High pressure synthesis of LiMeO2-ZnO (Me=Fe 3+, Ti3+) solid solutions with a rock salt structure
Metastable LiMeO 2 -ZnO (Me=Fe 3+ , Ti 3+ ) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with LiMeO 2 complex oxides at 7.7 GPa and 1350-1450 K. The structure, phase composition, thermal stability and thermal expansion of the recovered s...
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| Published in | High pressure research Vol. 31; no. 2; pp. 304 - 309 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Taylor & Francis
01.06.2011
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Metastable LiMeO
2
-ZnO (Me=Fe
3+
, Ti
3+
) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with LiMeO
2
complex oxides at 7.7 GPa and 1350-1450 K. The structure, phase composition, thermal stability and thermal expansion of the recovered samples have been studied by X-ray diffraction with synchrotron radiation. At ambient pressure, rock salt LiMeO
2
-ZnO solid solutions are kinetically stable up to 670-800 K, depending on the composition. |
|---|---|
| AbstractList | Metastable LiMeO2-ZnO (Me=Fe 3+, Ti3+) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with LiMeO2 complex oxides at 7.7GPa and 1350-1450K. The structure, phase composition, thermal stability and thermal expansion of the recovered samples have been studied by X-ray diffraction with synchrotron radiation. At ambient pressure, rock salt LiMeO2-ZnO solid solutions are kinetically stable up to 670-800K, depending on the composition. Metastable LiMeO 2 -ZnO (Me=Fe 3+ , Ti 3+ ) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with LiMeO 2 complex oxides at 7.7 GPa and 1350-1450 K. The structure, phase composition, thermal stability and thermal expansion of the recovered samples have been studied by X-ray diffraction with synchrotron radiation. At ambient pressure, rock salt LiMeO 2 -ZnO solid solutions are kinetically stable up to 670-800 K, depending on the composition. |
| Author | Sokolov, P. S. Solozhenko, V. L. Baranov, A. N. Tafeenko, V. A. |
| Author_xml | – sequence: 1 givenname: P. S. surname: Sokolov fullname: Sokolov, P. S. organization: Chemistry Department , Moscow State University – sequence: 2 givenname: A. N. surname: Baranov fullname: Baranov, A. N. organization: Chemistry Department , Moscow State University – sequence: 3 givenname: V. A. surname: Tafeenko fullname: Tafeenko, V. A. organization: Chemistry Department , Moscow State University – sequence: 4 givenname: V. L. surname: Solozhenko fullname: Solozhenko, V. L. email: vladimir.solozhenko@univ-paris13.fr organization: LSPM-CNRS , Université Paris Nord |
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| Copyright | Copyright Taylor & Francis Group, LLC 2011 |
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| Snippet | Metastable LiMeO
2
-ZnO (Me=Fe
3+
, Ti
3+
) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with... Metastable LiMeO2-ZnO (Me=Fe 3+, Ti3+) solid solutions with a rock salt crystal structure have been synthesized by the solid-state reaction of ZnO with LiMeO2... |
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| StartPage | 304 |
| SubjectTerms | chemical synthesis Crystal structure Diffraction high pressure high temperature Oxides Rock salt Solid solutions Synchrotron radiation Synthesis X-ray diffraction X-rays |
| Title | High pressure synthesis of LiMeO2-ZnO (Me=Fe 3+, Ti3+) solid solutions with a rock salt structure |
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