Method for manufacturing furan-2,5-dicarboxylic acid (FDCA) from a salt solution
The invention pertains to a method for manufacturing furan-2,5-dicarboxylic acid (FDCA) by converting a furan-2,5-dicarboxylate salt (MFDC) into furan-2,5-dicarboxylic acid (FDCA), comprising the steps of combining an aqueous solution of MFDC with a concentration of at least 5 wt.% with an inorganic...
Saved in:
Main Authors | , |
---|---|
Format | Patent |
Language | English |
Published |
28.09.2017
|
Subjects | |
Online Access | Get full text |
Cover
Loading…
Abstract | The invention pertains to a method for manufacturing furan-2,5-dicarboxylic acid (FDCA) by converting a furan-2,5-dicarboxylate salt (MFDC) into furan-2,5-dicarboxylic acid (FDCA), comprising the steps of combining an aqueous solution of MFDC with a concentration of at least 5 wt.% with an inorganic acid (HY), to form a reaction mixture comprising solid FDCA in a concentration of 1-15 wt.% in a solution of a salt resulting from the cation of the furan-2,5-dicarboxylate salt and the anion of the inorganic acid (MY solution), removing solid FDCA from the reaction mixture in a solid/liquid separation step, and providing part of the MY solution resulting from the solid/liquid separation step to the step of combining MFDC with HY. The step of providing part of the MY salt solution resulting from the solid/liquid separation step to the step of combining MFDC with HY makes it possible to obtain a stable and economic process which results in an FDCA product with good quality, and obtained in high yield. |
---|---|
AbstractList | The invention pertains to a method for manufacturing furan-2,5-dicarboxylic acid (FDCA) by converting a furan-2,5-dicarboxylate salt (MFDC) into furan-2,5-dicarboxylic acid (FDCA), comprising the steps of combining an aqueous solution of MFDC with a concentration of at least 5 wt.% with an inorganic acid (HY), to form a reaction mixture comprising solid FDCA in a concentration of 1-15 wt.% in a solution of a salt resulting from the cation of the furan-2,5-dicarboxylate salt and the anion of the inorganic acid (MY solution), removing solid FDCA from the reaction mixture in a solid/liquid separation step, and providing part of the MY solution resulting from the solid/liquid separation step to the step of combining MFDC with HY. The step of providing part of the MY salt solution resulting from the solid/liquid separation step to the step of combining MFDC with HY makes it possible to obtain a stable and economic process which results in an FDCA product with good quality, and obtained in high yield. |
Author | Van Krieken, Jan De Haan, Andre Banier |
Author_xml | – fullname: Van Krieken, Jan – fullname: De Haan, Andre Banier |
BookMark | eNqNyrsKwjAUANAMOvj6hwsuChZMqu6lWlwEB53LNb3RQJpb8gD9exc_wOksZypGnj1NxPVC6cUdGA7Qo88GdcrB-ieYHNAXarMvOqsxPPj9cVYDatvBqjnW1RpM4B4QIroEkV1Olv1cjA26SIufM7FsTrf6XNDALcUBNXlKbXVXW3lQpZI7Vcnyv_UF3h44Kw |
ContentType | Patent |
DBID | EVB |
DatabaseName | esp@cenet |
DatabaseTitleList | |
