Cascade anchoring strategy for general mass production of high-loading single-atomic metal-nitrogen catalysts
Although single-atomically dispersed metal-N x on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-N x is greatly challenging since the loading and single-atomic dispersion have to be balanced at...
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| Published in | Nature communications Vol. 10; no. 1; pp. 1278 - 11 |
|---|---|
| Main Authors | , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
20.03.2019
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Although single-atomically dispersed metal-N
x
on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-N
x
is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-N
x
. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O
2
reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO
2
reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-N
x
sites for diverse high-performance applications.
Although single atom catalysts (SACs) with high-loading metal-Nx have great potential in heterogeneous catalysis, their scalable synthesis remains challenging. Here, the authors develop a general cascade anchoring strategy for the mass production of a series of metal-Nx SACs with a metal loading up to 12.1 wt%. |
|---|---|
| AbstractList | Although single-atomically dispersed metal-N
x
on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-N
x
is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-N
x
. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O
2
reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO
2
reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-N
x
sites for diverse high-performance applications. Although single-atomically dispersed metal-Nx on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-Nx is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-Nx. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O2 reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO2 reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-Nx sites for diverse high-performance applications. Although single-atomically dispersed metal-N x on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-N x is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-N x . Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O 2 reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO 2 reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-N x sites for diverse high-performance applications. Although single atom catalysts (SACs) with high-loading metal-Nx have great potential in heterogeneous catalysis, their scalable synthesis remains challenging. Here, the authors develop a general cascade anchoring strategy for the mass production of a series of metal-Nx SACs with a metal loading up to 12.1 wt%. Although single atom catalysts (SACs) with high-loading metal-Nx have great potential in heterogeneous catalysis, their scalable synthesis remains challenging. Here, the authors develop a general cascade anchoring strategy for the mass production of a series of metal-Nx SACs with a metal loading up to 12.1 wt%. Although single-atomically dispersed metal-N on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-N is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-N . Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-N sites for diverse high-performance applications. Although single-atomically dispersed metal-Nx on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-Nx is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-Nx. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O2 reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO2 reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-Nx sites for diverse high-performance applications.Although single-atomically dispersed metal-Nx on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-Nx is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-Nx. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O2 reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO2 reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-Nx sites for diverse high-performance applications. Although single-atomically dispersed metal-Nx on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such single-atom catalysts (SACs) with high-loading metal-Nx is greatly challenging since the loading and single-atomic dispersion have to be balanced at high temperature for forming metal-Nx. Herein, we develop a general cascade anchoring strategy for the mass production of a series of M-NC SACs with a metal loading up to 12.1 wt%. Systematic investigation reveals that the chelation of metal ions, physical isolation of chelate complex upon high loading, and the binding with N-species at elevated temperature are essential to achieving high-loading M-NC SACs. As a demonstration, high-loading Fe-NC SAC shows superior electrocatalytic performance for O2 reduction and Ni-NC SAC exhibits high electrocatalytic activity for CO2 reduction. The strategy paves a universal way to produce stable M-NC SAC with high-density metal-Nx sites for diverse high-performance applications.Although single atom catalysts (SACs) with high-loading metal-Nx have great potential in heterogeneous catalysis, their scalable synthesis remains challenging. Here, the authors develop a general cascade anchoring strategy for the mass production of a series of metal-Nx SACs with a metal loading up to 12.1 wt%. |
