Thermal and mechanical behavior of ZrTiO4-TiO2 porous ceramics by direct foaming
This paper reports the production of micro porous ceramics consisting of TiO2 and ZrO2 by direct foaming. ZrO2 particles in a colloidal suspension were partially hydrophobized using propyl gallate as an amphiphile at a suitable pH range of around 3.5–4.5. A TiO2 suspension with different mole ratios...
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| Published in | Ceramics international Vol. 42; no. 13; pp. 14395 - 14402 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.10.2016
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| Abstract | This paper reports the production of micro porous ceramics consisting of TiO2 and ZrO2 by direct foaming. ZrO2 particles in a colloidal suspension were partially hydrophobized using propyl gallate as an amphiphile at a suitable pH range of around 3.5–4.5. A TiO2 suspension with different mole ratios was added to the surface modified ZrO2 suspension to obtain ZrTiO4-TiO2 porous ceramics in the sintered sample. The influence of the TiO2 content and calcination temperature on the phase transformation, microstructure, and thermal properties of the materials was determined by thermal analysis, X-ray diffraction, field emission scanning electron microscopy, and dilatometry. The crystallization of ZrTiO4 (orthorhombic) was observed at 1100°C on the thermal hysteresis curve due to anisotropic thermal expansion. The compressive load and displacement of the sintered porous ceramics samples were calculated using the Hertzian indentation method. |
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| AbstractList | This paper reports the production of micro porous ceramics consisting of TiO2 and ZrO2 by direct foaming. ZrO2 particles in a colloidal suspension were partially hydrophobized using propyl gallate as an amphiphile at a suitable pH range of around 3.5–4.5. A TiO2 suspension with different mole ratios was added to the surface modified ZrO2 suspension to obtain ZrTiO4-TiO2 porous ceramics in the sintered sample. The influence of the TiO2 content and calcination temperature on the phase transformation, microstructure, and thermal properties of the materials was determined by thermal analysis, X-ray diffraction, field emission scanning electron microscopy, and dilatometry. The crystallization of ZrTiO4 (orthorhombic) was observed at 1100°C on the thermal hysteresis curve due to anisotropic thermal expansion. The compressive load and displacement of the sintered porous ceramics samples were calculated using the Hertzian indentation method. |
| Author | Park, Jung Gyu Lee, Kee Sung Bhaskar, Subhasree Kim, Ik Jin Kim, Suk Young |
| Author_xml | – sequence: 1 givenname: Subhasree surname: Bhaskar fullname: Bhaskar, Subhasree organization: Institute of Processing and Application of Inorganic Materials (PAIM), Department of Materials Science and Engineering, Hanseo University, 46, Hanseo 1-ro, Haemi-myeon, Seosan, Chungcheongnam-do 356-706, Republic of Korea – sequence: 2 givenname: Jung Gyu surname: Park fullname: Park, Jung Gyu organization: Institute of Processing and Application of Inorganic Materials (PAIM), Department of Materials Science and Engineering, Hanseo University, 46, Hanseo 1-ro, Haemi-myeon, Seosan, Chungcheongnam-do 356-706, Republic of Korea – sequence: 3 givenname: Kee Sung surname: Lee fullname: Lee, Kee Sung organization: School of Mechanical Systems Engineering, Kookmin University, 77, Jeongneung-ro, Seongbuk-gu, Seoul 02707, Republic of Korea – sequence: 4 givenname: Suk Young surname: Kim fullname: Kim, Suk Young organization: School of Materials Science & Engineering, Yeungnam University, Gyeongsan, Gyeongbuk, Republic of Korea – sequence: 5 givenname: Ik Jin surname: Kim fullname: Kim, Ik Jin email: ijkim@hanseo.ac.kr organization: Institute of Processing and Application of Inorganic Materials (PAIM), Department of Materials Science and Engineering, Hanseo University, 46, Hanseo 1-ro, Haemi-myeon, Seosan, Chungcheongnam-do 356-706, Republic of Korea |
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| Copyright | 2016 Elsevier Ltd and Techna Group S.r.l. |
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| DOI | 10.1016/j.ceramint.2016.06.019 |
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| Keywords | Quasi-plastic behavior ZrTio4-Tio2 porous ceramics Direct foaming Thermal hysteresis Hertzian indentations |
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| SubjectTerms | Direct foaming Hertzian indentations Quasi-plastic behavior Thermal hysteresis ZrTio4-Tio2 porous ceramics |
| Title | Thermal and mechanical behavior of ZrTiO4-TiO2 porous ceramics by direct foaming |
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