Method for determining content of diminazene and antipyrine in diminazene particle

The invention discloses a method for determining content of diminazene and antipyrine in diminazene particles, and belongs to HPLC (high performance liquid chromatography). The chromatographic conditions of the method is as follows: (1) octadecyl silane-bonded silica gel is DiamonsilC18 column (250m...

Full description

Saved in:
Bibliographic Details
Main Authors WEI GUIXIANG, LV HULIN, MA JINBO, LI QIAN
Format Patent
LanguageChinese
English
Published 15.08.2012
Subjects
INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES
MEASURING
PHYSICS
TESTING
Online AccessGet full text

Cover

Abstract The invention discloses a method for determining content of diminazene and antipyrine in diminazene particles, and belongs to HPLC (high performance liquid chromatography). The chromatographic conditions of the method is as follows: (1) octadecyl silane-bonded silica gel is DiamonsilC18 column (250mm*4.6mm, 5 mum) of a filler; (2) the mobile phase volume ratio of phosphate buffered saline to carbinol is 27 to 10; and (3) the measurement wavelength of an ultraviolet detector is 250nm, the flow velocity of the mobile phase is 0.5mL/min, the introduced sample volume is 20 muL, and the column temperature is 30 DEG C. The detection method disclosed by the invention is simple in operation, and enhance the sensitivity and the accuracy of the detection. The method disclosed by the invention is suitable for determining the content of diminazene and antipyrine in diminazene particles.
AbstractList The invention discloses a method for determining content of diminazene and antipyrine in diminazene particles, and belongs to HPLC (high performance liquid chromatography). The chromatographic conditions of the method is as follows: (1) octadecyl silane-bonded silica gel is DiamonsilC18 column (250mm*4.6mm, 5 mum) of a filler; (2) the mobile phase volume ratio of phosphate buffered saline to carbinol is 27 to 10; and (3) the measurement wavelength of an ultraviolet detector is 250nm, the flow velocity of the mobile phase is 0.5mL/min, the introduced sample volume is 20 muL, and the column temperature is 30 DEG C. The detection method disclosed by the invention is simple in operation, and enhance the sensitivity and the accuracy of the detection. The method disclosed by the invention is suitable for determining the content of diminazene and antipyrine in diminazene particles.
Author WEI GUIXIANG
LV HULIN
LI QIAN
MA JINBO
Author_xml – fullname: WEI GUIXIANG
– fullname: LV HULIN
– fullname: MA JINBO
– fullname: LI QIAN
BookMark eNrjYmDJy89L5WQI8k0tychPUUjLL1JISS1JLcrNzMvMS1dIzs8rSc0rUchPU0jJBIolVqXmpSok5qUAcUlmQWVRJpCbmYcsWZBYVJKZnJPKw8CalphTnMoLpbkZFN1cQ5w9dFML8uNTiwsSk4GqS-Kd_QwNjMyMzUwtjByNiVEDAHUuOjA
ContentType Patent
DBID EVB
DatabaseName esp@cenet
DatabaseTitleList
Database_xml – sequence: 1
  dbid: EVB
  name: esp@cenet
  url: http://worldwide.espacenet.com/singleLineSearch?locale=en_EP
  sourceTypes: Open Access Repository
DeliveryMethod fulltext_linktorsrc
Discipline Medicine
Chemistry
Sciences
Physics
ExternalDocumentID CN102636582A
GroupedDBID EVB
ID FETCH-epo_espacenet_CN102636582A3
IEDL.DBID EVB
IngestDate Fri Jul 19 16:30:27 EDT 2024
IsOpenAccess true
IsPeerReviewed false
IsScholarly false
Language Chinese
English
LinkModel DirectLink
MergedId FETCHMERGED-epo_espacenet_CN102636582A3
Notes Application Number: CN2012170211
OpenAccessLink https://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20120815&DB=EPODOC&CC=CN&NR=102636582A
ParticipantIDs epo_espacenet_CN102636582A
PublicationCentury 2000
PublicationDate 20120815
PublicationDateYYYYMMDD 2012-08-15
PublicationDate_xml – month: 08
  year: 2012
  text: 20120815
  day: 15
PublicationDecade 2010
PublicationYear 2012
RelatedCompanies HEBEI KEXING PHARMACEUTICAL CO.,LTD
RelatedCompanies_xml – name: HEBEI KEXING PHARMACEUTICAL CO.,LTD
Score 2.9696648
Snippet The invention discloses a method for determining content of diminazene and antipyrine in diminazene particles, and belongs to HPLC (high performance liquid...
SourceID epo
SourceType Open Access Repository
SubjectTerms INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES
MEASURING
PHYSICS
TESTING
Title Method for determining content of diminazene and antipyrine in diminazene particle
URI https://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20120815&DB=EPODOC&locale=&CC=CN&NR=102636582A
hasFullText 1
inHoldings 1
isFullTextHit
isPrint
link http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1LT4NAEJ7U-rxp1Wh9ZE0Mt8bwhgMxdoE0JqVNU01vDbtAxAMQwRj7653dUNuLHrjsJhN2YPhmhm9mAO65m7LMwUjVUWNTpG74wI1tjFpZbNoYQRtqLAmykTV6MZ4X5qID7-taGNkn9Es2R0SL4mjvjfxeV5skli-5lfUDy3GpfAznnq-00bGqIcKZij_0gunEn1CFUo9GSjRDX1ezdERb7WkHdoUbLfrsB69DUZVSbUNKeAx7U5RWNCfQWb314JCuJ6_14GDc_vDuwb5kaPIaF1srrE9hNpZjnwn6myRp6SyIQETQzlEiKTOSyGFdKzwYiYsEryavvkWhH8mL7c2qfXPO4C4M5nQ0wNtc_upkSaPNifRz6BZlkV4AMVzL1VXGLT1LDIO5LMNnpMe2mWiZw1l6Cf2_5fT_27yCI6FfkU5VzWvoNh-f6Q3iccNupSJ_AFqtkLA
link.rule.ids 230,309,786,891,25594,76904
linkProvider European Patent Office
linkToHtml http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1LS8NAEB5qfdSbRkXrawXJrUjeyaGI3bREbdJSovRWsnlgPSTBRsT-emeX1Paih73swrA7yeTbmXwzA3AbOynLbPRUbSUyeOgm7jiRhV4riwwLPWhdiQRBNjC9F_1pakwb8L7KhRF1Qr9EcUS0qBjtvRLf63IdxHIFt3Jxx-Y4VdwPwq4r196xoiLCGbLb6_bHI3dEZUq7NJCDCd51VVNDtFUftmDbQpeQ19nvv_Z4Vkq5CSmDA9gZo7S8OoTG8k2CFl11XpNgz69_eEuwKxia8QInaytcHMHEF22fCd43SVLTWRCBCKedo0RSZCQRzbqWeDAS5QmOal5-80Q_Ms83F8v6zTmGm0E_pF4Htzn71cmMBusTaSfQzIs8PQWiO6ajKSw2tSzRdeawDJ-RFllGomZ2zNIzaP8tp_3f4jW0vNAfzoaPwfM57HNd89CqYlxAs_r4TC8Rmyt2JZT6A0Vqk5s
openUrl ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Apatent&rft.title=Method+for+determining+content+of+diminazene+and+antipyrine+in+diminazene+particle&rft.inventor=WEI+GUIXIANG&rft.inventor=LV+HULIN&rft.inventor=MA+JINBO&rft.inventor=LI+QIAN&rft.date=2012-08-15&rft.externalDBID=A&rft.externalDocID=CN102636582A