气相色谱-串联质谱法测定化妆品中24种致敏芳香化合物
TQ658; 建立了化妆品中24种致敏芳香化合物的气相色谱-串联质谱(GC-MS/MS)分析方法.化妆品试样经甲醇超声提取,加入无水硫酸钠脱水,经离心过滤后,采用GC-MS/MS进行分析,外标法定量.结果显示,24种致敏芳香化合物的检出限为1～28μg/L,线性范围内相关系数均大于0.995.选取了香水、保湿水、洁面膏3种类型的化妆品作为加标基质来验证方法的准确度,24种致敏芳香化合物的加标回收率为70.1％～119.6％,相对标准偏差为0.8％～7.0％(n=6).该方法准确、灵敏,且前处理简单、快速,适用于化妆品中24种致敏芳香化合物的测定....
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| Published in | 日用化学工业 Vol. 50; no. 10; pp. 725 - 730 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | Chinese |
| Published |
宁波中盛产品检测有限公司,浙江 宁波 315000%宁波海关技术中心,浙江 宁波 315000
22.10.2020
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1001-1803 |
| DOI | 10.3969/j.issn.1001-1803.2020.10.012 |
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| Abstract | TQ658; 建立了化妆品中24种致敏芳香化合物的气相色谱-串联质谱(GC-MS/MS)分析方法.化妆品试样经甲醇超声提取,加入无水硫酸钠脱水,经离心过滤后,采用GC-MS/MS进行分析,外标法定量.结果显示,24种致敏芳香化合物的检出限为1～28μg/L,线性范围内相关系数均大于0.995.选取了香水、保湿水、洁面膏3种类型的化妆品作为加标基质来验证方法的准确度,24种致敏芳香化合物的加标回收率为70.1％～119.6％,相对标准偏差为0.8％～7.0％(n=6).该方法准确、灵敏,且前处理简单、快速,适用于化妆品中24种致敏芳香化合物的测定. |
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| AbstractList | TQ658; 建立了化妆品中24种致敏芳香化合物的气相色谱-串联质谱(GC-MS/MS)分析方法.化妆品试样经甲醇超声提取,加入无水硫酸钠脱水,经离心过滤后,采用GC-MS/MS进行分析,外标法定量.结果显示,24种致敏芳香化合物的检出限为1～28μg/L,线性范围内相关系数均大于0.995.选取了香水、保湿水、洁面膏3种类型的化妆品作为加标基质来验证方法的准确度,24种致敏芳香化合物的加标回收率为70.1％～119.6％,相对标准偏差为0.8％～7.0％(n=6).该方法准确、灵敏,且前处理简单、快速,适用于化妆品中24种致敏芳香化合物的测定. |
| Author | 龙培 郑琳 高佳男 许佳明 吴一鑫 任飞 肖道清 |
| AuthorAffiliation | 宁波中盛产品检测有限公司,浙江 宁波 315000%宁波海关技术中心,浙江 宁波 315000 |
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| Author_FL | ZHENG Lin XU Jia-ming LONG Pei WU Yi-xin GAO Jia-nan REN Fei XIAO Dao-qing |
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| Title | 气相色谱-串联质谱法测定化妆品中24种致敏芳香化合物 |
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