One‐step strategy for the synthesis of a derivatized cyclodextrin‐based monolithic column
Derivatized β‐cyclodextrin (β‐CD) functionalized monolithic columns were prepared by a “one‐step” strategy using click chemistry. First, the intended derivatized β‐CD monomers were synthesized by a click reaction between propargyl methacrylate and mono‐6‐azido‐β‐CD and then sulfonation or methylatio...
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| Published in | Journal of separation science Vol. 37; no. 14; pp. 1720 - 1727 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article Web Resource |
| Language | English |
| Published |
Weinheim
Wiley-VCH
01.07.2014
Blackwell Publishing Ltd Wiley Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1615-9306 1615-9314 1615-9314 |
| DOI | 10.1002/jssc.201400312 |
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| Abstract | Derivatized β‐cyclodextrin (β‐CD) functionalized monolithic columns were prepared by a “one‐step” strategy using click chemistry. First, the intended derivatized β‐CD monomers were synthesized by a click reaction between propargyl methacrylate and mono‐6‐azido‐β‐CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one‐step in situ copolymerization of the derivatized β‐CD monomer and ethylene glycol dimethacrylate. The sulfated β‐CD‐based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated β‐CD‐functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed‐phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD‐functionalized methacrylate monoliths. |
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| AbstractList | Derivatized [beta]-cyclodextrin ([beta]-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended derivatized [beta]-CD monomers were synthesized by a click reaction between propargyl methacrylate and mono-6-azido-[beta]-CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one-step in situ copolymerization of the derivatized [beta]-CD monomer and ethylene glycol dimethacrylate. The sulfated [beta]-CD-based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated [beta]-CD-functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed-phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD-functionalized methacrylate monoliths. Derivatized β‐cyclodextrin (β‐CD) functionalized monolithic columns were prepared by a “one‐step” strategy using click chemistry. First, the intended derivatized β‐CD monomers were synthesized by a click reaction between propargyl methacrylate and mono‐6‐azido‐β‐CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one‐step in situ copolymerization of the derivatized β‐CD monomer and ethylene glycol dimethacrylate. The sulfated β‐CD‐based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated β‐CD‐functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed‐phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD‐functionalized methacrylate monoliths. Derivatized β-cyclodextrin (β-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended derivatized β-CD monomers were synthesized by a click reaction between propargyl methacrylate and mono-6-azido-β-CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one-step in situ copolymerization of the derivatized β-CD monomer and ethylene glycol dimethacrylate. The sulfated β-CD-based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated β-CD-functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed-phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD-functionalized methacrylate monoliths.Derivatized β-cyclodextrin (β-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended derivatized β-CD