血清中医薬品のスクリーニングを目的としたミックスモード型固相抽出法の検討

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Published in日本鑑識科学技術学会誌 Vol. 9; no. 1; pp. 71 - 78
Main Authors 金森, 達之, 岩田, 祐子, 井上, 博之, 辻川, 健治, 岸, 徹, 大前, 義仁, 桑山, 健次
Format Journal Article
LanguageJapanese
Published 日本法科学技術学会 2004
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ISSN1342-8713
1882-2827
DOI10.3408/jasti.9.71

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Author 辻川, 健治
桑山, 健次
大前, 義仁
岩田, 祐子
金森, 達之
岸, 徹
井上, 博之
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  fullname: 大前, 義仁
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References 12) Clauwaert, K. M., Van Bocxlaer, J. F., Lambert, W. E., Van den Eeckhout, E. G. and Lemiere, F.: Narrow-bore HPLC in combination with fluorescence and electrospray mass spectrometric detection for the analysis of cocaine and metabolites in human hair. Anal. Chem., 70, 2336-2344 (1998).
15) Baselt, R. C.: Disposition of Toxic Drugs and Chemicals in Man Fifth Ed., Chemical Toxicology Institute, California, (2000).
10) Nguyen, H. and Nau, D. R.: Rapid method for the solid-phase extraction and GC-MS analysis of flunitrazepam and its major metabolites in urine. J. Anal. Toxicol., 24, 37-45 (2000).
9) Black, D. A., Clark, G. D., Haver, V. M., Garbin, J. A. and Saxon, A. J.: Analysis of urinary benzodiazepines using solid-phase extraction and gas chromatography-mass spectrometry. J. Anal. Toxicol., 18, 185-188 (1994).
4) Liu, R. H. and Gadzala, D. E.: Sample pretreatment. In: Handbook of Drug Analysis, pp. 35-53, American Chemical Society, Washington, DC, (1997).
2) Huck, C. W. and Bonn, G. K.: Recent developments in polymer-based sorbents for solid-phase extraction. J. Chromatogr. A, 885, 51-72 (2000).
7) Chen, X-H., Franke, J-P., Wijsbeek, J. and de Zeeuw, R. A.: Isolation of acidic, neutral and basic drugs from whole blood using a single mixed-mode solid-phase extraction column. J. Anal. Toxicol., 16, 351-355 (1992).
11) Soriano, T., Jurado, C., Menendez, M. and Repetto, M.: Improved solid-phase extraction method for systematic toxicological analysis in biological fluids. J. Anal. Toxicol., 25, 137-143 (2001).
16) Saito, T., Kusakabe, T., Jin, Z. B., Hasegawa, I., Yukawa, N. and Takeichi, S.: Determination of ten benzodiazepines in human whole blood by capillary gas chromatography with micro-electron capture detection. Jpn. J. Forensic Toxicol., 20, 268-276 (2002).
13) Yawney, J., Treacy, S., Hindmarsh, K. W. and Burczynski, F. J.: A general screening method for acidic, neutral and basic drugs in whole blood using the Oasis MCX® column. J. Anal. Toxicol., 26, 325-332 (2002).
3) 日本薬学会編：薬毒物化学試験法と注解　第 4 版（1992).
5) Pocci, R., Dixit, V. and Dixit, V. M.: Solid-phase extraction and GC/MS confirmation of barbiturates from human urine. J. Anal. Toxicol., 16, 45-47 (1992).
14) Bogusz, M. J., Maier, R.-D., Schiwy-Bochat, K.-H. and Kohis, U.: Applicability of various brands of mixed-phase extraction columns for opiate extraction from blood and serum. J. Chromatogr. B, 683, 177-188 (1996).
1) 科警研資料：薬物による中毒事故等の発生状況(平成12.1～平成12.12) 第44報（2002).
6) Chen, X-H., Wijsbeek, J., Veen, J. V., Franke, J-P. and de Zeeuw, R. A.: Solid-phase extraction for the screening of acidic, neutral and basic drugs in plasma using a single-column procedure on Bond Elut Certify. J. Chromatogr., 529, 161-166 (1990).
