Detection of the radical and reduced forms of α-(4-pyridyl 1-oxide)-N-tert-butylnitronelpentyl radical adduct formed on reaction of an oxidized linoleic acid with ferrous ions using high performance liquid chromatography with electrochemical detection
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Published in | Journal of separation science Vol. 25; no. 9; pp. 601 - 607 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
Weinheim
Wiley
2002
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Subjects | |
Online Access | Get full text |
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Author | IWAHASHI, Hideo NISHIZAKI, Koji TAKAGI, Ichiro |
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Author_xml | – sequence: 1 givenname: Hideo surname: IWAHASHI fullname: IWAHASHI, Hideo organization: Department of Chemistry, Wakayama Medical University, 811-1 Kimiidera, Wakayama 641-8509, Japan – sequence: 2 givenname: Koji surname: NISHIZAKI fullname: NISHIZAKI, Koji organization: Department of Chemistry, Faculty of Education, Wakayama University, 930 Sakaedani, Wakayama 640-8510, Japan – sequence: 3 givenname: Ichiro surname: TAKAGI fullname: TAKAGI, Ichiro organization: Department of Chemistry, Faculty of Education, Wakayama University, 930 Sakaedani, Wakayama 640-8510, Japan |
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Keywords | Chemical analysis Coupled method Nitrone Reaction product EPR spectrometry HPLC chromatography Radical scavenger Electrospray Electrochemical detector Linoleic acid Pyridine derivatives Iron II Ions Organic free radical Pentyl radicals Unsaturated fatty acid Oxidation Mass spectrometry Peroxidation |
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SubjectTerms | Aliphatic compounds Analytical chemistry Chemistry Chromatographic methods and physical methods associated with chromatography Exact sciences and technology Organic chemistry Other chromatographic methods Preparations and properties |
Title | Detection of the radical and reduced forms of α-(4-pyridyl 1-oxide)-N-tert-butylnitronelpentyl radical adduct formed on reaction of an oxidized linoleic acid with ferrous ions using high performance liquid chromatography with electrochemical detection |
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