Acetylenic Cyclophanes as Fullerene Precursors: Formation of C 60 H 6 and C 60 by Laser Desorption Mass Spectrometry of C 60 H 6 (CO) 12
A logical precursor of macrocycle C H , cyclophane C H (CO) (1) represents a building block in a possible total synthesis of C . In Fourier transform ion cyclotron resonance laser desorption mass spectroscopic experiments in the negative-ion mode, 1 fragments to C H (2) under successive loss of CO....
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| Published in | Angewandte Chemie International Edition Vol. 37; no. 9; p. 1226 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
18.05.1998
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| Subjects | |
| Online Access | Get full text |
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| Abstract | A logical precursor of macrocycle C
H
, cyclophane C
H
(CO)
(1) represents a building block in a possible total synthesis of C
. In Fourier transform ion cyclotron resonance laser desorption mass spectroscopic experiments in the negative-ion mode, 1 fragments to C
H
(2) under successive loss of CO. Further loss of six H atoms and rearrangement gives C
ions with a fullerenic structure. |
|---|---|
| AbstractList | A logical precursor of macrocycle C
H
, cyclophane C
H
(CO)
(1) represents a building block in a possible total synthesis of C
. In Fourier transform ion cyclotron resonance laser desorption mass spectroscopic experiments in the negative-ion mode, 1 fragments to C
H
(2) under successive loss of CO. Further loss of six H atoms and rearrangement gives C
ions with a fullerenic structure. |
| Author | Pastor, Salvador J Boulle, Christophe Parker, Timothy C Wilkins, Charles L Rubin, Yves Jalisatgi, Satish |
| Author_xml | – sequence: 1 givenname: Yves surname: Rubin fullname: Rubin, Yves organization: Department of Chemistry and Biochemistry, University of California, Los Angeles, Los Angeles, CA 90095-1569 (USA), Fax: (+1) 310-206-7649 – sequence: 2 givenname: Timothy C surname: Parker fullname: Parker, Timothy C organization: Department of Chemistry and Biochemistry, University of California, Los Angeles, Los Angeles, CA 90095-1569 (USA), Fax: (+1) 310-206-7649 – sequence: 3 givenname: Salvador J surname: Pastor fullname: Pastor, Salvador J organization: Department of Chemistry, University of California, Riverside, Riverside, CA 92521 (USA), Fax: (+1) 909-787-4713 – sequence: 4 givenname: Satish surname: Jalisatgi fullname: Jalisatgi, Satish organization: Department of Chemistry and Biochemistry, University of California, Los Angeles, Los Angeles, CA 90095-1569 (USA), Fax: (+1) 310-206-7649 – sequence: 5 givenname: Christophe surname: Boulle fullname: Boulle, Christophe organization: Department of Chemistry and Biochemistry, University of California, Los Angeles, Los Angeles, CA 90095-1569 (USA), Fax: (+1) 310-206-7649 – sequence: 6 givenname: Charles L surname: Wilkins fullname: Wilkins, Charles L organization: Department of Chemistry, University of California, Riverside, Riverside, CA 92521 (USA), Fax: (+1) 909-787-4713 |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29711224$$D View this record in MEDLINE/PubMed |
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| Copyright | 1998 WILEY-VCH Verlag GmbH, Weinheim, Fed. Rep. of Germany. |
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| Keywords | Cage compounds Fullerenes Carbon allotropes Mass spectrometry Alkynes |
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| Snippet | A logical precursor of macrocycle C
H
, cyclophane C
H
(CO)
(1) represents a building block in a possible total synthesis of C
. In Fourier transform ion... |
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| Title | Acetylenic Cyclophanes as Fullerene Precursors: Formation of C 60 H 6 and C 60 by Laser Desorption Mass Spectrometry of C 60 H 6 (CO) 12 |
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