anisotropy (
K
u
∼ 1 × 10
7
erg cm
−3
) and a large saturation magnetization (
M
s
∼ 234 emu g
−1
), though unfortunately thermally unstable, has been
quantitatively
studied.
The thermal stability of α′′-Fe
16
N
2
, which has a large magnetocrystalline anisotropy (
K
u
∼ 1 × 10
7
erg cm
−3
) and a large saturation magnetization (
M
s
∼ 234 emu g
−1
), though unfortunately thermally unstable, has been
quantitatively
studied. |
| Author | Kobayashi, Naoya Takano, Mikio Ogawa, Tomoyuki Gallage, Ruwan Hayashi, Naoaki Ogata, Yasunobu Takahashi, Migaku Kusano, Yoshihiro Kohara, Kaori Yamamoto, Shinpei |
| AuthorAffiliation | Kyoto University Department of Fine & Applied Arts Kurashiki University of Science and the Arts Department of Electronic Engineering Toda Kogyo Corporation New Industry Creation Hatchery Center (NICHe) Graduate School of Engineering T&T Innovations Inc Institute for Integrated Cell-Material Sciences (iCeMS) Tohoku University |
| AuthorAffiliation_xml | – name: New Industry Creation Hatchery Center (NICHe) – name: Graduate School of Engineering – name: Kyoto University – name: Department of Electronic Engineering – name: Institute for Integrated Cell-Material Sciences (iCeMS) – name: Kurashiki University of Science and the Arts – name: Tohoku University – name: Department of Fine & Applied Arts – name: T&T Innovations Inc – name: Toda Kogyo Corporation |
| Author_xml | – sequence: 1 givenname: Shinpei surname: Yamamoto fullname: Yamamoto, Shinpei – sequence: 2 givenname: Ruwan surname: Gallage fullname: Gallage, Ruwan – sequence: 3 givenname: Yasunobu surname: Ogata fullname: Ogata, Yasunobu – sequence: 4 givenname: Yoshihiro surname: Kusano fullname: Kusano, Yoshihiro – sequence: 5 givenname: Naoya surname: Kobayashi fullname: Kobayashi, Naoya – sequence: 6 givenname: Tomoyuki surname: Ogawa fullname: Ogawa, Tomoyuki – sequence: 7 givenname: Naoaki surname: Hayashi fullname: Hayashi, Naoaki – sequence: 8 givenname: Kaori surname: Kohara fullname: Kohara, Kaori – sequence: 9 givenname: Migaku surname: Takahashi fullname: Takahashi, Migaku – sequence: 10 givenname: Mikio surname: Takano fullname: Takano, Mikio |
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| Notes | (Fig. S7); mass spectroscopic data (Fig. S8); XRD pattern of the sample heat-treated at 373 K for 14 days under N amor (Fig. S3); plots of 16 (Fig. S9); Rietveld refinement results (Table S1) and values (Table S2). See DOI nanoparticles and an empty borosilicate capillary (Fig. S1); typical examples of the Rietveld analyses (Fig. S2); XRD patterns of the samples heat-treated at 473, 493, 503 and 513 K under N , N / 2 t 4 1/2 (Fig. S4); experimental data collected under an Ar atmosphere (Fig. S5 and S6); thermal stability of α′′-Fe and vs. t w Electronic supplementary information (ESI) available: Details of experiments; XRD patterns of the pristine α′′-Fe 10.1039/c3cc43590c Fe |
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| References_xml | – issn: 2011 doi: Takahashi – issn: 2011 doi: Ogawa – publication-title: US Pat. doi: Takahashi Djayaprawira Shoji – issn: 2012 doi: Takahashi – doi: Takahashi Ogawa Ogata Kobayashi |
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| Snippet | The thermal stability of α′′-Fe
16
N
2
, which attracts much interest because of its superior magnetic properties featuring a large magnetocrystalline... |
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| Title | Quantitative understanding of thermal stability of α′′-Fe16N2Electronic supplementary information (ESI) available: Details of experiments; XRD patterns of the pristine α′′-Fe16N2 nanoparticles and an empty borosilicate capillary (Fig. S1); typical examples of the Rietveld analyses (Fig. S2); XRD patterns of the samples heat-treated at 473, 493, 503 and 513 K under N2 (Fig. S3); plots of wFe, wFe4N, and wamorvs. t/t1/2 (Fig. S4); experimental data collected under an Ar atmosphere (Fig. S5 and S6) |
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