Method for preparing full-hydrolysis catalyst with nickel monatomic double active sites
The invention relates to the technical field of preparation of sub-nano materials and in particular to a method for preparing a full-hydrolysis catalyst with nickel monatomic double active sites. Themethod comprises the following steps: by taking nickel acetylacetone and a metal organic framework st...
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Format | Patent |
Language | Chinese English |
Published |
20.12.2019
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Abstract | The invention relates to the technical field of preparation of sub-nano materials and in particular to a method for preparing a full-hydrolysis catalyst with nickel monatomic double active sites. Themethod comprises the following steps: by taking nickel acetylacetone and a metal organic framework structure as raw materials, and ethanol as a solvent, performing dissolution, stirring, mixing, cleaning and vacuum drying so as to obtain ZIF-67; dissolving the ZIF-67 and the nickel acetylacetone into the ethanol, performing ultrasonic dispersion, and performing stirring till the materials are completely dried; and introducing argon, increasing the temperature to 700-750 DEG C, keeping the temperature for 2-3 hours, and performing natural furnace cooling, so as to obtain the full-hydrolysis catalyst with nickel monatomic double active sites. The method has the advantages of being low in cost, rapid in reaction velocity, mild in reaction, easy in reaction control, energy-saving and environment-friendly, high in prod |
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AbstractList | The invention relates to the technical field of preparation of sub-nano materials and in particular to a method for preparing a full-hydrolysis catalyst with nickel monatomic double active sites. Themethod comprises the following steps: by taking nickel acetylacetone and a metal organic framework structure as raw materials, and ethanol as a solvent, performing dissolution, stirring, mixing, cleaning and vacuum drying so as to obtain ZIF-67; dissolving the ZIF-67 and the nickel acetylacetone into the ethanol, performing ultrasonic dispersion, and performing stirring till the materials are completely dried; and introducing argon, increasing the temperature to 700-750 DEG C, keeping the temperature for 2-3 hours, and performing natural furnace cooling, so as to obtain the full-hydrolysis catalyst with nickel monatomic double active sites. The method has the advantages of being low in cost, rapid in reaction velocity, mild in reaction, easy in reaction control, energy-saving and environment-friendly, high in prod |
Author | LI YASHU GONG YITAO LI DONGXIANG LAI WEIHONG CHOU SHULEI LI YONGCHENG |
Author_xml | – fullname: LI YASHU – fullname: LI YONGCHENG – fullname: GONG YITAO – fullname: LI DONGXIANG – fullname: CHOU SHULEI – fullname: LAI WEIHONG |
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DocumentTitleAlternate | 一种制备镍单原子双活性位点的全水解催化剂的方法 |
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Snippet | The invention relates to the technical field of preparation of sub-nano materials and in particular to a method for preparing a full-hydrolysis catalyst with... |
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Title | Method for preparing full-hydrolysis catalyst with nickel monatomic double active sites |
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