Induced core-shell structure and the electric properties of (K 0.48 Na 0.52 ) 0.95 Li 0.05 Nb 0.95 Sb 0.05 O 3 ceramics

The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K Na ) Li Nb Sb O (x = 0.04, 0.00, -0.02, -0.04 and -0.08) ceramics. For x = -0.02 and -0.04, larger coercive fields and lower remnant polarizations were obtained; besides, an additio...

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Published inPhysical chemistry chemical physics : PCCP Vol. 19; no. 3; pp. 1868 - 1874
Main Authors Zhou, Min, Lu, Xiaomei, Yang, Dianyuan, He, Ju, Huang, Fengzhen, Mei, Fang, Ren, Xianming, Xu, Xingyu, Li, Yang, Zhu, Jinsong
Format Journal Article
LanguageEnglish
Published England 18.01.2017
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Abstract The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K Na ) Li Nb Sb O (x = 0.04, 0.00, -0.02, -0.04 and -0.08) ceramics. For x = -0.02 and -0.04, larger coercive fields and lower remnant polarizations were obtained; besides, an additional dielectric relaxation behavior was observed with the activation energy E being about 2.19 eV and 1.92 eV, respectively. Furthermore, the grain and grain boundary contributions to the capacitance were separated using impedance spectroscopy, which, combined with back-scattering characterization, firmly indicates the core-shell structure of K-deficient samples (x = -0.02 and -0.04). Unlike the cores, the shells possess a large amount of K vacancies (). This work paves a way for regulating the fine structure and more on the electrical properties of KNN-based materials.
AbstractList The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K 0.48(1+x) Na 0.52 ) 0.95 Li 0.05 Nb 0.95 Sb 0.05 O 3 ( x = 0.04, 0.00, −0.02, −0.04 and −0.08) ceramics. For x = −0.02 and −0.04, larger coercive fields and lower remnant polarizations were obtained; besides, an additional dielectric relaxation behavior was observed with the activation energy E a being about 2.19 eV and 1.92 eV, respectively. Furthermore, the grain and grain boundary contributions to the capacitance were separated using impedance spectroscopy, which, combined with back-scattering characterization, firmly indicates the core–shell structure of K-deficient samples ( x = −0.02 and −0.04). Unlike the cores, the shells possess a large amount of K + vacancies ( ). This work paves a way for regulating the fine structure and more on the electrical properties of KNN-based materials.
The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K Na ) Li Nb Sb O (x = 0.04, 0.00, -0.02, -0.04 and -0.08) ceramics. For x = -0.02 and -0.04, larger coercive fields and lower remnant polarizations were obtained; besides, an additional dielectric relaxation behavior was observed with the activation energy E being about 2.19 eV and 1.92 eV, respectively. Furthermore, the grain and grain boundary contributions to the capacitance were separated using impedance spectroscopy, which, combined with back-scattering characterization, firmly indicates the core-shell structure of K-deficient samples (x = -0.02 and -0.04). Unlike the cores, the shells possess a large amount of K vacancies (). This work paves a way for regulating the fine structure and more on the electrical properties of KNN-based materials.
Author Huang, Fengzhen
Xu, Xingyu
Yang, Dianyuan
Zhou, Min
Mei, Fang
Li, Yang
He, Ju
Zhu, Jinsong
Lu, Xiaomei
Ren, Xianming
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Snippet The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K Na ) Li Nb Sb O (x = 0.04, 0.00, -0.02,...
The relationship among dielectric anomaly, ferroelectric response, defects, and microstructures was established for (K 0.48(1+x) Na 0.52 ) 0.95 Li 0.05 Nb 0.95...
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Title Induced core-shell structure and the electric properties of (K 0.48 Na 0.52 ) 0.95 Li 0.05 Nb 0.95 Sb 0.05 O 3 ceramics
URI https://www.ncbi.nlm.nih.gov/pubmed/28000815
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