Copper Speciation for Natural Water by On-site Sample Treatment/Solid-phase Extraction/Inductively Coupled Plasma Mass Spectrometry
Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning step...
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| Published in | Analytical Sciences Vol. 34; no. 6; pp. 725 - 728 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Singapore
The Japan Society for Analytical Chemistry
2018
Springer Nature Singapore Nature Publishing Group |
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| Online Access | Get full text |
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| Abstract | Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO3 and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg−1, respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan. |
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| AbstractList | Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO
3
and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg
−1
, respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan. Keywords Copper, seawater, redox speciation, ICP-MS Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO3 and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg−1, respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan. Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg , respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan. Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO3 and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg-1, respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan.Herein, we determined the contents of Cu(I), Cu(II), and hydrophobic Cu in natural water using on-site sample treatment, solid-phase extraction (SPE), and inductively coupled plasma mass spectrometry (ICP-MS) analysis. To prevent Cu species changes in the sampling, filtering and preconditioning steps were performed in a closed system using plastic syringes and a disposable membrane filter. Bathocuproin disulfonate (BCS) and ethylenediaminetetraacetic acid (EDTA) were selected as a Cu(I)-selective complexing agent and a Cu(II) masking agent, respectively, whereas ascorbic acid (AA) was used to reduce Cu(II) to Cu(I). Pre-conditioned samples were passed through a hydrophobic SPE column, and the retained Cu species were eluted with ethanol. Subsequently, the eluate was concentrated, and the residue was re-dissolved in 2 M HNO3 and subjected to ICP-MS analysis. No artificial changes of Cu(I) and Cu(II) species were observed at any time, with the analytical detection limit of total Cu and the blank value equaling 0.0008 and 0.0025 μg kg-1, respectively. The developed method was applied to real estuarine, riverine, and seawater samples collected in Tokushima prefecture, Japan. |
| Author | YAMADA, Yohei KAMIMURA, Miki NOZOE, Kosuke TAKAYANAGI, Toshio YABUTANI, Tomoki KISHIBE, Shingo |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29887562$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.2116/analsci.33.807 10.1246/bcsj.73.895 10.1246/bcsj.74.31 10.2116/bunsekikagaku.47.109 10.1039/b308213j 10.2116/analsci.28.463 10.2116/bunsekikagaku.50.433 10.1016/0304-4203(82)90030-5 10.1016/j.ecss.2012.06.009 10.2116/analsci.33.487 10.1246/bcsj.20160404 10.2116/analsci.13.Supplement_393 10.2116/analsci.33.1231 10.1016/j.marchem.2009.07.004 10.1039/C7MT00023E 10.2116/bunsekikagaku.66.825 10.2116/analsci.33.1345 10.2116/bunsekikagaku.39.5_301 10.1246/bcsj.72.2253 10.1016/0016-7037(88)90008-7 10.1016/j.marpolbul.2013.08.027 |
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Chem.1982113431:CAS:528:DyaL38XlsFShtr8%3D10.1016/0304-4203(82)90030-5 YabutaniTJiSMouriFSawatariHItohAChibaKHaraguchiHBull. Chem. Soc. Jpn.199972116310.1246/bcsj.72.2253 LinY CChang-ChienG PChingP CChenW HLinY CMar. Pollut. Bull.2013762661:CAS:528:DC%2BC3sXhsVOntL3N10.1016/j.marpolbul.2013.08.02724054783 KatoTSugaharaSKajitaniTSengaYEgawaMKamiyaHSeikeYAnal Sci2017334871:CAS:528:DC%2BC2sXhtFKlsbvN10.2116/analsci.33.48728392526 H Higuchi (34060014_CR11) 2009; 11 J W Moffett (34060014_CR7) 1988; 52 H Kominami (34060014_CR9) 2017; 66 T Yabutani (34060014_CR15) 2000; 73 A Itoh (34060014_CR23) 1997; 13 H Iwai (34060014_CR3) 2017; 33 A Itoh (34060014_CR4) 2017; 90 Y Zheng (34060014_CR5) 2017; 33 T Yabutani (34060014_CR14) 2012; 28 H Tanaka (34060014_CR18) 2012; 111 H Haraguchi (34060014_CR1) 2017; 9 K Hirose (34060014_CR21) 1982; 11 K Isshiki (34060014_CR22) 1989; 21 H Yamada (34060014_CR20) 2001; 50 H Haraguchi (34060014_CR2) 2004; 19 T Kato (34060014_CR12) 2017; 33 T Yabutani (34060014_CR16) 2001; 74 A Itoh (34060014_CR19) 1998; 47 Y C Lin (34060014_CR17) 2013; 76 Y Kikuchi (34060014_CR10) 1990; 39 N Ozbek (34060014_CR13) 2017; 33 T Yabutani (34060014_CR8) 1999; 72 M González-Dávila (34060014_CR6) 2009; 115 |
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| SubjectTerms | Acetic acid Analytical Chemistry Ascorbic acid Chemical analysis Chemistry Conditioning Copper Emission spectroscopy Estuaries Estuarine environments Ethanol Ethylenediaminetetraacetic acids Hydrophobicity ICP-MS Inductively coupled plasma mass spectrometry Ions Masking Mass spectrometry Mass spectroscopy Preconditioning redox speciation Scientific imaging Seawater Solid phases Speciation Species Syringes Water analysis |
| Title | Copper Speciation for Natural Water by On-site Sample Treatment/Solid-phase Extraction/Inductively Coupled Plasma Mass Spectrometry |
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