High-Yield Electrosynthesis of Hydrogen Peroxide from Oxygen Reduction by Hierarchically Porous Carbon
H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost‐effective electrocatalysts for H2O2 synthesis. Here, hie...
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| Published in | Angewandte Chemie International Edition Vol. 54; no. 23; pp. 6837 - 6841 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.06.2015
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost‐effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0–70.2 %, most of them >90.0 % at pH 1–4 and >80.0 % at pH 7). High‐yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6–62.0 mmol L−1 (2.5 h) and corresponding H2O2 production rates of 395.7–110.2 mmol h−1 g−1 at pH 1–7 and −0.5 V. Moreover, HPC was energy‐efficient for H2O2 production with current efficiency of 81.8–70.8 %. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp3‐C and defects, large surface area and fast mass transfer.
The electroreduction of O2 is achieved with hierarchically porous carbon (HPC) to give H2O2. It exhibits good selectivity, a high production rate, and current efficiency for the electrosynthesis of H2O2 at a wide range of pH values. The correlation between H2O2 production rate and sp3‐C atoms and defects was explored. This provides an effective method for tuning the activity of carbon materials for the selective electrosynthesis of H2O2. RE=reference electrode. |
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| AbstractList | H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost-effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0-70.2%, most of them >90.0% at pH 1-4 and >80.0% at pH 7). High-yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6-62.0 mmol L(-1) (2.5 h) and corresponding H2O2 production rates of 395.7-110.2 mmol h(-1) g(-1) at pH 1-7 and -0.5 V. Moreover, HPC was energy-efficient for H2O2 production with current efficiency of 81.8-70.8%. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp(3)-C and defects, large surface area and fast mass transfer. H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost-effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0-70.2%, most of them >90.0% at pH 1-4 and >80.0% at pH 7). High-yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6-62.0 mmol L(-1) (2.5 h) and corresponding H2O2 production rates of 395.7-110.2 mmol h(-1) g(-1) at pH 1-7 and -0.5 V. Moreover, HPC was energy-efficient for H2O2 production with current efficiency of 81.8-70.8%. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp(3)-C and defects, large surface area and fast mass transfer.H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost-effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0-70.2%, most of them >90.0% at pH 1-4 and >80.0% at pH 7). High-yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6-62.0 mmol L(-1) (2.5 h) and corresponding H2O2 production rates of 395.7-110.2 mmol h(-1) g(-1) at pH 1-7 and -0.5 V. Moreover, HPC was energy-efficient for H2O2 production with current efficiency of 81.8-70.8%. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp(3)-C and defects, large surface area and fast mass transfer. H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost-effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0-70.2%, most of them >90.0% at pH1-4 and >80.0% at pH7). High-yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6-62.0mmolL-1 (2.5h) and corresponding H2O2 production rates of 395.7-110.2mmolh-1g-1 at pH1-7 and -0.5V. Moreover, HPC was energy-efficient for H2O2 production with current efficiency of 81.8-70.8%. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp3-C and defects, large surface area and fast mass transfer. H 2 O 2 production by electroreduction of O 2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost‐effective electrocatalysts for H 2 O 2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H 2 O 2 from O 2 reduction. It exhibited high activity for O 2 reduction and good H 2 O 2 selectivity (95.0–70.2 %, most of them >90.0 % at pH 1–4 and >80.0 % at pH 7). High‐yield H 2 O 2 generation has been achieved on HPC with H 2 O 2 concentrations of 222.6–62.0 mmol L −1 (2.5 h) and corresponding H 2 O 2 production rates of 395.7–110.2 mmol h −1 g −1 at pH 1–7 and −0.5 V. Moreover, HPC was energy‐efficient for H 2 O 2 production with current efficiency of 81.8–70.8 %. The exceptional performance of HPC for electrosynthesis of H 2 O 2 could be attributed to its high content of sp 3 ‐C and defects, large surface area and fast mass transfer. H sub(2)O sub(2) production by electroreduction of O sub(2) is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost-effective electrocatalysts for H sub(2)O sub(2) synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H sub(2)O sub(2) from O sub(2) reduction. It exhibited high activity for O sub(2) reduction and good H sub(2)O sub(2) selectivity (95.0-70.2%, most of them >90.0% at