monomers were synthesized by a click reaction between propargyl methacrylate and mono-6-azido-β-CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one-step in situ copolymerization of the derivatized β-CD monomer and ethylene glycol dimethacrylate. The sulfated β-CD-based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated β-CD-functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed-phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD-functionalized methacrylate monoliths. Derivatized [beta]-cyclodextrin ([beta]-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended derivatized [beta]-CD monomers were synthesized by a click reaction between propargyl methacrylate and mono-6-azido-[beta]-CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one-step in situ copolymerization of the derivatized [beta]-CD monomer and ethylene glycol dimethacrylate. The sulfated [beta]-CD-based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated [beta]-CD-functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed-phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD-functionalized methacrylate monoliths. [PUBLICATION ABSTRACT] Derivatized β‐cyclodextrin (β‐CD) functionalized monolithic columns were prepared by a “one‐step” strategy using click chemistry. First, the intended derivatized β‐CD monomers were synthesized by a click reaction between propargyl methacrylate and mono‐6‐azido‐β‐CD and then sulfonation or methylation was carried out. Finally, monolithic columns were prepared through a one‐step in situ copolymerization of the derivatized β‐CD monomer and ethylene glycol dimethacrylate. The sulfated β‐CD‐based monolith was successfully applied to the hydrophilic interaction liquid chromatography separation of nucleosides and small peptides, while the methylated β‐CD‐functionalized monolith was useful for the separation of nonpolar compounds and drug enantiomers in capillary reversed‐phase liquid chromatography. The structures of the monomers were characterized by Fourier transform infrared spectroscopy and mass spectrometry. The physicochemical properties and column performance of monoliths were evaluated by scanning electron microscopy and micro high performance liquid chromatography. This strategy has considerable prospects for the preparation of other derivatized CD‐functionalized methacrylate monoliths. |
| Author | Zhang, Qiaoxuan Zhao, Xianglong Jiang, Zhengjin Yao, Zhe Crommen, Jacques Ran, Danni Guo, Jialiang |
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| Cites_doi | 10.1002/marc.200800584 10.1002/jssc.200700631 10.1002/jssc.201300231 10.1016/j.chroma.2012.01.065 10.1016/S0021-9673(02)00840-3 10.1016/j.ijpharm.2012.04.069 10.1002/jssc.201300374 10.1016/j.jbbm.2006.08.009 10.2116/analsci.14.1021 10.2116/analsci.26.943 10.1016/S0008-6215(03)00359-8 10.1007/s00216-003-2181-x 10.1016/j.ijhydene.2009.06.027 10.1002/1522-2683(20000901)21:15<3135::AID-ELPS3135>3.0.CO;2-7 10.1002/elps.201000647 10.1021/ac200414r 10.1002/macp.201100526 10.1016/j.chroma.2008.12.014 10.1016/j.jchromb.2010.07.020 10.1016/j.chroma.2004.01.053 10.1002/elps.200500906 10.1002/jssc.201100282 10.1016/j.talanta.2010.03.016 10.1021/ac951199e |
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| Keywords | Capillary column Performance evaluation Purine derivatives Fourier transformation Separation Chromatographic retention HPLC chromatography Mass copolymerization Derivatization Retention time Characterization Crosslinked copolymer Functionalization Enantiomer Nucleoside Derivatized β-cyclodextrin Click chemistry Stationary phase Alkanophenone Hydrophilic Interaction Liquid chromatography Oligosaccharide Monolithic column Chiral stationary phase Acebutolol Ketone Monolithic columns Infrared spectrometry Reversed phase chromatography Cyclodextrin Ultraviolet detector Optical resolution Preparation Pyrimidine derivatives Methacrylate copolymer Inclusion compound Radical copolymerization Mass spectrometry Apolar compound Beta blocking agent |