| ArticleNumber | 1278 |
| Author | Huang, Lin-Bo Wu, Jinpeng He, Chao Zhang, Yun Zhao, Lu Hu, Jin-Song Gu, Lin Zhang, Qing-Hua Zhang, Lin-Juan Yang, Wanli Wan, Li-Jun Wu, Ze-Yuan Liu, Xiao-Zhi |
| Author_xml | – sequence: 1 givenname: Lu surname: Zhao fullname: Zhao, Lu organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 2 givenname: Yun surname: Zhang fullname: Zhang, Yun organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, College of Chemistry and Materials Science, Sichuan Normal University – sequence: 3 givenname: Lin-Bo surname: Huang fullname: Huang, Lin-Bo organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 4 givenname: Xiao-Zhi surname: Liu fullname: Liu, Xiao-Zhi organization: University of Chinese Academy of Sciences, Beijing National Research Center for Condensed Matter Physics, Collaborative Innovation Center of Quantum Matter, Institute of Physics, Chinese Academy of Sciences – sequence: 5 givenname: Qing-Hua surname: Zhang fullname: Zhang, Qing-Hua organization: Beijing National Research Center for Condensed Matter Physics, Collaborative Innovation Center of Quantum Matter, Institute of Physics, Chinese Academy of Sciences – sequence: 6 givenname: Chao surname: He fullname: He, Chao organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 7 givenname: Ze-Yuan surname: Wu fullname: Wu, Ze-Yuan organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 8 givenname: Lin-Juan surname: Zhang fullname: Zhang, Lin-Juan organization: Shanghai Synchrotron Radiation Facility, Shanghai Institute of Applied Physics, Chinese Academy of Sciences – sequence: 9 givenname: Jinpeng orcidid: 0000-0002-7082-4123 surname: Wu fullname: Wu, Jinpeng organization: Advanced Light Source, Lawrence Berkeley National Laboratory – sequence: 10 givenname: Wanli orcidid: 0000-0003-0666-8063 surname: Yang fullname: Yang, Wanli organization: Advanced Light Source, Lawrence Berkeley National Laboratory – sequence: 11 givenname: Lin orcidid: 0000-0002-7504-031X surname: Gu fullname: Gu, Lin organization: Beijing National Research Center for Condensed Matter Physics, Collaborative Innovation Center of Quantum Matter, Institute of Physics, Chinese Academy of Sciences – sequence: 12 givenname: Jin-Song surname: Hu fullname: Hu, Jin-Song email: hujs@iccas.ac.cn organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 13 givenname: Li-Jun surname: Wan fullname: Wan, Li-Jun organization: Beijing National Laboratory for Molecular Sciences (BNLMS), CAS Key Laboratory of Molecular Nanostructure and Nanotechnology, Institute of Chemistry, Chinese Academy of Sciences, University of Chinese Academy of Sciences |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30894539$$D View this record in MEDLINE/PubMed https://www.osti.gov/servlets/purl/1559195$$D View this record in Osti.gov |
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| Snippet | Although single-atomically dispersed metal-N
x
on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such... Although single-atomically dispersed metal-N on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such... Although single-atomically dispersed metal-Nx on carbon support (M-NC) has great potential in heterogeneous catalysis, the scalable synthesis of such... Although single atom catalysts (SACs) with high-loading metal-Nx have great potential in heterogeneous catalysis, their scalable synthesis remains challenging.... |
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| SubjectTerms | 140/133 140/146 147/135 147/137 147/143 639/301/299/161 639/301/299/886 639/638/77/884 Anchoring Atomic properties Carbon Carbon dioxide Catalysis Catalysts Catalytic oxidation Chelates Chelating agents Chelation Chemical synthesis Coordination compounds Dispersion Glucose High temperature Humanities and Social Sciences INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY Iron Laboratories Mass production Metal ions Metals multidisciplinary Nickel Nitrogen Physics Reduction Science Science (multidisciplinary) Single atom catalysts Strategy |
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| Title | Cascade anchoring strategy for general mass production of high-loading single-atomic metal-nitrogen catalysts |
| URI | https://link.springer.com/article/10.1038/s41467-019-09290-y https://www.ncbi.nlm.nih.gov/pubmed/30894539 https://www.proquest.com/docview/2194563920 https://www.proquest.com/docview/2195257653 https://www.osti.gov/servlets/purl/1559195 https://pubmed.ncbi.nlm.nih.gov/PMC6426845 https://doaj.org/article/ee6594d9ca654f159a3278748f9567d5 |
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