Efficacy of a solution-based approach for making sodalite waste forms for an oxide reduction salt utilized in the reprocessing of used uranium oxide fuel
This paper describes the various approaches evaluated for making solution-derived sodalite with a LiCl–Li2O oxide reduction salt selected to dissolve used uranium oxide fuel so the uranium can be recovered and recycled. The approaches include modified sol–gel and solution-based synthesis processes....
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| Published in | Journal of nuclear materials Vol. 459; no. C; pp. 313 - 322 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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United States
Elsevier B.V
01.04.2015
Elsevier |
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| Abstract | This paper describes the various approaches evaluated for making solution-derived sodalite with a LiCl–Li2O oxide reduction salt selected to dissolve used uranium oxide fuel so the uranium can be recovered and recycled. The approaches include modified sol–gel and solution-based synthesis processes. As-made products were mixed with 5 and 10mass% of a Na2O–B2O3–SiO2 glass binder and these, along with product without a binder, were heated using either a cold-press-and-sinter method or hot uniaxial pressing. The results demonstrate the limitation of sodalite yield due to the fast intermediate reactions between Na+ and Cl− to form halite in solution and Li2O and SiO2 to form lithium silicates (e.g., Li2SiO3 or Li2Si2O5) in the calcined and sintered pellets. The results show that pellets can be made with high sodalite fractions in the crystalline product (∼92mass%) and low porosities using a solution-based approach and this LiCl–Li2O salt but that the incorporation of Li into the sodalite is low. |
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| AbstractList | This paper describes the various approaches evaluated for making solution-derived sodalite with a LiCl–Li2O oxide reduction salt selected to dissolve used uranium oxide fuel so the uranium can be recovered and recycled. The approaches include modified sol–gel and solution-based synthesis processes. As-made products were mixed with 5 and 10mass% of a Na2O–B2O3–SiO2 glass binder and these, along with product without a binder, were heated using either a cold-press-and-sinter method or hot uniaxial pressing. The results demonstrate the limitation of sodalite yield due to the fast intermediate reactions between Na+ and Cl− to form halite in solution and Li2O and SiO2 to form lithium silicates (e.g., Li2SiO3 or Li2Si2O5) in the calcined and sintered pellets. The results show that pellets can be made with high sodalite fractions in the crystalline product (∼92mass%) and low porosities using a solution-based approach and this LiCl–Li2O salt but that the incorporation of Li into the sodalite is low. This paper describes the various approaches evaluated for making solution-derived sodalite with a LiClLi sub(2)O oxide reduction salt selected to dissolve used uranium oxide fuel so the uranium can be recovered and recycled. The approaches include modified sol-gel and solution-based synthesis processes. As-made products were mixed with 5 and 10 mass% of a Na sub(2)O-B sub(2)O sub(3)-SiO sub(2) glass binder and these, along with product without a binder, were heated using either a cold-press-and-sinter method or hot uniaxial pressing. The results demonstrate the limitation of sodalite yield due to the fast intermediate reactions between Na super(+) and Cl super(-) to form halite in solution and Li sub(2)O and SiO sub(2) to form lithium silicates (e.g., Li sub(2)SiO sub(3) or Li sub(2)Si sub(2)O sub(5)) in the calcined and sintered pellets. The results show that pellets can be made with high sodalite fractions in the crystalline product (~92 mass%) and low porosities using a solution-based approach and this LiCl-Li sub(2)O salt but that the incorporation of Li into the sodalite is low. This paper describes the various approaches attempted to make solution-derived sodalite with a LiCl-Li2O oxide reduction salt used to dissolve used uranium oxide fuel so the uranium can be recovered and recycled. The approaches include modified sol-gel and solutionbased synthesis processes. As-made products were mixed with 5 and 10 mass% of a Na2O-B2O3- SiO2 glass binder and these, along with product without a binder, were heated using either a cold-press-and-sinter method or hot uniaxial pressing. The results demonstrate the limitation of sodalite yield due to the fast intermediate reactions between Na+ and Cl- to form halite in solution and Li2O and SiO2 to form lithium silicates (e.g., Li2SiO3 or Li2Si2O5) in the calcined and sintered pellets. The results show that pellets can be made with high sodalite fractions in the crystalline product (~92 mass%) and low porosities using a solution-based approach and this LiCl-Li2O salt but that the incorporation of Li into the sodalite is low. |
| Author | Pierce, David A. Matyáš, Josef Frank, Steven M. Riley, Brian J. Burns, Carolyne A. |
| Author_xml | – sequence: 1 givenname: Brian J. surname: Riley fullname: Riley, Brian J. email: brian.riley@pnnl.gov organization: Pacific Northwest National Laboratory, Richland, WA 99352, United States – sequence: 2 givenname: David A. surname: Pierce fullname: Pierce, David A. organization: Pacific Northwest National Laboratory, Richland, WA 99352, United States – sequence: 3 givenname: Steven M. surname: Frank fullname: Frank, Steven M. organization: Idaho National Laboratory, Idaho Falls, ID 83402, United States – sequence: 4 givenname: Josef surname: Matyáš fullname: Matyáš, Josef organization: Pacific Northwest National Laboratory, Richland, WA 99352, United States – sequence: 5 givenname: Carolyne A. surname: Burns fullname: Burns, Carolyne A. organization: Pacific Northwest National Laboratory, Richland, WA 99352, United States |
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| Snippet | This paper describes the various approaches evaluated for making solution-derived sodalite with a LiCl–Li2O oxide reduction salt selected to dissolve used... This paper describes the various approaches evaluated for making solution-derived sodalite with a LiClLi sub(2)O oxide reduction salt selected to dissolve used... This paper describes the various approaches attempted to make solution-derived sodalite with a LiCl-Li2O oxide reduction salt used to dissolve used uranium... |
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| SubjectTerms | Binders electrochemical Lithium lithium chloride NUCLEAR FUEL CYCLE AND FUEL MATERIALS Nuclear fuels Oxides Pellets Reduction Sodalite Uranium oxides |
| Title | Efficacy of a solution-based approach for making sodalite waste forms for an oxide reduction salt utilized in the reprocessing of used uranium oxide fuel |
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