Employing Cu@Fe 3 O 4 /SiO 2 @MWCNTs as New Catalyst for the Green Synthesis of New Pyridopyrroloindoles Using Multicomponent Reactions of Isatins
ABSTRACT By using a multicomponent reaction involving isatins, diamines or aminoalcohols, activated acetylenic compounds, haloketones, and ammonium acetate in aqueous media in the presence of Cu@Fe 3 O 4 /SiO 2 @MWCNTs as new catalyst, the novel pyridopyrroloindole was produced in high yields. This...
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| Published in | Applied organometallic chemistry |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
29.08.2024
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| Abstract | ABSTRACT By using a multicomponent reaction involving isatins, diamines or aminoalcohols, activated acetylenic compounds, haloketones, and ammonium acetate in aqueous media in the presence of Cu@Fe 3 O 4 /SiO 2 @MWCNTs as new catalyst, the novel pyridopyrroloindole was produced in high yields. This catalyst was produced by employing Petasites hybridus rhizome water extract as a green media and moderate base. The pyridopyrroloindole derivatives were newly synthesized compounds, and their antioxidant properties were assessed using the 2,2‐diphenyl‐1‐picrylhydrazyl (DPPH) radical trapping and ferric reducing ability of plasma (FRAP) experiments. The pyridopyrroloindole 6b showed higher performance than butylated hydroxytoluene (BHT) and tert‐butylhydroquinone (TBHQ) better results. This method is used to make pyridopyrroloindole derivatives, and it has the advantages of a quick reaction, high yields, and the ability to separate the products easily. |
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| AbstractList | ABSTRACT By using a multicomponent reaction involving isatins, diamines or aminoalcohols, activated acetylenic compounds, haloketones, and ammonium acetate in aqueous media in the presence of Cu@Fe 3 O 4 /SiO 2 @MWCNTs as new catalyst, the novel pyridopyrroloindole was produced in high yields. This catalyst was produced by employing Petasites hybridus rhizome water extract as a green media and moderate base. The pyridopyrroloindole derivatives were newly synthesized compounds, and their antioxidant properties were assessed using the 2,2‐diphenyl‐1‐picrylhydrazyl (DPPH) radical trapping and ferric reducing ability of plasma (FRAP) experiments. The pyridopyrroloindole 6b showed higher performance than butylated hydroxytoluene (BHT) and tert‐butylhydroquinone (TBHQ) better results. This method is used to make pyridopyrroloindole derivatives, and it has the advantages of a quick reaction, high yields, and the ability to separate the products easily. |
| Author | Hossaini, Zinatossadat Hojjati, Mahsa Shirangi, Hannaneh Sadat Sheikholeslami‐Farahani, Fatemeh |
| Author_xml | – sequence: 1 givenname: Fatemeh orcidid: 0000-0002-7213-8645 surname: Sheikholeslami‐Farahani fullname: Sheikholeslami‐Farahani, Fatemeh organization: Department of Chemistry, Firoozkooh Branch Islamic Azad University Firoozkooh Iran – sequence: 2 givenname: Mahsa orcidid: 0009-0005-1638-8964 surname: Hojjati fullname: Hojjati, Mahsa organization: Department of Natural Sciences, School of Science and Technology The University of Georgia Tbilisi Georgia – sequence: 3 givenname: Hannaneh Sadat orcidid: 0009-0002-3255-2814 surname: Shirangi fullname: Shirangi, Hannaneh Sadat organization: Department of Chemistry, Gorgan Branch Islamic Azad University Gorgan Iran – sequence: 4 givenname: Zinatossadat orcidid: 0000-0001-7193-1759 surname: Hossaini fullname: Hossaini, Zinatossadat organization: Department of Chemistry, Qaemshahr Branch Islamic Azad University Qaemshahr Iran |
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