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| References | Ng, S. C., Ong, T. T., Fu, P., Ching, C. B., J. Chromatogr. A 2002, 968, 31-40. Guerrouache, M., Millot, M. C., Carbonnier, B., Macromol. Rapid Commun. 2009, 30, 109-113. Koide, T., Ueno, K., Anal. Sci. 1998, 14, 1021-1023. Selvam, S., Rajiv Gandhi, R., Suresh, J., Gowri, S., Ravikumar, S., Sundrarajan, M., Int. J. Pharm. 2012, 434, 366-374. Tian, Y., Zhong, C., Fu, E., Zeng, Z., J. Chromatogr. A 2009, 1216, 1000-1007. Lubda, D., Cabrera, K., Nakanishi, K., Lindner, W., Anal. Bioanal. Chem. 2003, 377, 892-901. Salwiński, A., Roy, V., Agrofoglio, L. A., Delépée, R., Macromol. Chem. Phys. 2011, 212, 2700-2707. Zhang, M. Q., El Rassi, Z., Electrophoresis 2000, 21, 3135-3140. Sun, X. L., Lin, D., He, X. W., Chen, L. X., Zhang, Y. K., Talanta 2010, 82, 404-408. Chen, M. L., Li, L. M., Yuan, B. F., Ma, Q., Feng, Y. Q., J. Chromatogr. A 2012, 1230, 54-60. Ng, S.C., Ong, T.T., Fu, P., Ching, C.B., J. Chromatogr. A 2002, 968, 31-40. Marechal A., El-Debs R., Dugas V., Demesmay C., J. Sep. Sci. 2013, 36, 2049-2062. Hsieh, M.L., Li, G.Y., Chau, L.K., Hon, Y.S., J. Sep. Sci. 2008, 31, 1819-1827. Lecourt, T., Mallet, J.M., Sinaÿ, P., Carbohydr. Chem. 2003, 338, 2417-2419. Jiang, Z. J., Smith, N. W., Ferguson, P. D., Taylor, M. R., J. Biochem. Biophys. Methods 2007, 70, 39-45. Guo, J., Zhang, Q., Peng, Y., Liu, Z., Rao, L., He, T., Crommen, J., Sun, P., Jiang, Z., J. Sep. Sci. 2013, 36, 2441-2449. Lin, B., Shi, Z.G., Zhang, H.J., Ng, S.C., Feng, Y.Q., Electrophoresis 2006, 27, 3057-3065. Stalcup, A. M., Gahm, K. H., Anal. Chem. 1996, 68, 1369-1374. Yuan, R., Wang, Y., Ding, G., Anal. Sci. 2010, 26, 943-947. Gu, C. Y., Shamsi, S. A., Electrophoresis 2011, 32, 2727-2737. Zhang, Z. B., Wu, M. H., Wu, R. A., Dong, J., Ou, J. J., Zou, H. F., Anal. Chem. 2011, 83, 3616-3622. Yang, T., Int. J. Hydrogen Energy 2009, 34, 6917-6924. Lv, Y. Q., Hughes, T. C., Hao, X., Mei, D., Tan, T., J. Sep. Sci. 2011, 34, 2131-2137. Lv, Y. Q., Mei, D. P., Pan, X. X., Tan, T. W., J. Chromatogr. B 2010, 878, 2461-2464. Freitag, R., J. Chromatogr. A 2004, 1033, 267-273. 2009; 34 2009; 1216 2011; 212 2009; 30 2010; 26 2003; 338 2013; 36 2012; 1230 2010; 878 2000; 21 2006; 27 2011; 83 2011; 32 2007; 70 2002; 968 2011; 34 2004; 1033 2008; 31 1996; 68 2012; 434 2003; 377 1998; 14 2010; 82 e_1_2_8_24_1 e_1_2_8_25_1 e_1_2_8_26_1 e_1_2_8_3_1 e_1_2_8_2_1 e_1_2_8_5_1 e_1_2_8_4_1 e_1_2_8_7_1 e_1_2_8_6_1 e_1_2_8_9_1 e_1_2_8_8_1 e_1_2_8_20_1 e_1_2_8_21_1 e_1_2_8_22_1 e_1_2_8_23_1 e_1_2_8_17_1 e_1_2_8_18_1 e_1_2_8_19_1 e_1_2_8_13_1 e_1_2_8_14_1 e_1_2_8_15_1 e_1_2_8_16_1 e_1_2_8_10_1 e_1_2_8_11_1 e_1_2_8_12_1 |
| References_xml | – reference: Gu, C. Y., Shamsi, S. A., Electrophoresis 2011, 32, 2727-2737. – reference: Ng, S.C., Ong, T.T., Fu, P., Ching, C.B., J. Chromatogr. A 2002, 968, 31-40. – reference: Marechal A., El-Debs R., Dugas V., Demesmay C., J. Sep. Sci. 2013, 36, 2049-2062. – reference: Guerrouache, M., Millot, M. C., Carbonnier, B., Macromol. Rapid Commun. 