Solvent-mediated assembly of atom-precise gold–silver nanoclusters to semiconducting one-dimensional materials

Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve d...

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Published inNature communications Vol. 11; no. 1; pp. 2229 - 8
Main Authors Yuan, Peng, Zhang, Ruihua, Selenius, Elli, Ruan, Pengpeng, Yao, Yangrong, Zhou, Yang, Malola, Sami, Häkkinen, Hannu, Teo, Boon K., Cao, Yang, Zheng, Nanfeng
Format Journal Article
LanguageEnglish
Published London Nature Publishing Group UK 06.05.2020
Nature Publishing Group
Nature Portfolio
Subjects
119/118
639/925/357/1016
639/925/357/354
639/925/357/995
Anisotropy
Atomic structure
Clusters
Crystal structure
Crystals
Density functional theory
Design
Field effect transistors
Gold
Hole mobility
Humanities and Social Sciences
multidisciplinary
Nanoclusters
Nanomaterials
Nanotechnology
P-type semiconductors
Polymerization
Polymers
Properties (attributes)
Science
Science (multidisciplinary)
Self-assembly
Semiconductor devices
Silver
Single crystals
Solvents
X-ray diffraction
Online AccessGet full text

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Abstract Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold–silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag–Au–Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p -type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm 2 V −1 s −1 , and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties. Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Here, the authors demonstrate a solvent-mediated polymerization of atom-precise gold–silver nanoclusters into macroscopic single crystals with highly anisotropic p -type semiconducting characteristics.
AbstractList Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold–silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag–Au–Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p -type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm 2 V −1 s −1 , and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties. Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Here, the authors demonstrate a solvent-mediated polymerization of atom-precise gold–silver nanoclusters into macroscopic single crystals with highly anisotropic p -type semiconducting characteristics.
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold–silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag–Au–Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p -type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm 2 V −1 s −1 , and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties.
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold-silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag-Au-Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p-type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm V s , and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties.
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Here, the authors demonstrate a solvent-mediated polymerization of atom-precise gold–silver nanoclusters into macroscopic single crystals with highly anisotropic p-type semiconducting characteristics.
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold–silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag–Au–Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p-type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm2 V−1 s−1, and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties.Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Here, the authors demonstrate a solvent-mediated polymerization of atom-precise gold–silver nanoclusters into macroscopic single crystals with highly anisotropic p-type semiconducting characteristics.
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold-silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag-Au-Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p-type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm2 V-1 s-1, and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties.Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Atom-precise metal nanoclusters are well-characterizable building blocks for designing tunable nanomaterials, but it has been challenging to achieve directed assembly to macroscopic functional cluster-based materials with highly anisotropic properties. Here, we discover a solvent-mediated assembly of 34-atom intermetallic gold-silver clusters protected by 20 1-ethynyladamantanes into 1D polymers with Ag-Au-Ag bonds between neighboring clusters as shown directly by the atomic structure from single-crystal X-ray diffraction analysis. Density functional theory calculations predict that the single crystals of cluster polymers have a band gap of about 1.3 eV. Field-effect transistors fabricated with single crystals of cluster polymers feature highly anisotropic p-type semiconductor properties with ≈1800-fold conductivity in the direction of the polymer as compared to cross directions, hole mobility of ≈0.02 cm2 V-1 s-1, and an ON/OFF ratio up to ≈4000. This performance holds promise for further design of functional cluster-based materials with highly anisotropic semiconducting properties.
ArticleNumber 2229
Author Häkkinen, Hannu
Zheng, Nanfeng
Malola, Sami
Zhou, Yang
Ruan, Pengpeng
Cao, Yang
Yuan, Peng
Selenius, Elli
Zhang, Ruihua
Yao, Yangrong
Teo, Boon K.
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/32376829$$D View this record in MEDLINE/PubMed
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SSID ssj0000391844
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Snippet Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior....
Bottom-up design of functional device components based on nanometer-sized building blocks relies on accurate control of their self-assembly behavior. Here, the...
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StartPage 2229
SubjectTerms 119/118
639/925/357/1016
639/925/357/354
639/925/357/995
Anisotropy
Atomic structure
Clusters
Crystal structure
Crystals
Density functional theory
Design
Field effect transistors
Gold
Hole mobility
Humanities and Social Sciences
multidisciplinary
Nanoclusters
Nanomaterials
Nanotechnology
P-type semiconductors
Polymerization
Polymers
Properties (attributes)
Science
Science (multidisciplinary)
Self-assembly
Semiconductor devices
Silver
Single crystals
Solvents
X-ray diffraction
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Title Solvent-mediated assembly of atom-precise gold–silver nanoclusters to semiconducting one-dimensional materials
URI https://link.springer.com/article/10.1038/s41467-020-16062-6
https://www.ncbi.nlm.nih.gov/pubmed/32376829
https://www.proquest.com/docview/2399211539
https://www.proquest.com/docview/2399830306
https://pubmed.ncbi.nlm.nih.gov/PMC7203111
https://doaj.org/article/7e78097684564beda99abfe396f555ab
Volume 11
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