Synthesis and characterization of some metal complexes of [N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol- 4 ylcarbamothioyl) acetamide]

• Published in: Ibn Al-Haitham Journal for Pure and Applied Sciences Vol. 28; no. 2; pp. 102 - 115
• Main Authors: Sarhan, Basimah Muhsin, Latif, Sajid Mahmud, Wahid, Inas Jasim
• Format: Journal Article
• Language: Arabic; English
• Published: بغداد، العراق جامعة بغداد، كلية التربية ابن الهيثم 2015
• Subjects: Aminoantipyrine; Complexes; Inorganic compounds; Metal complexes; Synthesis; أمينو أنتيبيرين; الجبر الخطي; المركبات غير العضوية; الهندسة

A new ligand [N- (1,5- dimethyl -3- oxo- 2 – phenyl - 2 ,3 – dihydro -1H- pyrazol -4-ylcarbamothioyl) acetamide] (AAD) was synthesized by reaction of acetyl isothiocyanate with 4-aminoantipyrine, The ligand was characterized by micro elemental analysis C.H.N.S., FT-IR ,UV-Vis and 1H-13CNMR spectra,...