2009, 30, 109-113. – reference: Yuan, R., Wang, Y., Ding, G., Anal. Sci. 2010, 26, 943-947. – reference: Lin, B., Shi, Z.G., Zhang, H.J., Ng, S.C., Feng, Y.Q., Electrophoresis 2006, 27, 3057-3065. – reference: Stalcup, A. M., Gahm, K. H., Anal. Chem. 1996, 68, 1369-1374. – reference: Guo, J., Zhang, Q., Peng, Y., Liu, Z., Rao, L., He, T., Crommen, J., Sun, P., Jiang, Z., J. Sep. Sci. 2013, 36, 2441-2449. – reference: Tian, Y., Zhong, C., Fu, E., Zeng, Z., J. Chromatogr. A 2009, 1216, 1000-1007. – reference: Ng, S. C., Ong, T. T., Fu, P., Ching, C. B., J. Chromatogr. A 2002, 968, 31-40. – reference: Koide, T., Ueno, K., Anal. Sci. 1998, 14, 1021-1023. – reference: Lv, Y. Q., Mei, D. P., Pan, X. X., Tan, T. W., J. Chromatogr. B 2010, 878, 2461-2464. – reference: Yang, T., Int. J. Hydrogen Energy 2009, 34, 6917-6924. – reference: Sun, X. L., Lin, D., He, X. W., Chen, L. X., Zhang, Y. K., Talanta 2010, 82, 404-408. – reference: Lubda, D., Cabrera, K., Nakanishi, K., Lindner, W., Anal. Bioanal. Chem. 2003, 377, 892-901. – reference: Salwiński, A., Roy, V., Agrofoglio, L. A., Delépée, R., Macromol. Chem. Phys. 2011, 212, 2700-2707. – reference: Lecourt, T., Mallet, J.M., Sinaÿ, P., Carbohydr. Chem. 2003, 338, 2417-2419. – reference: Selvam, S., Rajiv Gandhi, R., Suresh, J., Gowri, S., Ravikumar, S., Sundrarajan, M., Int. J. Pharm. 2012, 434, 366-374. – reference: Chen, M. L., Li, L. M., Yuan, B. F., Ma, Q., Feng, Y. Q., J. Chromatogr. A 2012, 1230, 54-60. – reference: Lv, Y. Q., Hughes, T. C., Hao, X., Mei, D., Tan, T., J. Sep. Sci. 2011, 34, 2131-2137. – reference: Hsieh, M.L., Li, G.Y., Chau, L.K., Hon, Y.S., J. Sep. Sci. 2008, 31, 1819-1827. – reference: Freitag, R., J. Chromatogr. A 2004, 1033, 267-273. – reference: Zhang, M. Q., El Rassi, Z., Electrophoresis 2000, 21, 3135-3140. – reference: Zhang, Z. B., Wu, M. H., Wu, R. A., Dong, J., Ou, J. J., Zou, H. F., Anal. Chem. 2011, 83, 3616-3622. – reference: Jiang, Z. J., Smith, N. W., Ferguson, P. D., Taylor, M. R., J. Biochem. Biophys. Methods 2007, 70, 39-45. – volume: 1216 start-page: 1000 year: 2009 end-page: 1007 publication-title: J. Chromatogr. A – volume: 70 start-page: 39 year: 2007 end-page: 45 publication-title: J. Biochem. Biophys. Methods – volume: 1033 start-page: 267 year: 2004 end-page: 273 publication-title: J. Chromatogr. A – volume: 36 start-page: 2441 year: 2013 end-page: 2449 publication-title: J. Sep. Sci. – volume: 32 start-page: 2727 year: 2011 end-page: 2737 publication-title: Electrophoresis – volume: 434 start-page: 366 year: 2012 end-page: 374 publication-title: Int. J. Pharm. – volume: 212 start-page: 2700 year: 2011 end-page: 2707 publication-title: Macromol. Chem. Phys. – volume: 83 start-page: 3616 year: 2011 end-page: 3622 publication-title: Anal. Chem. – volume: 878 start-page: 2461 year: 2010 end-page: 2464 publication-title: J. Chromatogr. B – volume: 1230 start-page: 54 year: 2012 end-page: 60 publication-title: J. Chromatogr. A – volume: 14 start-page: 1021 year: 1998 end-page: 1023 publication-title: Anal. Sci. – volume: 30 start-page: 109 year: 2009 end-page: 113 publication-title: Macromol. Rapid Commun. – volume: 36 start-page: 2049 year: 2013 end-page: 2062 publication-title: J. Sep. Sci. – volume: 26 start-page: 943 year: 2010 end-page: 947 publication-title: Anal. Sci. – volume: 21 start-page: 3135 year: 2000 end-page: 3140 publication-title: Electrophoresis – volume: 968 start-page: 31 year: 2002 end-page: 40 publication-title: J. Chromatogr. A – volume: 34 start-page: 2131 year: 2011 end-page: 2137 publication-title: J. Sep. Sci. – volume: 377 start-page: 892 year: 2003 end-page: 901 publication-title: Anal. Bioanal. Chem. – volume: 82 start-page: 404 year: 2010 end-page: 408 publication-title: Talanta – volume: 27 start-page: 3057 year: 2006 end-page: 3065 