Quadrupole vs. Magnetic Sector Glow Discharge Mass Spectrometry: Comparison of Quantitative Analytical Capabilities

The glow discharge (GD) ion source has developed rapidly over the last several years as a versatile mass spectrometric ion source for complete elemental characterization of metal alloys at sub-ppm concentrations. Recently, the GD ion source has been coupled with a quadrupole mass spectrometer, which...

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Published inJournal of analytical atomic spectrometry Vol. 7; no. 6; pp. 943 - 949
Main Authors Raith, A, Vieth, W, Huneke, J C, Hutton, R C
Format Journal Article
LanguageEnglish
Published 06.01.1992
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Abstract The glow discharge (GD) ion source has developed rapidly over the last several years as a versatile mass spectrometric ion source for complete elemental characterization of metal alloys at sub-ppm concentrations. Recently, the GD ion source has been coupled with a quadrupole mass spectrometer, which allows fast mass scanning with detection limits of sub-ppm levels and is suitable for production ontrol and rapid characterization of 3N--5N pure materials. A comparison has been made between the well-estalished GD with a mass spectrometry double focusing magnetic sector mass spectrometer and the GD quadrupole mass spectrometer, including basic studies on polyatomic-ion abundaces, stability of relative sensitivity factors and a direct comparison of analytical results on several materials. Aluminum in steels is analyzed.
AbstractList The glow discharge (GD) ion source has developed rapidly over the last several years as a versatile mass spectrometric ion source for complete elemental characterization of metal alloys at sub-ppm concentrations. Recently, the GD ion source has been coupled with a quadrupole mass spectrometer, which allows fast mass scanning with detection limits of sub-ppm levels and is suitable for production ontrol and rapid characterization of 3N--5N pure materials. A comparison has been made between the well-estalished GD with a mass spectrometry double focusing magnetic sector mass spectrometer and the GD quadrupole mass spectrometer, including basic studies on polyatomic-ion abundaces, stability of relative sensitivity factors and a direct comparison of analytical results on several materials. Aluminum in steels is analyzed.
Author Vieth, W
Raith, A
Hutton, R C
Huneke, J C
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