Effect of Central Metal Ions of Analogous Metal-Organic Frameworks on Adsorption of Organoarsenic Compounds from Water: Plausible Mechanism of Adsorption and Water Purification

The adsorptive removal of organoarsenic compounds such as p‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL‐100‐Fe) exhibits a much higher adsorption capacity for AS...

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Published inChemistry : a European journal Vol. 21; no. 1; pp. 347 - 354
Main Authors Jun, Jong Won, Tong, Minman, Jung, Beom K., Hasan, Zubair, Zhong, Chongli, Jhung, Sung Hwa
Format Journal Article
LanguageEnglish
Published Weinheim WILEY-VCH Verlag 02.01.2015
WILEY‐VCH Verlag
Wiley Subscription Services, Inc
Subjects
Activated carbon
Activation
Adsorption
Arsanilic Acid - chemistry
arsenic
Chemistry
Coordination Complexes - chemistry
Desorption
Hydrogen-Ion Concentration
Ions - chemistry
iron
Iron - chemistry
Mathematical analysis
Metal-organic frameworks
Metalorganic compounds
Organometallic Compounds - chemistry
Roxarsone - chemistry
Spectroscopy, Fourier Transform Infrared
Surface chemistry
Water Pollutants, Chemical - chemistry
Water Purification
water purification
iron
adsorption
arsenic
metal-organic frameworks
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Abstract The adsorptive removal of organoarsenic compounds such as p‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL‐100‐Fe) exhibits a much higher adsorption capacity for ASA and ROX than activated carbon, zeolite (HY), goethite, and other MOFs. The adsorption of ASA and ROX over MIL‐100‐Fe is also much more rapid than that over activated carbon. Moreover, the used MIL‐100‐Fe can be recycled by simply washing with acidic ethanol. Therefore, it is determined that a MOF such as MIL‐100‐Fe can be used to remove organoarsenic compounds from contaminated water because of its high adsorption capacity, rapid adsorption, and ready regeneration. Moreover, only one of three analogous MIL‐100 species (MIL‐100‐Fe, rather than MIL‐100‐Al or MIL‐100‐Cr) can effectively remove the organoarsenic compounds. This selective and high adsorption over MIL‐100‐Fe, different from other analogous MIL‐100 species, can be explained (through calculations) by the facile desorption of water from MIL‐100‐Fe as well as the large (absolute value) replacement energy (difference between the adsorption energies of the organoarsenic compounds and water) exhibited by MIL‐100‐Fe. A plausible adsorption/desorption mechanism is proposed based on the surface charge of the MOFs, FTIR results, calculations, and the reactivation results with respect to the solvents used in the experiments. As seen in MOFs: Among three analogous metal–organic frameworks (MOFs; MIL‐100‐Al, MIL‐100‐Cr, and MIL‐100‐Fe), only MIL‐100‐Fe is found to be very effective in the adsorption of organic arsenic compounds from water. This preferential adsorption and the adsorption mechanism can be explained with detailed investigation and calculations on the metal ion sites within the MOFs.
AbstractList The adsorptive removal of organoarsenic compounds such as p-arsanilic acid (ASA) and roxarsone (ROX) from water using metal-organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL-100-Fe) exhibits a much higher adsorption capacity for ASA and ROX than activated carbon, zeolite (HY), goethite, and other MOFs. The adsorption of ASA and ROX over MIL-100-Fe is also much more rapid than that over activated carbon. Moreover, the used MIL-100-Fe can be recycled by simply washing with acidic ethanol. Therefore, it is determined that a MOF such as MIL-100-Fe can be used to remove organoarsenic compounds from contaminated water because of its high adsorption capacity, rapid adsorption, and ready regeneration. Moreover, only one of three analogous MIL-100 species (MIL-100-Fe, rather than MIL-100-Al or MIL-100-Cr) can effectively remove the organoarsenic compounds. This selective and high adsorption over MIL-100-Fe, different from other analogous MIL-100 species, can be explained (through calculations) by the facile desorption of water from MIL-100-Fe as well as the large (absolute value) replacement energy (difference between the adsorption energies of the organoarsenic compounds and water) exhibited by MIL-100-Fe. A plausible adsorption/desorption mechanism is proposed based on the surface charge of the MOFs, FTIR results, calculations, and the reactivation results with respect to the solvents used in the experiments.
