Method for synthesizing pinane superoxide by oxidizing pinane

The invention discloses a method for synthesizing pinane superoxide by oxidizing pinane, and belongs to the technical field of deep processing of terpenoids. According to the method, an initiator is replaced by the pinane superoxide, the pH value of a reaction system is adjusted by adding an organic...

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Bibliographic Details
Main Authors CHEN JIANQUAN, HUANG LEI, LI JIEPENG, SU BINGLIAN, LI ZHAN, CHEN WEIQIANG
Format Patent
LanguageChinese
English
Published 19.11.2014
Subjects
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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Summary:The invention discloses a method for synthesizing pinane superoxide by oxidizing pinane, and belongs to the technical field of deep processing of terpenoids. According to the method, an initiator is replaced by the pinane superoxide, the pH value of a reaction system is adjusted by adding an organic alkali, the reaction process of materials in a reaction kettle is analyzed, and the pressure in the kettle and the temperatures of the reaction materials are adjusted correspondingly, so that a reaction proceeds to high yield of the pinane superoxide in a mild and ordered way, and the aim of obtaining a high-quality and high-purity pinane superoxide product is fulfilled.
Bibliography:Application Number: CN20141396839