Efficient Shape-Stabilized Phase-Change Material Based on Novel Mesoporous Carbon Microspheres as a Matrix for Polyethylene Glycol: Preparation and Thermal Prope
Novel mesoporous carbon microspheres (MCMS), which exhibited a large surface area and were developed by the pyrolysis of polydopamine microspheres (PDAMS), were used as a supporting material for polyethylene glycol (PEG) to prepare a new type of efficient form-stable phase-change material (MCMS-PEG)...
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Published in | JOM (1989) Vol. 71; no. 12; pp. 4547 - 4555 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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New York
Springer Nature B.V
01.12.2019
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Abstract | Novel mesoporous carbon microspheres (MCMS), which exhibited a large surface area and were developed by the pyrolysis of polydopamine microspheres (PDAMS), were used as a supporting material for polyethylene glycol (PEG) to prepare a new type of efficient form-stable phase-change material (MCMS-PEG). Using a simple vacuum impregnation strategy, the preparation of polydopamine microspheres via a biomimetic method was facile, simple and environmentally friendly. Characterization of MCMS-PEG was performed by scanning electron microscopy (SEM), x-ray diffraction (XRD), x-ray photoelectron spectroscopy (XPS), differential scanning calorimetry (DSC), Fourier-transform infrared spectroscopy (FT-IR) and thermogravimetric analysis (TGA). The results suggested that MCMS-PEG possessed high latent heats of 112.08 J/g during the melting process and 107.34 J/g during the solidification process. Additionally, MCMS-PEG presented an enhanced thermal conductivity and excellent thermal stability. Therefore, the novel mesoporous carbon microspheres developed in this study could be used as efficient supports for the preparation of shape-stabilized phase-change materials. |
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AbstractList | Novel mesoporous carbon microspheres (MCMS), which exhibited a large surface area and were developed by the pyrolysis of polydopamine microspheres (PDAMS), were used as a supporting material for polyethylene glycol (PEG) to prepare a new type of efficient form-stable phase-change material (MCMS-PEG). Using a simple vacuum impregnation strategy, the preparation of polydopamine microspheres via a biomimetic method was facile, simple and environmentally friendly. Characterization of MCMS-PEG was performed by scanning electron microscopy (SEM), x-ray diffraction (XRD), x-ray photoelectron spectroscopy (XPS), differential scanning calorimetry (DSC), Fourier-transform infrared spectroscopy (FT-IR) and thermogravimetric analysis (TGA). The results suggested that MCMS-PEG possessed high latent heats of 112.08 J/g during the melting process and 107.34 J/g during the solidification process. Additionally, MCMS-PEG presented an enhanced thermal conductivity and excellent thermal stability. Therefore, the novel mesoporous carbon microspheres developed in this study could be used as efficient supports for the preparation of shape-stabilized phase-change materials. |
Author | Liu, Yu Chen, Zhengshou Ding, Han Liu, Yi Shi, Qian Gao, Junkai Chen, Yan Tang, Xi |
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Copyright | Copyright Springer Nature B.V. Dec 2019 |
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DOI | 10.1007/s11837-019-03787-z |
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SubjectTerms | Biomimetics Carbon Conductivity Differential scanning calorimetry Dopamine Energy storage Fourier transforms Graphene Heat conductivity Infrared analysis Infrared spectroscopy Microspheres Phase change materials Photoelectrons Polyethylene glycol Porous materials Pyrolysis Scanning electron microscopy Solidification Solids Spectrum analysis Temperature Thermal conductivity Thermal energy Thermal stability Thermogravimetric analysis X ray photoelectron spectroscopy |
Title | Efficient Shape-Stabilized Phase-Change Material Based on Novel Mesoporous Carbon Microspheres as a Matrix for Polyethylene Glycol: Preparation and Thermal Prope |
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