The adsorptive removal of organoarsenic compounds such as p-arsanilic acid (ASA) and roxarsone (ROX) from water using metal-organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL-100-Fe) exhibits a much higher adsorption capacity for ASA and ROX than activated carbon, zeolite (HY), goethite, and other MOFs. The adsorption of ASA and ROX over MIL-100-Fe is also much more rapid than that over activated carbon. Moreover, the used MIL-100-Fe can be recycled by simply washing with acidic ethanol. Therefore, it is determined that a MOF such as MIL-100-Fe can be used to remove organoarsenic compounds from contaminated water because of its high adsorption capacity, rapid adsorption, and ready regeneration. Moreover, only one of three analogous MIL-100 species (MIL-100-Fe, rather than MIL-100-Al or MIL-100-Cr) can effectively remove the organoarsenic compounds. This selective and high adsorption over MIL-100-Fe, different from other analogous MIL-100 species, can be explained (through calculations) by the facile desorption of water from MIL-100-Fe as well as the large (absolute value) replacement energy (difference between the adsorption energies of the organoarsenic compounds and water) exhibited by MIL-100-Fe. A plausible adsorption/desorption mechanism is proposed based on the surface charge of the MOFs, FTIR results, calculations, and the reactivation results with respect to the solvents used in the experiments. As seen in MOFs: Among three analogous metal-organic frameworks (MOFs; MIL-100-Al, MIL-100-Cr, and MIL-100-Fe), only MIL-100-Fe is found to be very effective in the adsorption of organic arsenic compounds from water. This preferential adsorption and the adsorption mechanism can be explained with detailed investigation and calculations on the metal ion sites within the MOFs.
The adsorptive removal of organoarsenic compounds such as p‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL‐100‐Fe) exhibits a much higher adsorption capacity for ASA and ROX than activated carbon, zeolite (HY), goethite, and other MOFs. The adsorption of ASA and ROX over MIL‐100‐Fe is also much more rapid than that over activated carbon. Moreover, the used MIL‐100‐Fe can be recycled by simply washing with acidic ethanol. Therefore, it is determined that a MOF such as MIL‐100‐Fe can be used to remove organoarsenic compounds from contaminated water because of its high adsorption capacity, rapid adsorption, and ready regeneration. Moreover, only one of three analogous MIL‐100 species (MIL‐100‐Fe, rather than MIL‐100‐Al or MIL‐100‐Cr) can effectively remove the organoarsenic compounds. This selective and high adsorption over MIL‐100‐Fe, different from other analogous MIL‐100 species, can be explained (through calculations) by the facile desorption of water from MIL‐100‐Fe as well as the large (absolute value) replacement energy (difference between the adsorption energies of the organoarsenic compounds and water) exhibited by MIL‐100‐Fe. A plausible adsorption/desorption mechanism is proposed based on the surface charge of the MOFs, FTIR results, calculations, and the reactivation results with respect to the solvents used in the experiments. As seen in MOFs: Among three analogous metal–organic frameworks (MOFs; MIL‐100‐Al, MIL‐100‐Cr, and MIL‐100‐Fe), only MIL‐100‐Fe is found to be very effective in the adsorption of organic arsenic compounds from water. This preferential adsorption and the adsorption mechanism can be explained with detailed investigation and calculations on the metal ion sites within the MOFs.
Abstract The adsorptive removal of organoarsenic compounds such as p ‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs) has been investigated for the first time. A MOF, iron benzenetricarboxylate (also called MIL‐100‐Fe) exhibits a much higher adsorption capacity for ASA and ROX than activated carbon, zeolite (HY), goethite, and other MOFs. The adsorption of ASA and ROX over MIL‐100‐Fe is also much more rapid than that over activated carbon. Moreover, the used MIL‐100‐Fe can be recycled by simply washing with acidic ethanol. Therefore, it is determined that a MOF such as MIL‐100‐Fe can be used to remove organoarsenic compounds from contaminated water because of its high adsorption capacity, rapid adsorption, and ready regeneration. Moreover, only one of three analogous MIL‐100 species (MIL‐100‐Fe, rather than MIL‐100‐Al or MIL‐100‐Cr) can effectively remove the organoarsenic compounds. This selective and high adsorption over MIL‐100‐Fe, different from other analogous MIL‐100 species, can be explained (through calculations) by the facile desorption of water from MIL‐100‐Fe as well as the large (absolute value) replacement energy (difference between the adsorption energies of the organoarsenic compounds and water) exhibited by MIL‐100‐Fe. A plausible adsorption/desorption mechanism is proposed based on the surface charge of the MOFs, FTIR results, calculations, and the reactivation results with respect to the solvents used in the experiments.
