Method for synthesizing erucamide propyl betaine
The invention discloses a method for synthesizing erucamide propyl betaine, relating to a method for manufacturing viscoelastic surfactants. The method for synthesizing the erucamide propyl betaine comprises the steps of carrying out a condensation reaction, a reduced pressure distillation reaction...
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Format | Patent |
Language | Chinese English |
Published |
25.07.2012
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Abstract | The invention discloses a method for synthesizing erucamide propyl betaine, relating to a method for manufacturing viscoelastic surfactants. The method for synthesizing the erucamide propyl betaine comprises the steps of carrying out a condensation reaction, a reduced pressure distillation reaction and a quaternary amination reaction and comprises the concrete steps of firstly putting erucic acid, dimethylamino propylamine and a catalyst in a reaction kettle and reacting for 6-10 hours at a temperature of 140-200 DEG C; keeping the temperature and carrying out reduced pressure distillation for 30-60 minutes and vacuumizing to 600-650mHg; neutralizing the erucic acid by using dilute alkaline water and rinsing till to be neutral; and adding a sodium chloroacetate aqueous solution into a mixed solvent of intermediate tertiary amine and carrying out the quaternary amination reaction for 4-8 hours at a temperature of 60-90 DEG C, wherein, finally, the tertiary amine conversion rate is up to more than 98% and the c |
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AbstractList | The invention discloses a method for synthesizing erucamide propyl betaine, relating to a method for manufacturing viscoelastic surfactants. The method for synthesizing the erucamide propyl betaine comprises the steps of carrying out a condensation reaction, a reduced pressure distillation reaction and a quaternary amination reaction and comprises the concrete steps of firstly putting erucic acid, dimethylamino propylamine and a catalyst in a reaction kettle and reacting for 6-10 hours at a temperature of 140-200 DEG C; keeping the temperature and carrying out reduced pressure distillation for 30-60 minutes and vacuumizing to 600-650mHg; neutralizing the erucic acid by using dilute alkaline water and rinsing till to be neutral; and adding a sodium chloroacetate aqueous solution into a mixed solvent of intermediate tertiary amine and carrying out the quaternary amination reaction for 4-8 hours at a temperature of 60-90 DEG C, wherein, finally, the tertiary amine conversion rate is up to more than 98% and the c |
Author | FENG MINGKE HE ZUHUI FENG ZIWEI ZHU JIN LIU YONG |
Author_xml | – fullname: HE ZUHUI – fullname: ZHU JIN – fullname: FENG ZIWEI – fullname: FENG MINGKE – fullname: LIU YONG |
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Notes | Application Number: CN2012147173 |
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Snippet | The invention discloses a method for synthesizing erucamide propyl betaine, relating to a method for manufacturing viscoelastic surfactants. The method for... |
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Title | Method for synthesizing erucamide propyl betaine |
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