Nano-TiO 2 catalyzed microwave synthesis of [alpha] -Hydroxyphosphonates

A simple, novel and green method is reported for the synthesis of α-hydroxyphosphonates by hydro-phosphonylation of various structurally diversified aldehydes (aromatic/ heteroaromatic) using Nano-TiO 2 as catalyst under solvent free microwave condition. Environmentally benign reaction procedures, s...

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Published inOrganic communications Vol. 7; no. 3; p. 98
Main Authors S Siva Prasad, Jayaprakash, S H, Rao, K Umamaheswara, N Bakthavatchala Reddy, P Chenna Rohini Kumar, Reddy, C Suresh
Format Journal Article
LanguageEnglish
Published Gebze ACG Publications 01.07.2014
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Abstract A simple, novel and green method is reported for the synthesis of α-hydroxyphosphonates by hydro-phosphonylation of various structurally diversified aldehydes (aromatic/ heteroaromatic) using Nano-TiO 2 as catalyst under solvent free microwave condition. Environmentally benign reaction procedures, short reaction times, easy work-up, high product yields, and reusability of catalyst for several cycles with consistent activity makes this protocol a highly attentive one.
AbstractList A simple, novel and green method is reported for the synthesis of α-hydroxyphosphonates by hydro-phosphonylation of various structurally diversified aldehydes (aromatic/ heteroaromatic) using Nano-TiO 2 as catalyst under solvent free microwave condition. Environmentally benign reaction procedures, short reaction times, easy work-up, high product yields, and reusability of catalyst for several cycles with consistent activity makes this protocol a highly attentive one.
Author Reddy, C Suresh
Rao, K Umamaheswara
S Siva Prasad
N Bakthavatchala Reddy
Jayaprakash, S H
P Chenna Rohini Kumar
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