High Reversible Lithium Storage Capacity and Structural Changes of Fe2O3 Nanoparticles Confined inside Carbon Nanotubes
The structural evolution of electrochemically prelithiated Fe2O3 nanoparticles confined in carbon nanotubes (CNTs) during lithium insertion/extraction is studied by in situ transmission electron microscopy. It is found that the aggregation and coarsening of Fe core‐containing Li2O (Fe@Li2O) nanograi...
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| Published in | Advanced energy materials Vol. 6; no. 3 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Blackwell Publishing Ltd
04.02.2016
Wiley Subscription Services, Inc |
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| Abstract | The structural evolution of electrochemically prelithiated Fe2O3 nanoparticles confined in carbon nanotubes (CNTs) during lithium insertion/extraction is studied by in situ transmission electron microscopy. It is found that the aggregation and coarsening of Fe core‐containing Li2O (Fe@Li2O) nanograins formed during the charge process are prevented by the spatial restriction of the CNTs. A high reversible capacity of 2071 mA h g−1 for the encapsulated Fe2O3 nanoparticles in CNTs is demonstrated when the material is used as the anode of lithium ion batteries. This is the highest reversible capacity ever reported for an Fe2O3 electrode. The significantly improved lithium storage capacity of the Fe2O3 nanoparticles is attributed to the extra lithium storage due to the enhanced interfacial lithium storage and reversible reaction of LiOH to form LiH and solid‐electrolyte‐interphase conversion originating from the nanoconfinement of CNTs as well as the very small particle size of the Fe@Li2O nanograins and their good electrical contact with CNTs.
An in situ transmission electron microscopy study reveals that carbon nanotubes (CNTs) accommodate volume expansion of lithiated Fe2O3 nanoparticles and prevent their exfoliation and electrical disconnection, hence leading to improved lithium‐storage performance. A high lithium‐storage‐capacity is achieved for the Fe2O3 confined inside CNTs, due to the enhanced interfacial lithium reaction, reversible reaction of LiOH, and solid‐electrolyte‐interphase conversion by the CNT nanoconfinement. |
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| AbstractList | The structural evolution of electrochemically prelithiated Fe2O3 nanoparticles confined in carbon nanotubes (CNTs) during lithium insertion/extraction is studied by in situ transmission electron microscopy. It is found that the aggregation and coarsening of Fe core-containing Li2O (Fe@Li2O) nanograins formed during the charge process are prevented by the spatial restriction of the CNTs. A high reversible capacity of 2071 mA h g-1 for the encapsulated Fe2O3 nanoparticles in CNTs is demonstrated when the material is used as the anode of lithium ion batteries. This is the highest reversible capacity ever reported for an Fe2O3 electrode. The significantly improved lithium storage capacity of the Fe2O3 nanoparticles is attributed to the extra lithium storage due to the enhanced interfacial lithium storage and reversible reaction of LiOH to form LiH and solid-electrolyte-interphase conversion originating from the nanoconfinement of CNTs as well as the very small particle size of the Fe@Li2O nanograins and their good electrical contact with CNTs. The structural evolution of electrochemically prelithiated Fe2O3 nanoparticles confined in carbon nanotubes (CNTs) during lithium insertion/extraction is studied by in situ transmission electron microscopy. It is found that the aggregation and coarsening of Fe core‐containing Li2O (Fe@Li2O) nanograins formed during the charge process are prevented by the spatial restriction of the CNTs. A high reversible capacity of 2071 mA h g−1 for the encapsulated Fe2O3 nanoparticles in CNTs is demonstrated when the material is used as the anode of lithium ion batteries. This is the highest reversible capacity ever reported for an Fe2O3 electrode. The significantly improved lithium storage capacity of the Fe2O3 nanoparticles is attributed to the extra lithium storage due to the enhanced interfacial lithium storage and reversible reaction of LiOH to form LiH and solid‐electrolyte‐interphase conversion originating from the nanoconfinement of CNTs as well as the very small particle size of the Fe@Li2O nanograins and their good electrical contact with CNTs. An in situ transmission electron microscopy study reveals that carbon nanotubes (CNTs) accommodate volume expansion of lithiated Fe2O3 nanoparticles and prevent their exfoliation and electrical disconnection, hence leading to improved lithium‐storage performance. A high lithium‐storage‐capacity is achieved for the Fe2O3 confined inside CNTs, due to the enhanced interfacial lithium reaction, reversible reaction of LiOH, and solid‐electrolyte‐interphase conversion by the CNT nanoconfinement. |
| Author | Zhang, Lili Li, Feng Yu, Wan-Jing Cheng, Hui-Ming Hou, Peng-Xiang Liu, Chang |
| Author_xml | – sequence: 1 givenname: Wan-Jing surname: Yu fullname: Yu, Wan-Jing organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China – sequence: 2 givenname: Lili surname: Zhang fullname: Zhang, Lili organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China – sequence: 3 givenname: Peng-Xiang surname: Hou fullname: Hou, Peng-Xiang organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China – sequence: 4 givenname: Feng surname: Li fullname: Li, Feng organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China – sequence: 5 givenname: Chang surname: Liu fullname: Liu, Chang email: cliu@imr.ac.cn organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China – sequence: 6 givenname: Hui-Ming surname: Cheng fullname: Cheng, Hui-Ming email: cliu@imr.ac.cn organization: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, 110016, Shenyang, China |
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| Copyright | 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim |
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| Notes | ArticleID:AENM201501755 istex:A347FE223D9C9562C778EFB211BBA23ECCA8DF69 National Natural Science Foundation of China - No. 51102242; No. 51172241; No. 51221264; No. 51272257 Chinese Academy of Sciences - No. KGZD-EW-T06 Ministry of Science and Technology of China - No. 2011CB932601; No. 2011CB932604 ark:/67375/WNG-KCPCXSLB-2 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 |
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| PublicationDate | February 4, 2016 |
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| PublicationPlace | Weinheim |
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| PublicationTitle | Advanced energy materials |
| PublicationTitleAlternate | Adv. Energy Mater |
| PublicationYear | 2016 |
| Publisher | Blackwell Publishing Ltd Wiley Subscription Services, Inc |
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| Snippet | The structural evolution of electrochemically prelithiated Fe2O3 nanoparticles confined in carbon nanotubes (CNTs) during lithium insertion/extraction is... |
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| SubjectTerms | Carbon nanotubes Coarsening confinement effects Electric contacts Electron microscopy Fe2O3 nanoparticles Hematite in situ TEM Iron oxides Lithium Lithium-ion batteries Nanoparticles Nanotubes Storage capacity Transmission electron microscopy |
| Title | High Reversible Lithium Storage Capacity and Structural Changes of Fe2O3 Nanoparticles Confined inside Carbon Nanotubes |
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