Database_xml | – sequence: 1 dbid: EVB name: esp@cenet url: http://worldwide.espacenet.com/singleLineSearch?locale=en_EP sourceTypes: Open Access Repository |
DeliveryMethod | fulltext_linktorsrc |
Discipline | Medicine Chemistry Sciences |
ExternalDocumentID | AU2016232142A1 |
GroupedDBID | EVB |
ID | FETCH-epo_espacenet_AU2016232142A13 |
IEDL.DBID | EVB |
IngestDate | Fri Jul 19 13:02:25 EDT 2024 |
IsOpenAccess | true |
IsPeerReviewed | false |
IsScholarly | false |
Language | English |
LinkModel | DirectLink |
MergedId | FETCHMERGED-epo_espacenet_AU2016232142A13 |
Notes | Application Number: AU20160232142 |
OpenAccessLink | https://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170928&DB=EPODOC&CC=AU&NR=2016232142A1 |
ParticipantIDs | epo_espacenet_AU2016232142A1 |
PublicationCentury | 2000 |
PublicationDate | 20170928 |
PublicationDateYYYYMMDD | 2017-09-28 |
PublicationDate_xml | – month: 09 year: 2017 text: 20170928 day: 28 |
PublicationDecade | 2010 |
PublicationYear | 2017 |
RelatedCompanies | Purac Biochem BV |
RelatedCompanies_xml | – name: Purac Biochem BV |
Score | 3.115389 |
Snippet | The invention pertains to a method for manufacturing furan-2,5-dicarboxylic acid (FDCA) by converting a furan-2,5-dicarboxylate salt (MFDC) into... |
SourceID | epo |
SourceType | Open Access Repository |
SubjectTerms | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
Title | Method for manufacturing furan-2,5-dicarboxylic acid (FDCA) from a salt solution |
URI | https://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170928&DB=EPODOC&locale=&CC=AU&NR=2016232142A1 |
hasFullText | 1 |
inHoldings | 1 |
isFullTextHit | |
isPrint | |
link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV3dS8MwED_GFPVNp-LHlIBSFAxubTO7hyFd2jKEfSCb7G2kbQKD2Y21Q_3vvYRN97S3koOQHPnl7nr53QHcNx2FolhQVleKuniGaCyFosJVaBDiWipN64Rur9EZuW9jNi7BbMOFMXVCv0xxRERUgngvzH29-P-JFZi3lflzPMWh-Ws0bAXWOjquv9SatmcF7VY46Ad9bnGOkaTVe9cyNPS6vpiPsdKedqR1pf3wo615KYttoxIdw_4A58uKEyjJrAKHfNN7rQIH3XXKGz_X6MtPYdA17Z4J-pnkU2QrTUowLEOiVmhyqP3EqE67LOP59w_ug4hkmpKHKOD-I9E8EiJILmYF2Zy3M7iLwiHvUFza5E8TE3-0vQ_nHMrZPJMXQJzEZQrRxdIGxroSQeeh55YyR2dBpe1eQnXXTFe7xddwpHWrn0nYXhXKxXIlb9AWF_GtUeEvk2eLzg |
link.rule.ids | 230,309,786,891,25594,76904 |
linkProvider | European Patent Office |
linkToHtml | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV3dSwJBEB_EInsrK7KsFoqjoCW9Dz8eJPQ-uMo7j9DwTfa8XRDsFD2p_vtmFy2ffDtuYLkd9re_nZv9zQDcNQ2BpphRqyoENXEN0ZgzQZkpkBDiSsJV64QgrPkD83VoDXMw3WhhVJ3QL1UcERE1Rrxnar-e___EctTdyuVTPMFXs2ev33K0dXRcrVeaekNzOi036jk9W7NtjCS18F3akOhlfbE2xkp7dQwKZaV996MjdSnzbVLxjmA_wvHS7BhyPC1Cwd70XivCQbBOeePjGn3LE4gC1e6Z4DmTfLJ0JUUJSmVIxAoph-qPFpVpl0U8-_7BeRA2niTk3nPs9gOROhLCyJJNM7JZb6dw67l926f4aaM_T4zag-15GGeQT2cpPwdijE1LILqspIaxLkfQNfDklliGzIJy3SxBeddIF7vNN1Dw-0F31H0J3y7hUPpZXpnQG2XIZ4sVv0JezuJr5c5fQw6OuQ |
openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Apatent&rft.title=Method+for+manufacturing+furan-2%2C5-dicarboxylic+acid+%28FDCA%29+from+a+salt+solution&rft.inventor=Van+Krieken%2C+Jan&rft.inventor=De+Haan%2C+Andre+Banier&rft.date=2017-09-28&rft.externalDBID=A1&rft.externalDocID=AU2016232142A1 |