The Effect of Combining Femtosecond Laser and Electron Irradiation on Silica Glass

This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and...

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Published inNanomaterials (Basel, Switzerland) Vol. 14; no. 23; p. 1909
Main Authors Shchedrina, Nadezhda, Allaoui, Roqya, Sosa, Matilde, Nemeth, Gergely, Borondics, Ferenc, Ollier, Nadege, Lancry, Matthieu
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 28.11.2024
MDPI
Subjects
birefringence
Densification
Electron irradiation
femtosecond laser
Harsh environments
High energy electrons
Irradiation
Laser radiation
Lasers
Light microscopy
Microscopy
nanogratings
Optical microscopy
Optical properties
Optics
Periodicity
Plasma
Point defects
Radiation
Retardance
Silica
Silica glass
Silicon
Spectroscopy
Spectrum analysis
type II modifications
France
Germany
type II modifications
nanogratings
electron irradiation
density
femtosecond laser
metamict phase
birefringence
silica glass
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Abstract This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and Raman D band intensity, which is an indicator of local glass densification. S-SNOM and nano-FTIR measurements further revealed changes in the Si-O-Si vibrational bands, indicating partial relaxation of the densified nanolayers under electron irradiation. Our findings reveal significant optical modifications due to subsequent electron irradiation, including reduced retardance and phase values, which are in agreement with the relaxation of the local densification. SEM analysis confirmed the preservation of nanogratings' morphology including their periodicity. Apart from revealing fundamental aspects related to glass densification within nanogratings, this study also underscores the potential of combined fs-laser and electron irradiation techniques in understanding silica glass behavior under high radiation conditions, which is crucial for applications in harsh environments.
AbstractList This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and Raman D band intensity, which is an indicator of local glass densification. S-SNOM and nano-FTIR measurements further revealed changes in the Si-O-Si vibrational bands, indicating partial relaxation of the densified nanolayers under electron irradiation. Our findings reveal significant optical modifications due to subsequent electron irradiation, including reduced retardance and phase values, which are in agreement with the relaxation of the local densification. SEM analysis confirmed the preservation of nanogratings' morphology including their periodicity. Apart from revealing fundamental aspects related to glass densification within nanogratings, this study also underscores the potential of combined fs-laser and electron irradiation techniques in understanding silica glass behavior under high radiation conditions, which is crucial for applications in harsh environments.
This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and Raman D2 band intensity, which is an indicator of local glass densification. S-SNOM and nano-FTIR measurements further revealed changes in the Si–O–Si vibrational bands, indicating partial relaxation of the densified nanolayers under electron irradiation. Our findings reveal significant optical modifications due to subsequent electron irradiation, including reduced retardance and phase values, which are in agreement with the relaxation of the local densification. SEM analysis confirmed the preservation of nanogratings’ morphology including their periodicity. Apart from revealing fundamental aspects related to glass densification within nanogratings, this study also underscores the potential of combined fs-laser and electron irradiation techniques in understanding silica glass behavior under high radiation conditions, which is crucial for applications in harsh environments.
This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and Raman D[sub.2] band intensity, which is an indicator of local glass densification. S-SNOM and nano-FTIR measurements further revealed changes in the Si–O–Si vibrational bands, indicating partial relaxation of the densified nanolayers under electron irradiation. Our findings reveal significant optical modifications due to subsequent electron irradiation, including reduced retardance and phase values, which are in agreement with the relaxation of the local densification. SEM analysis confirmed the preservation of nanogratings’ morphology including their periodicity. Apart from revealing fundamental aspects related to glass densification within nanogratings, this study also underscores the potential of combined fs-laser and electron irradiation techniques in understanding silica glass behavior under high radiation conditions, which is crucial for applications in harsh environments.
This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV, 4.9 GGy) irradiation. Using optical microscopy and spectroscopy techniques, we analyzed retardance, phase shifts, nanograting periodicity, and Raman D 2 band intensity, which is an indicator of local glass densification. S-SNOM and nano-FTIR measurements further revealed changes in the Si–O–Si vibrational bands, indicating partial relaxation of the densified nanolayers under electron irradiation. Our findings reveal significant optical modifications due to subsequent electron irradiation, including reduced retardance and phase values, which are in agreement with the relaxation of the local densification. SEM analysis confirmed the preservation of nanogratings’ morphology including their periodicity. Apart from revealing fundamental aspects related to glass densification within nanogratings, this study also underscores the potential of combined fs-laser and electron irradiation techniques in understanding silica glass behavior under high radiation conditions, which is crucial for applications in harsh environments.
Audience Academic
Author Sosa, Matilde
Borondics, Ferenc
Ollier, Nadege
Shchedrina, Nadezhda
Allaoui, Roqya
Nemeth, Gergely
Lancry, Matthieu
AuthorAffiliation 2 Laboratoire des Solides Irradiés, École Polytechnique-CEA-CNRS, 91128 Palaiseau, France; nadege.ollier@polytechnique.edu
3 Université Paris-Saclay, CEA, List, 91120 Palaiseau, France
4 SMIS Beamline, SOLEIL Synchrotron, L’Orme des Merisiers, RD128, 91190 Saint Aubin, France; gergely.nemeth@synchrotron-soleil.fr (G.N.); ferenc.borondics@synchrotron-soleil.fr (F.B.)
1 Institut de Chimie Moléculaire et des Matériaux d’Orsay, Université Paris-Saclay, Rue du Doyen Georges Poitou, 91405 Orsay, France; allaouiroqya@gmail.com (R.A.); matilde.sosa-marti@universite-paris-saclay.fr (M.S.)
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Issue 23
Keywords type II modifications
nanogratings
electron irradiation
density
femtosecond laser
metamict phase
birefringence
silica glass
Language English
License Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
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Snippet This study investigates the structural and optical responses of silica glass to femtosecond (fs) laser irradiation followed by high-energy electron (2.5 MeV,...
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SubjectTerms birefringence
Densification
Electron irradiation
femtosecond laser
Harsh environments
High energy electrons
Irradiation
Laser radiation
Lasers
Light microscopy
Microscopy
nanogratings
Optical microscopy
Optical properties
Optics
Periodicity
Plasma
Point defects
Radiation
Retardance
Silica
Silica glass
Silicon
Spectroscopy
Spectrum analysis
type II modifications
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Title The Effect of Combining Femtosecond Laser and Electron Irradiation on Silica Glass
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