Examination of competitive lanthanide sorption onto smectites and its significance in the management of radioactive waste

The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (Kd; Kd,des), and desorption rates (Rdes) were determined from batch tests in two media: deionized water a...

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Published in	Journal of hazardous materials Vol. 186; no. 2-3; pp. 1930 - 1941
Main Authors	Galunin, Evgeny, Alba, María D., Santos, Maria J., Abrão, Taufik, Vidal, Miquel
Format	Journal Article
Language	English
Published	Kidlington Elsevier B.V 28.02.2011 Elsevier
Subjects	Adsorption Algorithms Aluminum Silicates Applied sciences calcium cement Cements Chemical engineering clay Concentració dels ions d'hidrogen Deionization Desorption Engineered barriers Exact sciences and technology Fittings Hydrogen-Ion Concentration ions Isotherms Lanthanides Lanthanoid Series Elements - analysis Lanthanoid Series Elements - chemistry Lanthanum - analysis leachates Lutetium - analysis Microscopy, Electron, Scanning Pollution Radioactive Waste Radioactive wastes radionuclides rare earth elements Residus radioactius Silicates - chemistry Silici Silicon Smectites Smectitic clays Sorption sorption isotherms Wastes Water - chemistry X-Ray Diffraction Sorption Radioactive waste Engineered barriers Lanthanides Smectitic clays Correlation Lanthanide Radioactive pollution Adsorption isotherm Hazardous waste Desorption Radioisotope Retention Langmuir isotherm Batchwise Correlation analysis Smectite Cement Affinity Leachate
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Abstract	The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (Kd; Kd,des), and desorption rates (Rdes) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02molL−1 Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high Kd for La and for Lu (5–63×104Lkg−1). Lower Kd was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between Kd and Kd,des (R2 around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers.
AbstractList	The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (Kd; Kd,dₑₛ), and desorption rates (Rdₑₛ) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02molL⁻¹ Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high Kd for La and for Lu (5–63×10⁴Lkg⁻¹). Lower Kd was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between Kd and Kd,dₑₛ (R² around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers. The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (K(d); K(d,des)), and desorption rates (R(des)) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02 mol L(-1) Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high K(d) for La and for Lu (5-63×10(4) L kg(-1)). Lower K(d) was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between K(d) and K(d,des) (R(2) around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers. The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (K d; K d,des), and desorption rates (R des) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02molLa degree 1 Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high K d for La and for Lu (5-63A-104 Lkga degree 1). Lower K d was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between K d and K d,des (R 2 around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers. The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (Kd; Kd,des), and desorption rates (Rdes) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02 mol L−1 Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high Kd for La and for Lu (5-63 × 104 L kg−1). Lower Kd was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between Kd and Kd,des (R2 around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers. The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (K(d); K(d,des)), and desorption rates (R(des)) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02 mol L(-1) Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high K(d) for La and for Lu (5-63×10(4) L kg(-1)). Lower K(d) was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between K(d) and K(d,des) (R(2) around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers.The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (K(d); K(d,des)), and desorption rates (R(des)) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02 mol L(-1) Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high K(d) for La and for Lu (5-63×10(4) L kg(-1)). Lower K(d) was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between K(d) and K(d,des) (R(2) around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers. The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and desorption distribution coefficients (Kd; Kd,des), and desorption rates (Rdes) were determined from batch tests in two media: deionized water and, to consider the influence of cement leachates, 0.02molL−1 Ca. The competitive effect was lower when high-affinity sites were available, as in the water medium at the lowest range of initial lanthanide concentration, with high Kd for La and for Lu (5–63×104Lkg−1). Lower Kd was measured at higher initial concentrations and in the Ca medium, where Lu showed a stronger competitive effect. This was confirmed by fitting the sorption data to a two-solute Langmuir isotherm. The desorption data indicated that sorption was virtually irreversible for the scenarios with high sorption, with an excellent correlation between Kd and Kd,des (R2 around 0.9 for the two lanthanides). Assuming that radioactive waste is a mixture of radionuclides, and that Ca ions will be provided by the cement leachates, this would reduce the retention capacity of clay engineered barriers.
Author	Galunin, Evgeny Vidal, Miquel Abrão, Taufik Alba, María D. Santos, Maria J.
Author_xml	– sequence: 1 givenname: Evgeny surname: Galunin fullname: Galunin, Evgeny organization: Departament de Química Analítica, Universitat de Barcelona, Martí i Franqués 1-11, 08028 Barcelona, Spain – sequence: 2 givenname: María D. surname: Alba fullname: Alba, María D. organization: Instituto de Ciencia de Materiales de Sevilla, Consejo Superior de Investigaciones Científicas – Universidad de Sevilla, Av. Américo Vespucio 49, 41092 Sevilla, Spain – sequence: 3 givenname: Maria J. surname: Santos fullname: Santos, Maria J. organization: Departamento de Química, Universidade Estadual de Londrina, Londrina, PR 86051-990, Brazil – sequence: 4 givenname: Taufik surname: Abrão fullname: Abrão, Taufik organization: Instituto de Ciencia de Materiales de Sevilla, Consejo Superior de Investigaciones Científicas – Universidad de Sevilla, Av. Américo Vespucio 49, 41092 Sevilla, Spain – sequence: 5 givenname: Miquel surname: Vidal fullname: Vidal, Miquel email: miquel.vidal@ub.edu organization: Departament de Química Analítica, Universitat de Barcelona, Martí i Franqués 1-11, 08028 Barcelona, Spain
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Keywords	Sorption Radioactive waste Engineered barriers Lanthanides Smectitic clays Correlation Lanthanide Radioactive pollution Adsorption isotherm Hazardous waste Desorption Radioisotope Retention Langmuir isotherm Batchwise Correlation analysis Smectite Cement Affinity Leachate
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Snippet	The competitive effect of La and Lu (analogues of radionuclides appearing in radioactive waste) in the sorption in four smectites was examined. Sorption and...
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SubjectTerms	Adsorption Algorithms Aluminum Silicates Applied sciences calcium cement Cements Chemical engineering clay Concentració dels ions d'hidrogen Deionization Desorption Engineered barriers Exact sciences and technology Fittings Hydrogen-Ion Concentration ions Isotherms Lanthanides Lanthanoid Series Elements - analysis Lanthanoid Series Elements - chemistry Lanthanum - analysis leachates Lutetium - analysis Microscopy, Electron, Scanning Pollution Radioactive Waste Radioactive wastes radionuclides rare earth elements Residus radioactius Silicates - chemistry Silici Silicon Smectites Smectitic clays Sorption sorption isotherms Wastes Water - chemistry X-Ray Diffraction
Title	Examination of competitive lanthanide sorption onto smectites and its significance in the management of radioactive waste
URI	https://dx.doi.org/10.1016/j.jhazmat.2010.12.098 https://www.ncbi.nlm.nih.gov/pubmed/21255915 https://www.proquest.com/docview/1694494381 https://www.proquest.com/docview/1770349961 https://www.proquest.com/docview/851747185 https://www.proquest.com/docview/867747670 https://recercat.cat/handle/2072/349175
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