pH1-4 and >80.0% at pH7). High-yield H sub(2)O sub(2) generation has been achieved on HPC with H sub(2)O sub(2) concentrations of 222.6-62.0mmolL super(-1) (2.5h) and corresponding H sub(2)O sub(2) production rates of 395.7-110.2mmolh super(-1)g super(-1) at pH1-7 and -0.5V. Moreover, HPC was energy-efficient for H sub(2)O sub(2) production with current efficiency of 81.8-70.8%. The exceptional performance of HPC for electrosynthesis of H sub(2)O sub(2) could be attributed to its high content of sp super(3)-C and defects, large surface area and fast mass transfer. The electroreduction of O sub(2) is achieved with hierarchically porous carbon (HPC) to give H sub(2)O sub(2). It exhibits good selectivity, a high production rate, and current efficiency for the electrosynthesis of H sub(2)O sub(2) at a wide range of pH values. The correlation between H sub(2)O sub(2) production rate and sp super(3)-C atoms and defects was explored. This provides an effective method for tuning the activity of carbon materials for the selective electrosynthesis of H sub(2)O sub(2). RE=reference electrode. H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries and environmental remediation. However, it remains a great challenge to develop cost‐effective electrocatalysts for H2O2 synthesis. Here, hierarchically porous carbon (HPC) was proposed for the electrosynthesis of H2O2 from O2 reduction. It exhibited high activity for O2 reduction and good H2O2 selectivity (95.0–70.2 %, most of them >90.0 % at pH 1–4 and >80.0 % at pH 7). High‐yield H2O2 generation has been achieved on HPC with H2O2 concentrations of 222.6–62.0 mmol L−1 (2.5 h) and corresponding H2O2 production rates of 395.7–110.2 mmol h−1 g−1 at pH 1–7 and −0.5 V. Moreover, HPC was energy‐efficient for H2O2 production with current efficiency of 81.8–70.8 %. The exceptional performance of HPC for electrosynthesis of H2O2 could be attributed to its high content of sp3‐C and defects, large surface area and fast mass transfer. The electroreduction of O2 is achieved with hierarchically porous carbon (HPC) to give H2O2. It exhibits good selectivity, a high production rate, and current efficiency for the electrosynthesis of H2O2 at a wide range of pH values. The correlation between H2O2 production rate and sp3‐C atoms and defects was explored. This provides an effective method for tuning the activity of carbon materials for the selective electrosynthesis of H2O2. RE=reference electrode. |
| Author | Chen, Shuo Quan, Xie Fan, Xinfei Liu, Yanming Wang, Hua |
| Author_xml | – sequence: 1 givenname: Yanming surname: Liu fullname: Liu, Yanming organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education, China), Faculty of Chemical, Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024 (China) – sequence: 2 givenname: Xie surname: Quan fullname: Quan, Xie email: quanxie@dlut.edu.cn organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education, China), Faculty of Chemical, Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024 (China) – sequence: 3 givenname: Xinfei surname: Fan fullname: Fan, Xinfei organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education, China), Faculty of Chemical, Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024 (China) – sequence: 4 givenname: Hua surname: Wang fullname: Wang, Hua organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education, China), Faculty of Chemical, Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024 (China) – sequence: 5 givenname: Shuo surname: Chen fullname: Chen, Shuo organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education, China), Faculty of Chemical, Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116024 (China) |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25892325$$D View this record in MEDLINE/PubMed |
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| Keywords | porous carbon hydrogen peroxide synthesis electrochemistry electrocatalysis oxygen reduction |
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| Snippet | H2O2 production by electroreduction of O2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical industries... H 2 O 2 production by electroreduction of O 2 is an attractive alternative to the current anthraquinone process, which is highly desirable for chemical... H sub(2)O sub(2) production by electroreduction of O sub(2) is an attractive alternative to the current anthraquinone process, which is highly desirable for... |
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| SubjectTerms | Carbon Current efficiency Defects electrocatalysis electrochemistry Electrodes Electrowinning Energy efficiency Environmental cleanup Hydrogen peroxide hydrogen peroxide synthesis Mass transfer Oxygen oxygen reduction porous carbon Reduction Selectivity Tuning |
| Title | High-Yield Electrosynthesis of Hydrogen Peroxide from Oxygen Reduction by Hierarchically Porous Carbon |
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