Designable ultra-smooth ultra-thin solid-electrolyte interphases of three alkali metal anodes
Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte inte...
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| Published in | Nature communications Vol. 9; no. 1; pp. 1339 - 9 |
|---|---|
| Main Authors | , , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
09.04.2018
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm
–2
with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes.
The dendrite growth of alkali metal anodes leads to charge/discharge cycling instability. Here, the authors show that electrochemical polishing can yield near-perfect anodes of three alkali metals by constructing smooth and thin solid-electrolyte interphase layers. |
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| AbstractList | Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm
–2
with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes. The dendrite growth of alkali metal anodes leads to charge/discharge cycling instability. Here, the authors show that electrochemical polishing can yield near-perfect anodes of three alkali metals by constructing smooth and thin solid-electrolyte interphase layers. Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm –2 with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes. The dendrite growth of alkali metal anodes leads to charge/discharge cycling instability. Here, the authors show that electrochemical polishing can yield near-perfect anodes of three alkali metals by constructing smooth and thin solid-electrolyte interphase layers. Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes. Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm–2 with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes. Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm-2 with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes.Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and potassium metals achieved by electrochemical polishing, which removes microscopic defects and creates ultra-smooth ultra-thin solid-electrolyte interphase layers at metal surfaces for providing a homogeneous environment. Precise characterizations by AFM force probing with corroborative in-depth XPS profile analysis reveal that the ultra-smooth ultra-thin solid-electrolyte interphase can be designed to have alternating inorganic-rich and organic-rich/mixed multi-layered structure, which offers mechanical property of coupled rigidity and elasticity. The polished metal anodes exhibit significantly enhanced cycling stability, specifically the lithium anodes can cycle for over 200 times at a real current density of 2 mA cm-2 with 100% depth of discharge. Our work illustrates that an ultra-smooth ultra-thin solid-electrolyte interphase may be robust enough to suppress dendrite growth and thus serve as an initial layer for further improved protection of alkali metal anodes. |
| ArticleNumber | 1339 |
| Author | Chen, Zhao-Bin Tang, Shuai Wu, De-Yin Li, Yi-Juan Dong, Quan-Feng Hu, Wei-Qiang Gu, Yu Wu, Qi-Hui Wang, Wei-Wei Fang, Yuan Zhang, Qing-Hong Zheng, Ming-Sen Mao, Bing-Wei Yan, Jia-Wei Fan, Chun-Hai |
| Author_xml | – sequence: 1 givenname: Yu surname: Gu fullname: Gu, Yu organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 2 givenname: Wei-Wei surname: Wang fullname: Wang, Wei-Wei organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 3 givenname: Yi-Juan surname: Li fullname: Li, Yi-Juan organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 4 givenname: Qi-Hui surname: Wu fullname: Wu, Qi-Hui organization: Department of Materials Chemistry, College of Chemical Engineering and Materials Science, Quanzhou Normal University – sequence: 5 givenname: Shuai surname: Tang fullname: Tang, Shuai organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 6 givenname: Jia-Wei surname: Yan fullname: Yan, Jia-Wei organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 7 givenname: Ming-Sen orcidid: 0000-0001-9302-4631 surname: Zheng fullname: Zheng, Ming-Sen organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 8 givenname: De-Yin surname: Wu fullname: Wu, De-Yin organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 9 givenname: Chun-Hai orcidid: 0000-0002-7171-7338 surname: Fan fullname: Fan, Chun-Hai organization: Division of Physical Biology & Bioimaging Center, Shanghai Synchrotron Radiation Facility, CAS Key Laboratory of Interfacial Physics and Technology, Shanghai Institute of Applied Physics, Chinese Academy of Sciences – sequence: 10 givenname: Wei-Qiang surname: Hu fullname: Hu, Wei-Qiang organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 11 givenname: Zhao-Bin surname: Chen fullname: Chen, Zhao-Bin organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 12 givenname: Yuan surname: Fang fullname: Fang, Yuan organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 13 givenname: Qing-Hong surname: Zhang fullname: Zhang, Qing-Hong organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 14 givenname: Quan-Feng surname: Dong fullname: Dong, Quan-Feng email: qfdong@xmu.edu.cn organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University – sequence: 15 givenname: Bing-Wei surname: Mao fullname: Mao, Bing-Wei email: bwmao@xmu.edu.cn organization: State Key Laboratory of Physical Chemistry of Solid Surfaces and Department of Chemistry, iChEM, College of Chemistry and Chemical Engineering, Xiamen University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29632301$$D View this record in MEDLINE/PubMed |
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| Snippet | Dendrite growth of alkali metal anodes limited their lifetime for charge/discharge cycling. Here, we report near-perfect anodes of lithium, sodium, and... The dendrite growth of alkali metal anodes leads to charge/discharge cycling instability. Here, the authors show that electrochemical polishing can yield... |
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| SubjectTerms | 140/146 147/135 147/3 639/4077/4079/891 639/638/161 Alkali metals Anodes Anodic protection Atomic force microscopy Chemical polishing Cycles Dendrites Dendritic structure Discharge Elasticity Electrochemistry Electrolytes Electropolishing Humanities and Social Sciences Interphase Lithium Metal surfaces Metals multidisciplinary Multilayers Rigidity Science Science (multidisciplinary) Sodium Thin films X ray photoelectron spectroscopy |
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| Title | Designable ultra-smooth ultra-thin solid-electrolyte interphases of three alkali metal anodes |
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