基于压裂废水处理的三元两性聚合物絮凝剂的合成及性能

X703; 利用一种新的阳离子单体3-丙烯酰氧基-2-羟丙基三甲基氯化铵(AHPTAC)与丙烯酰胺(AM)和2-丙烯酰氨基-2-甲基丙磺酸(AMPS)通过水溶液聚合得到一种三元两性共聚物絮凝剂P(AM-AHPTAC-AMPS)(PAAA),将PAAA与聚合氯化铝铁(PAFC)复配用于处理两种压裂废水,并比较评价其与阳离子聚丙烯酰胺(CPAM)的絮凝性能.结果 表明:合成PAAA的最适宜条件为AM、AHPTAC和AMPS的物质的量之比为1∶3∶2、单体总用量占反应体系的质量比为20％、复合引发剂VA-044与(NH4)2S2O8-NaHSO3质量比为1∶1、复合引发剂用量占反应体系的质量比为0....

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Published in中国石油大学学报（自然科学版） Vol. 44; no. 2; pp. 151 - 157
Main Authors 祝威, 李明轩, 韩霞, 王芳, 王田丽, 丁一, 张龙力, 姜翠玉
Format Journal Article
LanguageChinese
Published 中国石化节能环保工程科技有限公司,湖北武汉430223%中国石油大学(华东)理学院,山东青岛266580 20.04.2020
Subjects
压裂废水
3-丙烯酰氧基-2-羟丙基三甲基氯化铵
絮凝性能
三元共聚
两性聚丙烯酰胺絮凝剂
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ISSN1673-5005
DOI10.3969/j.issn.1673-5005.2020.02.019

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Abstract X703; 利用一种新的阳离子单体3-丙烯酰氧基-2-羟丙基三甲基氯化铵(AHPTAC)与丙烯酰胺(AM)和2-丙烯酰氨基-2-甲基丙磺酸(AMPS)通过水溶液聚合得到一种三元两性共聚物絮凝剂P(AM-AHPTAC-AMPS)(PAAA),将PAAA与聚合氯化铝铁(PAFC)复配用于处理两种压裂废水,并比较评价其与阳离子聚丙烯酰胺(CPAM)的絮凝性能.结果 表明:合成PAAA的最适宜条件为AM、AHPTAC和AMPS的物质的量之比为1∶3∶2、单体总用量占反应体系的质量比为20％、复合引发剂VA-044与(NH4)2S2O8-NaHSO3质量比为1∶1、复合引发剂用量占反应体系的质量比为0.2％、反应温度为55℃;PAAA/PAFC复合絮凝剂具有较好的絮凝性能,对胜利孤岛压裂废水及涪陵页岩气压裂废水的CODCr去除率分别为55.5％和82.7％;对水溶性有机污染物质含量高的废水去除效果更优,CODCr去除率比CPAM/PAFC提高26％.
AbstractList X703; 利用一种新的阳离子单体3-丙烯酰氧基-2-羟丙基三甲基氯化铵(AHPTAC)与丙烯酰胺(AM)和2-丙烯酰氨基-2-甲基丙磺酸(AMPS)通过水溶液聚合得到一种三元两性共聚物絮凝剂P(AM-AHPTAC-AMPS)(PAAA),将PAAA与聚合氯化铝铁(PAFC)复配用于处理两种压裂废水,并比较评价其与阳离子聚丙烯酰胺(CPAM)的絮凝性能.结果 表明:合成PAAA的最适宜条件为AM、AHPTAC和AMPS的物质的量之比为1∶3∶2、单体总用量占反应体系的质量比为20％、复合引发剂VA-044与(NH4)2S2O8-NaHSO3质量比为1∶1、复合引发剂用量占反应体系的质量比为0.2％、反应温度为55℃;PAAA/PAFC复合絮凝剂具有较好的絮凝性能,对胜利孤岛压裂废水及涪陵页岩气压裂废水的CODCr去除率分别为55.5％和82.7％;对水溶性有机污染物质含量高的废水去除效果更优,CODCr去除率比CPAM/PAFC提高26％.
Author 姜翠玉
王芳
丁一
韩霞
王田丽
李明轩
张龙力
祝威
AuthorAffiliation 中国石化节能环保工程科技有限公司,湖北武汉430223%中国石油大学(华东)理学院,山东青岛266580
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Author_FL WANG Fang
HAN Xia
WANG Tianli
LI Mingxuan
DING Yi
ZHU Wei
JIANG Cuiyu
ZHANG Longli
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Keywords 压裂废水
3-丙烯酰氧基-2-羟丙基三甲基氯化铵
絮凝性能
三元共聚
两性聚丙烯酰胺絮凝剂
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PublicationTitle 中国石油大学学报（自然科学版）
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Publisher 中国石化节能环保工程科技有限公司,湖北武汉430223%中国石油大学(华东)理学院,山东青岛266580
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