Development of a High-Density Microplasma Emission Source for a Micro Total Analysis System
To achieve a highly sensitive and onsite analysis of a small amount samples, a microplasma-based micro total analysis systems (μ-TAS) device was developed. A dielectric barrier discharge (DBD) that can generate a stable plasma at atmospheric pressure was generated in a microchip and used as the plas...
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Published in | Analytical Sciences Vol. 33; no. 4; pp. 505 - 510 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Singapore
The Japan Society for Analytical Chemistry
2017
Springer Nature Singapore Japan Science and Technology Agency |
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Abstract | To achieve a highly sensitive and onsite analysis of a small amount samples, a microplasma-based micro total analysis systems (μ-TAS) device was developed. A dielectric barrier discharge (DBD) that can generate a stable plasma at atmospheric pressure was generated in a microchip and used as the plasma source. The use of DBD suppresses the temperature rise of the electrodes and enables operation for long times because of a reduction of the electrode damage due to suppression of the current via dielectric interposing between the electrodes. It is expected that the analytical system can be miniaturized because helium plasma is generated in the microchannel contained in the microchip. Emissions from gaseous Cl, Br, and I were analyzed using the plasma source, and it was found that the detection limits for these analytes were 0.22, 0.18, and 0.14 ppm, respectively. The calibration curves for gaseous Cl, Br, and I were also plotted obtaining correlation coefficients of 0.975, 0.955 and 0.986, respectively, and showing good linearity for the developed plasma source. |
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AbstractList | To achieve a highly sensitive and onsite analysis of a small amount samples, a microplasma-based micro total analysis systems (μ-TAS) device was developed. A dielectric barrier discharge (DBD) that can generate a stable plasma at atmospheric pressure was generated in a microchip and used as the plasma source. The use of DBD suppresses the temperature rise of the electrodes and enables operation for long times because of a reduction of the electrode damage due to suppression of the current via dielectric interposing between the electrodes. It is expected that the analytical system can be miniaturized because helium plasma is generated in the microchannel contained in the microchip. Emissions from gaseous Cl, Br, and I were analyzed using the plasma source, and it was found that the detection limits for these analytes were 0.22, 0.18, and 0.14 ppm, respectively. The calibration curves for gaseous Cl, Br, and I were also plotted obtaining correlation coefficients of 0.975, 0.955 and 0.986, respectively, and showing good linearity for the developed plasma source. |
Author | HARIGANE, Ryoto KAKEGAWA, Ken MIYAHARA, Hidekazu OKINO, Akitoshi MARUO, Shoji AIDA, Mari |
Author_xml | – sequence: 1 fullname: KAKEGAWA, Ken organization: Laboratory for Future Interdisciplinary Research of Science and Technology, Tokyo Institute of Technology – sequence: 2 fullname: HARIGANE, Ryoto organization: Department of Mechanical Engineering and Materials Science, Yokohama National University – sequence: 3 fullname: AIDA, Mari organization: Laboratory for Future Interdisciplinary Research of Science and Technology, Tokyo Institute of Technology – sequence: 4 fullname: MIYAHARA, Hidekazu organization: Laboratory for Future Interdisciplinary Research of Science and Technology, Tokyo Institute of Technology – sequence: 5 fullname: MARUO, Shoji organization: Department of Mechanical Engineering and Materials Science, Yokohama National University – sequence: 6 fullname: OKINO, Akitoshi organization: Laboratory for Future Interdisciplinary Research of Science and Technology, Tokyo Institute of Technology |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28392529$$D View this record in MEDLINE/PubMed |
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CitedBy_id | crossref_primary_10_1016_j_infrared_2022_104252 crossref_primary_10_1109_TPS_2020_3020071 crossref_primary_10_1007_s11090_020_10057_3 crossref_primary_10_1039_C7JA00314E crossref_primary_10_5702_massspectrometry_S0075 |
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SubjectTerms | Analytical Chemistry atmospheric plasma Atmospheric pressure atomic emission spectroscopy Chemistry Electrodes Emissions gas analysis Helium Helium plasma micro plasma Micro total analysis systems Microchannels Microplasmas Plasma Semiconductors Temperature effects μ-TAS |
Title | Development of a High-Density Microplasma Emission Source for a Micro Total Analysis System |
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