基于HS-SPME-GC-MS和OAV分析不同干燥方式菊花脑的挥发性物质差异

TS255.3; 通过顶空固相微萃取结合气相色谱-质谱(headspace solid phase microextraction-gas chromatography-mass spectrometry,HS-SPME-GC-MS)联用法对热风干燥、真空冷冻干燥、微波-热风联合干燥菊花脑挥发性物质进行定性以及定量,明确干燥方式对菊花脑挥发性物质的影响,并探索菊花脑的关键呈香物质.结果表明:菊花脑中共分离出140种物质,新鲜菊花脑中检出112种物质,热风干燥样品中检出86种物质,微波-热风联合干燥样品中检出83种物质,真空冷冻干燥样品中检出85种物质,分别为萜烯类、酯类、醛类、醇类、芳香族化合...

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Published in食品科学 Vol. 44; no. 8; pp. 228 - 237
Main Authors 吴玉珍, 王洁琼, 余海涛, 余晓玉, 郁志芳
Format Magazine Article
LanguageChinese
Published 南京农业大学食品科技学院,江苏南京 210000 2023
Subjects
气相色谱-质谱
电子鼻
挥发性物质
菊花脑
干燥方式
差异分析
Online AccessGet full text
ISSN1002-6630
DOI10.7506/spkx1002-6630-20220328-350

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Abstract TS255.3; 通过顶空固相微萃取结合气相色谱-质谱(headspace solid phase microextraction-gas chromatography-mass spectrometry,HS-SPME-GC-MS)联用法对热风干燥、真空冷冻干燥、微波-热风联合干燥菊花脑挥发性物质进行定性以及定量,明确干燥方式对菊花脑挥发性物质的影响,并探索菊花脑的关键呈香物质.结果表明:菊花脑中共分离出140种物质,新鲜菊花脑中检出112种物质,热风干燥样品中检出86种物质,微波-热风联合干燥样品中检出83种物质,真空冷冻干燥样品中检出85种物质,分别为萜烯类、酯类、醛类、醇类、芳香族化合物以及其他类共六大类物质.萜烯类含量最高,分别在新鲜菊花脑中检出229 474.33 μg/kg,热风干燥样品中检出64 629.68 μg/kg,微波-热风联合干燥样品中检出56 469.88 μg/kg,真空冷冻干燥样品中检出70 832.87 μg/kg.与另两种干燥方式对比,真空冷冻干燥较好地保留了挥发性物质的丰度.真空冷冻干燥菊花脑与新鲜菊花脑风味相似,主要呈樟脑、松节油以及花草的清香.GC-MS结合气味活度值分析,明确β-罗勒烯、石竹烯以及反式-β-法尼烯是构成菊花脑香气的主要成分.电子鼻与GC-MS联合建立了一种菊花脑挥发性物质高效无损的检测分析方法,可实现不同干燥方式菊花脑的区别判断.本研究结果为明确干燥后菊花脑中挥发性物质的差异及菊花脑干燥方式的选择提供一定理论依据.
AbstractList TS255.3; 通过顶空固相微萃取结合气相色谱-质谱(headspace solid phase microextraction-gas chromatography-mass spectrometry,HS-SPME-GC-MS)联用法对热风干燥、真空冷冻干燥、微波-热风联合干燥菊花脑挥发性物质进行定性以及定量,明确干燥方式对菊花脑挥发性物质的影响,并探索菊花脑的关键呈香物质.结果表明:菊花脑中共分离出140种物质,新鲜菊花脑中检出112种物质,热风干燥样品中检出86种物质,微波-热风联合干燥样品中检出83种物质,真空冷冻干燥样品中检出85种物质,分别为萜烯类、酯类、醛类、醇类、芳香族化合物以及其他类共六大类物质.萜烯类含量最高,分别在新鲜菊花脑中检出229 474.33 μg/kg,热风干燥样品中检出64 629.68 μg/kg,微波-热风联合干燥样品中检出56 469.88 μg/kg,真空冷冻干燥样品中检出70 832.87 μg/kg.与另两种干燥方式对比,真空冷冻干燥较好地保留了挥发性物质的丰度.真空冷冻干燥菊花脑与新鲜菊花脑风味相似,主要呈樟脑、松节油以及花草的清香.GC-MS结合气味活度值分析,明确β-罗勒烯、石竹烯以及反式-β-法尼烯是构成菊花脑香气的主要成分.电子鼻与GC-MS联合建立了一种菊花脑挥发性物质高效无损的检测分析方法,可实现不同干燥方式菊花脑的区别判断.本研究结果为明确干燥后菊花脑中挥发性物质的差异及菊花脑干燥方式的选择提供一定理论依据.
Author 王洁琼
余晓玉
吴玉珍
余海涛
郁志芳
AuthorAffiliation 南京农业大学食品科技学院,江苏南京 210000
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YU Xiaoyu
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YU Zhifang
YU Haitao
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DocumentTitle_FL Analysis of Volatile Components in Chrysanthemum nankingense Leaves Dried by Different Methods by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry and Calculation of Odor Activity Value
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Keywords 气相色谱-质谱
电子鼻
挥发性物质
菊花脑
干燥方式
差异分析
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StartPage 228
Title 基于HS-SPME-GC-MS和OAV分析不同干燥方式菊花脑的挥发性物质差异
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