8) Chen, X-H., Wijsbeek, J., Franke, J-P. and de Zeeuw, R. A.: A single-column procedure on Bond Elut Certify for systematic toxicological analysis of drugs in plasma and urine. J. Forensic Sci., 37, 61-71 (1992).
References_xml – reference: 1) 科警研資料：薬物による中毒事故等の発生状況(平成12.1～平成12.12) 第44報（2002).
– reference: 16) Saito, T., Kusakabe, T., Jin, Z. B., Hasegawa, I., Yukawa, N. and Takeichi, S.: Determination of ten benzodiazepines in human whole blood by capillary gas chromatography with micro-electron capture detection. Jpn. J. Forensic Toxicol., 20, 268-276 (2002).
– reference: 12) Clauwaert, K. M., Van Bocxlaer, J. F., Lambert, W. E., Van den Eeckhout, E. G. and Lemiere, F.: Narrow-bore HPLC in combination with fluorescence and electrospray mass spectrometric detection for the analysis of cocaine and metabolites in human hair. Anal. Chem., 70, 2336-2344 (1998).
– reference: 8) Chen, X-H., Wijsbeek, J., Franke, J-P. and de Zeeuw, R. A.: A single-column procedure on Bond Elut Certify for systematic toxicological analysis of drugs in plasma and urine. J. Forensic Sci., 37, 61-71 (1992).
– reference: 15) Baselt, R. C.: Disposition of Toxic Drugs and Chemicals in Man Fifth Ed., Chemical Toxicology Institute, California, (2000).
– reference: 7) Chen, X-H., Franke, J-P., Wijsbeek, J. and de Zeeuw, R. A.: Isolation of acidic, neutral and basic drugs from whole blood using a single mixed-mode solid-phase extraction column. J. Anal. Toxicol., 16, 351-355 (1992).
– reference: 4) Liu, R. H. and Gadzala, D. E.: Sample pretreatment. In: Handbook of Drug Analysis, pp. 35-53, American Chemical Society, Washington, DC, (1997).
– reference: 5) Pocci, R., Dixit, V. and Dixit, V. M.: Solid-phase extraction and GC/MS confirmation of barbiturates from human urine. J. Anal. Toxicol., 16, 45-47 (1992).
– reference: 6) Chen, X-H., Wijsbeek, J., Veen, J. V., Franke, J-P. and de Zeeuw, R. A.: Solid-phase extraction for the screening of acidic, neutral and basic drugs in plasma using a single-column procedure on Bond Elut Certify. J. Chromatogr., 529, 161-166 (1990).
– reference: 14) Bogusz, M. J., Maier, R.-D., Schiwy-Bochat, K.-H. and Kohis, U.: Applicability of various brands of mixed-phase extraction columns for opiate extraction from blood and serum. J. Chromatogr. B, 683, 177-188 (1996).
– reference: 9) Black, D. A., Clark, G. D., Haver, V. M., Garbin, J. A. and Saxon, A. J.: Analysis of urinary benzodiazepines using solid-phase extraction and gas chromatography-mass spectrometry. J. Anal. Toxicol., 18, 185-188 (1994).
– reference: 3) 日本薬学会編：薬毒物化学試験法と注解　第 4 版（1992).
– reference: 2) Huck, C. W. and Bonn, G. K.: Recent developments in polymer-based sorbents for solid-phase extraction. J. Chromatogr. A, 885, 51-72 (2000).
– reference: 10) Nguyen, H. and Nau, D. R.: Rapid method for the solid-phase extraction and GC-MS analysis of flunitrazepam and its major metabolites in urine. J. Anal. Toxicol., 24, 37-45 (2000).
– reference: 11) Soriano, T., Jurado, C., Menendez, M. and Repetto, M.: Improved solid-phase extraction method for systematic toxicological analysis in biological fluids. J. Anal. Toxicol., 25, 137-143 (2001).
– reference: 13) Yawney, J., Treacy, S., Hindmarsh, K. W. and Burczynski, F. J.: A general screening method for acidic, neutral and basic drugs in whole blood using the Oasis MCX® column. J. Anal. Toxicol., 26, 325-332 (2002).
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Title 血清中医薬品のスクリーニングを目的としたミックスモード型固相抽出法の検討
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