Highly efficient activation of sulfite by oxygen vacancies-enriched ZnCe0.4Fe1.6O4 for methylparaben degradation

•ZnCe0.4Fe1.6O4 exhibited a higher catalytic activity than that of ZnFe2O4.•About 85.2 % of MeP was removed in ZnCe0.4Fe1.6O4/PMS system within 60 min.•SO4− and OH was the main reactive oxygen species for MeP degradation.•Oxygen vacancies on ZnCe0.4Fe1.6O4 surface were crucial for sulfite activation...

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Published inChemical engineering journal (Lausanne, Switzerland : 1996) Vol. 494; p. 152901
Main Authors Qin, Hangdao, Hao, Junnan, Cheng, Hao, Huang, Jiming, Wu, Sizhan, Chen, Jing, Shi, Wei
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.08.2024
Subjects
Degradation
Methylparaben
Oxygen vacancy
Sulfite
ZnCe0.4Fe1.6O4
Sulfite
Degradation
ZnCe0.4Fe1.6O4
Methylparaben
Oxygen vacancy
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Abstract •ZnCe0.4Fe1.6O4 exhibited a higher catalytic activity than that of ZnFe2O4.•About 85.2 % of MeP was removed in ZnCe0.4Fe1.6O4/PMS system within 60 min.•SO4− and OH was the main reactive oxygen species for MeP degradation.•Oxygen vacancies on ZnCe0.4Fe1.6O4 surface were crucial for sulfite activation.•The practical application prospect of ZnCe0.4Fe1.6O4/sulfite system was investigated. The exploitation of a novel catalyst was of great significance for sulfate radical-based advanced oxidation processes (AOPs) using sulfite as the precursor of sulfate radical. Herein, oxygen vacancies-enriched ZnCe0.4Fe1.6O4 was prepared and applied to activate sulfite for the degradation of methylparaben (MeP). ZnCe0.4Fe1.6O4 showed superior catalytic activity than that of ZnFe2O4, allowing an 85.2 % removal efficiency of MeP within 60 min. The initial pH showed a significant effect on the catalytic performance, and about 92.1 % of MeP could be removed at pH of 9.56 in ZnCe0.4Fe1.6O4/sulfite system. The quenching experiments and EPR tests verified SO4− and OH were the main reactive oxygen species (ROS) in ZnCe0.4Fe1.6O4/sulfite system. The catalytic mechanism was elucidated further by X-ray photoelectron spectroscopy (XPS) analysis of ZnCe0.4Fe1.6O4 before and after the reaction. The recycles of Zn2+/Zn3+, Fe2+/Fe3+ and Ce3+/Ce4+ were the key factor for the activation of sulfite, and oxygen vacancies on catalyst surface promoted the activation of sulfite. The degradation intermediates of MeP were determined by a liquid chromatography-mass spectrometer (LC-MS) and the degradation pathway was proposed. The reusability of ZnCe0.4Fe1.6O4 was evidenced by the recycling experiments. In addition, ZnCe0.4Fe1.6O4/sulfite system exhibited excellent applicability in treating other organic contaminants.
AbstractList •ZnCe0.4Fe1.6O4 exhibited a higher catalytic activity than that of ZnFe2O4.•About 85.2 % of MeP was removed in ZnCe0.4Fe1.6O4/PMS system within 60 min.•SO4− and OH was the main reactive oxygen species for MeP degradation.•Oxygen vacancies on ZnCe0.4Fe1.6O4 surface were crucial for sulfite activation.•The practical application prospect of ZnCe0.4Fe1.6O4/sulfite system was investigated. The exploitation of a novel catalyst was of great significance for sulfate radical-based advanced oxidation processes (AOPs) using sulfite as the precursor of sulfate radical. Herein, oxygen vacancies-enriched ZnCe0.4Fe1.6O4 was prepared and applied to activate sulfite for the degradation of methylparaben (MeP). ZnCe0.4Fe1.6O4 showed superior catalytic activity than that of ZnFe2O4, allowing an 85.2 % removal efficiency of MeP within 60 min. The initial pH showed a significant effect on the catalytic performance, and about 92.1 % of MeP could be removed at pH of 9.56 in ZnCe0.4Fe1.6O4/sulfite system. The quenching experiments and EPR tests verified SO4− and OH were the main reactive oxygen species (ROS) in ZnCe0.4Fe1.6O4/sulfite system. The catalytic mechanism was elucidated further by X-ray photoelectron spectroscopy (XPS) analysis of ZnCe0.4Fe1.6O4 before and after the reaction. The recycles of Zn2+/Zn3+, Fe2+/Fe3+ and Ce3+/Ce4+ were the key factor for the activation of sulfite, and oxygen vacancies on catalyst surface promoted the activation of sulfite. The degradation intermediates of MeP were determined by a liquid chromatography-mass spectrometer (LC-MS) and the degradation pathway was proposed. The reusability of ZnCe0.4Fe1.6O4 was evidenced by the recycling experiments. In addition, ZnCe0.4Fe1.6O4/sulfite system exhibited excellent applicability in treating other organic contaminants.
ArticleNumber 152901
Author Huang, Jiming
Cheng, Hao
Shi, Wei
Qin, Hangdao
Wu, Sizhan
Hao, Junnan
Chen, Jing
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Keywords Sulfite
Degradation
ZnCe0.4Fe1.6O4
Methylparaben
Oxygen vacancy
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Snippet •ZnCe0.4Fe1.6O4 exhibited a higher catalytic activity than that of ZnFe2O4.•About 85.2 % of MeP was removed in ZnCe0.4Fe1.6O4/PMS system within 60 min.•SO4−...
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StartPage 152901
SubjectTerms Degradation
Methylparaben
Oxygen vacancy
Sulfite
ZnCe0.4Fe1.6O4
Title Highly efficient activation of sulfite by oxygen vacancies-enriched ZnCe0.4Fe1.6O4 for methylparaben degradation
URI https://dx.doi.org/10.1016/j.cej.2024.152901
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