publication-title: Electrophoresis – volume: 338 start-page: 2417 year: 2003 end-page: 2419 publication-title: Carbohydr. Chem. – volume: 34 start-page: 6917 year: 2009 end-page: 6924 publication-title: Int. J. Hydrogen Energy – volume: 31 start-page: 1819 year: 2008 end-page: 1827 publication-title: J. Sep. Sci. – volume: 68 start-page: 1369 year: 1996 end-page: 1374 publication-title: Anal. Chem. – ident: e_1_2_8_7_1 doi: 10.1002/marc.200800584 – ident: e_1_2_8_3_1 doi: 10.1002/jssc.200700631 – ident: e_1_2_8_22_1 doi: 10.1002/jssc.201300231 – ident: e_1_2_8_26_1 doi: 10.1016/j.chroma.2012.01.065 – ident: e_1_2_8_15_1 doi: 10.1016/S0021-9673(02)00840-3 – ident: e_1_2_8_23_1 doi: 10.1016/j.ijpharm.2012.04.069 – ident: e_1_2_8_21_1 doi: 10.1002/jssc.201300374 – ident: e_1_2_8_25_1 doi: 10.1016/j.jbbm.2006.08.009 – ident: e_1_2_8_4_1 doi: 10.2116/analsci.14.1021 – ident: e_1_2_8_17_1 doi: 10.2116/analsci.26.943 – ident: e_1_2_8_18_1 doi: 10.1016/S0008-6215(03)00359-8 – ident: e_1_2_8_5_1 doi: 10.1007/s00216-003-2181-x – ident: e_1_2_8_24_1 doi: 10.1016/j.ijhydene.2009.06.027 – ident: e_1_2_8_13_1 doi: 10.1002/1522-2683(20000901)21:15<3135::AID-ELPS3135>3.0.CO;2-7 – ident: e_1_2_8_19_1 doi: 10.1002/elps.201000647 – ident: e_1_2_8_20_1 doi: 10.1021/ac200414r – ident: e_1_2_8_9_1 doi: 10.1002/macp.201100526 – ident: e_1_2_8_10_1 doi: 10.1016/j.chroma.2008.12.014 – ident: e_1_2_8_11_1 doi: 10.1016/j.jchromb.2010.07.020 – ident: e_1_2_8_2_1 doi: 10.1016/j.chroma.2004.01.053 – ident: e_1_2_8_14_1 doi: 10.1002/elps.200500906 – ident: e_1_2_8_12_1 doi: 10.1002/jssc.201100282 – ident: e_1_2_8_8_1 doi: 10.1016/j.talanta.2010.03.016 – ident: e_1_2_8_6_1 doi: 10.1016/S0021-9673(02)00840-3 – ident: e_1_2_8_16_1 doi: 10.1021/ac951199e |
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| Snippet | Derivatized β‐cyclodextrin (β‐CD) functionalized monolithic columns were prepared by a “one‐step” strategy using click chemistry. First, the intended... Derivatized β-cyclodextrin (β-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended... Derivatized [beta]-cyclodextrin ([beta]-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended... Derivatized beta-cyclodextrin (beta-CD) functionalized monolithic columns were prepared by a "one-step" strategy using click chemistry. First, the intended... |
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| SubjectTerms | Analysis Analytical chemistry beta-cyclodextrin beta-Cyclodextrins - chemical synthesis beta-Cyclodextrins - chemistry beta-Cyclodextrins/chemical synthesis/chemistry Biological and medical sciences Cadmium Chemical engineering Chemical synthesis Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography Chromatography, High Pressure Liquid - instrumentation Click Chemistry Columns (structural) Derivatized beta-cyclodextrin Derivatized β-cyclodextrin drugs enantiomers Exact sciences and technology Fourier transform infrared spectroscopy Fourier transforms General pharmacology high performance liquid chromatography Human health sciences hydrophilic interactions Liquid chromatography Mass spectrometry Medical sciences Methacrylates - chemistry methylation Monolithic columns Monomers non-polar compounds Nucleosides Other chromatographic methods Peptides Pharmacie, pharmacologie & toxicologie Pharmacology. Drug treatments Pharmacy, pharmacology & toxicology physicochemical properties scanning electron microscopy Sciences de la santé humaine Separation Strategy |
| Title | One‐step strategy for the synthesis of a derivatized cyclodextrin‐based monolithic column |
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