Author Jhung, Sung Hwa
Hasan, Zubair
Jun, Jong Won
Tong, Minman
Jung, Beom K.
Zhong, Chongli
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  surname: Jun
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  organization: Department of Chemistry and Green-Nano Materials Research Centre, Kyungpook National University, Daegu 702-701 (Republic of Korea), Fax: (+82) 53-950-6330
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  surname: Tong
  fullname: Tong, Minman
  organization: State Key Laboratory of Organic-Inorganic Composites, Beijing University of Chemical Technology, Beijing, 100029 (P. R. China), Fax: (+86) 10-64419862
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  givenname: Beom K.
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  fullname: Jung, Beom K.
  organization: Department of Chemistry and Green-Nano Materials Research Centre, Kyungpook National University, Daegu 702-701 (Republic of Korea), Fax: (+82) 53-950-6330
– sequence: 4
  givenname: Zubair
  surname: Hasan
  fullname: Hasan, Zubair
  organization: Department of Chemistry and Green-Nano Materials Research Centre, Kyungpook National University, Daegu 702-701 (Republic of Korea), Fax: (+82) 53-950-6330
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  givenname: Chongli
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  email: zhongcl@mail.buct.edu.cn
  organization: State Key Laboratory of Organic-Inorganic Composites, Beijing University of Chemical Technology, Beijing, 100029 (P. R. China), Fax: (+86) 10-64419862
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  givenname: Sung Hwa
  surname: Jhung
  fullname: Jhung, Sung Hwa
  email: sung@knu.ac.kr
  organization: Department of Chemistry and Green-Nano Materials Research Centre, Kyungpook National University, Daegu 702-701 (Republic of Korea), Fax: (+82) 53-950-6330
BackLink https://www.ncbi.nlm.nih.gov/pubmed/25298118$$D View this record in MEDLINE/PubMed
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2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
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Issue 1
Keywords water purification
iron
adsorption
arsenic
metal-organic frameworks
Language English
License 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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National Research Foundation of Korea - No. 2013R1A2A2A01007176
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2011; 358
2010; 12
2010; 16
2009; 43
2013; 1
2007; 149
2008; 37
2009; 113
2011; 13
2008 2008; 47 120
2012; 14
2012; 209
2010; 26
2012; 377
2012 2012; 51 124
2009; 90
2013; 52
2013; 117
2013; 113
2013; 234
2008; 24
2005; 309
2009; 19
2012; 24
2005; 39
2012; 22
2014; 246
2014; 11
2014; 118
2007; 19
2004 2004; 43 116
2009; 21
2012
2013; 42
2007
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2009; 131
2013; 260
2014; 43
2008; 160
2012; 152
2012; 112
2012; 157
2006; 40
2010; 46
2002; 124
2010; 134
2013; 244–245
2013; 135
2011 2011; 50 123
2008; 42
2011; 47
2007; 41
2011; 185
2014; 224
2014; 420
2012; 85
2011; 186
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Snippet The adsorptive removal of organoarsenic compounds such as p‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs) has been...
The adsorptive removal of organoarsenic compounds such as p-arsanilic acid (ASA) and roxarsone (ROX) from water using metal-organic frameworks (MOFs) has been...
Abstract The adsorptive removal of organoarsenic compounds such as p ‐arsanilic acid (ASA) and roxarsone (ROX) from water using metal–organic frameworks (MOFs)...
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SubjectTerms Activated carbon
Activation
Adsorption
Arsanilic Acid - chemistry
arsenic
Chemistry
Coordination Complexes - chemistry
Desorption
Hydrogen-Ion Concentration
Ions - chemistry
iron
Iron - chemistry
Mathematical analysis
Metal-organic frameworks
Metalorganic compounds
Organometallic Compounds - chemistry
Roxarsone - chemistry
Spectroscopy, Fourier Transform Infrared
Surface chemistry
Water Pollutants, Chemical - chemistry
Water Purification
Title Effect of Central Metal Ions of Analogous Metal-Organic Frameworks on Adsorption of Organoarsenic Compounds from Water: Plausible Mechanism of Adsorption and Water Purification
URI https://api.istex.fr/ark:/67375/WNG-DM01591G-6/fulltext.pdf
https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fchem.201404658
https://www.ncbi.nlm.nih.gov/pubmed/25298118
https://www.proquest.com/docview/1638883077
https://search.proquest.com/docview/1639979874
https://search.proquest.com/docview/1786193359
Volume 21
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