Effect of the itinerant electron density on the magnetization and Curie temperature of Sr 2 FeMoO 6 ceramics

The itinerant electron density ( n ) near the Fermi level has a close correlation with the physical properties of Sr 2 FeMoO 6 . Two series of single-phase Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) and Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1, 0.2, 0.3) ceramics were specially design...

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Published inRSC advances Vol. 8; no. 51; pp. 29071 - 29077
Main Authors Wang, Jin-Feng, Shi, Teng-Fei, Zhuang, Zhao-Tong, Gao, Qian-Qian, Zhang, Yan-Ming
Format Journal Article
LanguageEnglish
Published England 14.08.2018
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Abstract The itinerant electron density ( n ) near the Fermi level has a close correlation with the physical properties of Sr 2 FeMoO 6 . Two series of single-phase Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) and Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1, 0.2, 0.3) ceramics were specially designed and the itinerant electron density ( n ) of them can be artificially controlled to be: n = 1 − y and n = 1 − y + 3 x = 1 + 0.5 y , respectively. The corresponding crystal structure, magnetization and the ferromagnetic Curie temperature ( T C ) of two subjects were investigated systematically. The X-ray diffraction analysis indicates that Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) have comparable Fe/Mo anti-site defect (ASD) content in spite of decreased n . However, a drastically improved Fe/Mo ASD can be observed in Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1, 0.2, 0.3) caused by the intrinsic wrong occupation of normal Fe sites with excess Mo. Magnetization–magnetic field ( M – H ) behavior confirms that it is the Fe/Mo ASD not n that dominantly determines the magnetization properties. Interestingly, approximately when n ≤ 0.9, T C of Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) exhibits an overall increase with decreasing n , which is contrary to the T C response in electron-doped SFMO. Such abnormal T C is supposed to relate with the ratio variation of n (Mo)/ n (Fe). Moreover, when n ≥ 1, T C of Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.3) exhibits a considerable rise of about 75 K over that of Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1), resulting from improved n caused by introducing excess Mo into Sr (2−y) Na y FeMoO 6 . Maybe, our work can provide an effective strategy to artificially control n and ferromagnetic T C accordingly, and provoke further investigation on the FeMo-baseddouble perovskites.
AbstractList The itinerant electron density ( ) near the Fermi level has a close correlation with the physical properties of Sr FeMoO . Two series of single-phase Sr Na FeMoO ( = 0.1, 0.2, 0.3) and Sr Na Fe Mo O ( = 2 ; = 0.1, 0.2, 0.3) ceramics were specially designed and the itinerant electron density ( ) of them can be artificially controlled to be: = 1 - and = 1 - + 3 = 1 + 0.5 , respectively. The corresponding crystal structure, magnetization and the ferromagnetic Curie temperature ( ) of two subjects were investigated systematically. The X-ray diffraction analysis indicates that Sr Na FeMoO ( = 0.1, 0.2, 0.3) have comparable Fe/Mo anti-site defect (ASD) content in spite of decreased . However, a drastically improved Fe/Mo ASD can be observed in Sr Na Fe Mo O ( = 2 ; = 0.1, 0.2, 0.3) caused by the intrinsic wrong occupation of normal Fe sites with excess Mo. Magnetization-magnetic field ( - ) behavior confirms that it is the Fe/Mo ASD not that dominantly determines the magnetization properties. Interestingly, approximately when ≤ 0.9, of Sr Na FeMoO ( = 0.1, 0.2, 0.3) exhibits an overall increase with decreasing , which is contrary to the response in electron-doped SFMO. Such abnormal is supposed to relate with the ratio variation of (Mo)/ (Fe). Moreover, when ≥ 1, of Sr Na Fe Mo O ( = 2 ; = 0.3) exhibits a considerable rise of about 75 K over that of Sr Na Fe Mo O ( = 2 ; = 0.1), resulting from improved caused by introducing excess Mo into Sr Na FeMoO . Maybe, our work can provide an effective strategy to artificially control and ferromagnetic accordingly, and provoke further investigation on the FeMo-baseddouble perovskites.
The itinerant electron density ( n ) near the Fermi level has a close correlation with the physical properties of Sr 2 FeMoO 6 . Two series of single-phase Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) and Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1, 0.2, 0.3) ceramics were specially designed and the itinerant electron density ( n ) of them can be artificially controlled to be: n = 1 − y and n = 1 − y + 3 x = 1 + 0.5 y , respectively. The corresponding crystal structure, magnetization and the ferromagnetic Curie temperature ( T C ) of two subjects were investigated systematically. The X-ray diffraction analysis indicates that Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) have comparable Fe/Mo anti-site defect (ASD) content in spite of decreased n . However, a drastically improved Fe/Mo ASD can be observed in Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1, 0.2, 0.3) caused by the intrinsic wrong occupation of normal Fe sites with excess Mo. Magnetization–magnetic field ( M – H ) behavior confirms that it is the Fe/Mo ASD not n that dominantly determines the magnetization properties. Interestingly, approximately when n ≤ 0.9, T C of Sr (2−y) Na y FeMoO 6 ( y = 0.1, 0.2, 0.3) exhibits an overall increase with decreasing n , which is contrary to the T C response in electron-doped SFMO. Such abnormal T C is supposed to relate with the ratio variation of n (Mo)/ n (Fe). Moreover, when n ≥ 1, T C of Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.3) exhibits a considerable rise of about 75 K over that of Sr (2−y) Na y Fe (1−x) Mo (1+x) O 6 ( y = 2 x ; y = 0.1), resulting from improved n caused by introducing excess Mo into Sr (2−y) Na y FeMoO 6 . Maybe, our work can provide an effective strategy to artificially control n and ferromagnetic T C accordingly, and provoke further investigation on the FeMo-baseddouble perovskites.
Author Shi, Teng-Fei
Zhuang, Zhao-Tong
Gao, Qian-Qian
Wang, Jin-Feng
Zhang, Yan-Ming
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Snippet The itinerant electron density ( n ) near the Fermi level has a close correlation with the physical properties of Sr 2 FeMoO 6 . Two series of single-phase Sr...
The itinerant electron density ( ) near the Fermi level has a close correlation with the physical properties of Sr FeMoO . Two series of single-phase Sr Na...
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StartPage 29071
Title Effect of the itinerant electron density on the magnetization and Curie temperature of Sr 2 FeMoO 6 ceramics
URI https://www.ncbi.nlm.nih.gov/pubmed/35547967
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