Superparamagnetic CuFeO2 Nanoparticles in Deep Eutectic Solvent: an Efficient and Recyclable Catalytic System for the Synthesis of Imidazo[1,2-a]pyridines
Superparamagnetic CuFeO2 nanoparticles were prepared and characterized by XRD, SEM, TEM, FRIR spectroscopy, and vibrating sample magnetometry techniques. The catalytic activity of CuFeO2 nanoparticles was investigated in the one‐pot, three‐component reaction of 2‐aminopyridines, aldehydes, and alkyn...
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Published in | ChemCatChem Vol. 6; no. 10; pp. 2854 - 2859 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Abstract | Superparamagnetic CuFeO2 nanoparticles were prepared and characterized by XRD, SEM, TEM, FRIR spectroscopy, and vibrating sample magnetometry techniques. The catalytic activity of CuFeO2 nanoparticles was investigated in the one‐pot, three‐component reaction of 2‐aminopyridines, aldehydes, and alkynes using citric acid–dimethylurea melt as a green solvent. An array of imidazo[1,2‐a]pyridines were obtained in good to excellent yields. The catalytic system can be successfully reused six times with keeping its catalytic performance.
Green solvent and efficient catalyst: A recyclable catalytic system comprising magnetically recoverable CuFeO2 nanoparticles in a citric acid–dimethylurea melt is established as an efficient and environmentally friendly system for the one‐pot synthesis of imidazo[1,2‐a]pyridines. |
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AbstractList | Superparamagnetic CuFeO2 nanoparticles were prepared and characterized by XRD, SEM, TEM, FRIR spectroscopy, and vibrating sample magnetometry techniques. The catalytic activity of CuFeO2 nanoparticles was investigated in the one-pot, three-component reaction of 2-aminopyridines, aldehydes, and alkynes using citric acid-dimethylurea melt as a green solvent. An array of imidazo[1,2-a]pyridines were obtained in good to excellent yields. The catalytic system can be successfully reused six times with keeping its catalytic performance. [PUBLICATION ABSTRACT] Superparamagnetic CuFeO2 nanoparticles were prepared and characterized by XRD, SEM, TEM, FRIR spectroscopy, and vibrating sample magnetometry techniques. The catalytic activity of CuFeO2 nanoparticles was investigated in the one‐pot, three‐component reaction of 2‐aminopyridines, aldehydes, and alkynes using citric acid–dimethylurea melt as a green solvent. An array of imidazo[1,2‐a]pyridines were obtained in good to excellent yields. The catalytic system can be successfully reused six times with keeping its catalytic performance. Green solvent and efficient catalyst: A recyclable catalytic system comprising magnetically recoverable CuFeO2 nanoparticles in a citric acid–dimethylurea melt is established as an efficient and environmentally friendly system for the one‐pot synthesis of imidazo[1,2‐a]pyridines. |
Author | Ma, Er-Qian Lu, Jun Li, Xiao-Tang Mo, Li-Ping Zhang, Zhan-Hui |
Author_xml | – sequence: 1 givenname: Jun surname: Lu fullname: Lu, Jun organization: College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024 (P.R. China), Fax: (+86) 311-80787431 – sequence: 2 givenname: Xiao-Tang surname: Li fullname: Li, Xiao-Tang organization: College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024 (P.R. China), Fax: (+86) 311-80787431 – sequence: 3 givenname: Er-Qian surname: Ma fullname: Ma, Er-Qian organization: College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024 (P.R. China), Fax: (+86) 311-80787431 – sequence: 4 givenname: Li-Ping surname: Mo fullname: Mo, Li-Ping organization: College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024 (P.R. China), Fax: (+86) 311-80787431 – sequence: 5 givenname: Zhan-Hui surname: Zhang fullname: Zhang, Zhan-Hui email: zhanhui@mail.nankai.edu.cn organization: College of Chemistry & Material Science, Hebei Normal University, Shijiazhuang 050024 (P.R. China), Fax: (+86) 311-80787431 |
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Snippet | Superparamagnetic CuFeO2 nanoparticles were prepared and characterized by XRD, SEM, TEM, FRIR spectroscopy, and vibrating sample magnetometry techniques. The... |
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SubjectTerms | copper heterocycles iron magnetic properties multicomponent reactions Nanoparticles |
Title | Superparamagnetic CuFeO2 Nanoparticles in Deep Eutectic Solvent: an Efficient and Recyclable Catalytic System for the Synthesis of Imidazo[1,2-a]pyridines |
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