Inserting CO2 into Aryl C−H Bonds of Metal-Organic Frameworks: CO2 Utilization for Direct Heterogeneous C−H Activation
Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C−H bonds of the backbone of a metal–organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work deli...
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| Published in | Angewandte Chemie International Edition Vol. 55; no. 18; pp. 5472 - 5476 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Blackwell Publishing Ltd
25.04.2016
Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1433-7851 1521-3773 1521-3773 |
| DOI | 10.1002/anie.201511484 |
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| Abstract | Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C−H bonds of the backbone of a metal–organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C−H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions.
Framed: CO2 is utilized for heterogeneous C−H activation and carboxylation reactions on metal–organic frameworks (MOFs). The formed carboxylate groups serve as Brønsted acid sites and were shown to efficiently catalyze the methanolysis of epoxides. This work introduces a new avenue for CO2 chemical transformations under mild reaction conditions. |
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| AbstractList | Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C-H bonds of the backbone of a metal-organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C-H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions. Described for the first time is that carbon dioxide (CO2 ) can be successfully inserted into aryl C-H bonds of the backbone of a metal-organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C-H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions.Described for the first time is that carbon dioxide (CO2 ) can be successfully inserted into aryl C-H bonds of the backbone of a metal-organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C-H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions. Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C−H bonds of the backbone of a metal–organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C−H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions. Framed: CO2 is utilized for heterogeneous C−H activation and carboxylation reactions on metal–organic frameworks (MOFs). The formed carboxylate groups serve as Brønsted acid sites and were shown to efficiently catalyze the methanolysis of epoxides. This work introduces a new avenue for CO2 chemical transformations under mild reaction conditions. Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C−H bonds of the backbone of a metal–organic framework (MOF) to generate free carboxylate groups, which serve as Brønsted acid sites for efficiently catalyzing the methanolysis of epoxides. The work delineates the very first example of utilizing CO2 for heterogeneous C−H activation and carboxylation reactions on MOFs, and opens a new avenue for CO2 chemical transformations under mild reaction conditions. |
| Author | Leng, Kunyue Wu, Haifan Ma, Shengqian Gao, Wen-Yang Sun, Yinyong |
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| Keywords | X-ray diffraction C−H activation heterogeneous catalysis carbon dioxide fixation metal-organic frameworks |
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| Snippet | Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C−H bonds of the backbone of a metal–organic framework (MOF)... Described for the first time is that carbon dioxide (CO2 ) can be successfully inserted into aryl C-H bonds of the backbone of a metal-organic framework (MOF)... Described for the first time is that carbon dioxide (CO2) can be successfully inserted into aryl C-H bonds of the backbone of a metal-organic framework (MOF)... |
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| SubjectTerms | Aromatic compounds Carbon dioxide carbon dioxide fixation Carboxylation Chemical reactions C−H activation Epoxides heterogeneous catalysis Metal-organic frameworks Methanolysis X-ray diffraction |
| Title | Inserting CO2 into Aryl C−H Bonds of Metal-Organic Frameworks: CO2 Utilization for Direct Heterogeneous C−H Activation |
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