Intragranular cracking as a critical barrier for high-voltage usage of layer-structured cathode for lithium-ion batteries
LiNi 1/3 Mn 1/3 Co 1/3 O 2 -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular crac...
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| Published in | Nature communications Vol. 8; no. 1; p. 14101 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
16.01.2017
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | LiNi
1/3
Mn
1/3
Co
1/3
O
2
-layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi
1/3
Mn
1/3
Co
1/3
O
2
cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials.
Cycling-induced fracture can limit conditions for stable operation for various lithium-ion electrode materials. Here, the authors characterize fracture in nickel-manganese-cobalt oxide microscopically and provide evidence for dislocation-assisted, intragranular fracture operating above a critical voltage threshold. |
|---|---|
| AbstractList | LiNi1/3 Mn1/3 Co1/3 O2 -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi1/3 Mn1/3 Co1/3 O2 cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials. Cycling-induced fracture can limit conditions for stable operation for various lithium-ion electrode materials. Here, the authors characterize fracture in nickel-manganese-cobalt oxide microscopically and provide evidence for dislocation-assisted, intragranular fracture operating above a critical voltage threshold. LiNi1/3Mn1/3Co1/3O2 (NMC333) layered cathode is often fabricated as secondary particles of consisting of densely packed primary particles, which offers advantage of high energy density and alleviation of cathode side reactions/corrosions, but introduces other drawbacks, such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in the commercial NMC333 layered cathode by using advanced S/TEM. We found that the formation of the intragranular cracks is directly associated with high voltage cycling, which is an electrochemically driven and diffusion controlled process. The intragranular cracks were noticed to be characteristically initiated from grain interior, a consequence of dislocation based crack incubation mechanism. This observation is in sharp contrast with the general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surface. As a result, our study indicates that maintain a structural stability is the key step toward high voltage operation of layered cathode materials. LiNi Mn Co O -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi Mn Co O cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials. LiNi 1/3 Mn 1/3 Co 1/3 O 2 -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi 1/3 Mn 1/3 Co 1/3 O 2 cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials. Cycling-induced fracture can limit conditions for stable operation for various lithium-ion electrode materials. Here, the authors characterize fracture in nickel-manganese-cobalt oxide microscopically and provide evidence for dislocation-assisted, intragranular fracture operating above a critical voltage threshold. LiNi 1/3 Mn 1/3 Co 1/3 O 2 -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi 1/3 Mn 1/3 Co 1/3 O 2 cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials. LiNi1/3Mn1/3Co1/3O2-layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages for high energy density and alleviation of cathode side reactions/corrosions, but introduces drawbacks such as intergranular cracking. Here, we report unexpected observations on the nucleation and growth of intragranular cracks in a commercial LiNi1/3Mn1/3Co1/3O2 cathode by using advanced scanning transmission electron microscopy. We find the formation of the intragranular cracks is directly associated with high-voltage cycling, an electrochemically driven and diffusion-controlled process. The intragranular cracks are noticed to be characteristically initiated from the grain interior, a consequence of a dislocation-based crack incubation mechanism. This observation is in sharp contrast with general theoretical models, predicting the initiation of intragranular cracks from grain boundaries or particle surfaces. Our study emphasizes that maintaining structural stability is the key step towards high-voltage operation of layered-cathode materials. |
| ArticleNumber | 14101 |
| Author | Xiao, Jie Yan, Pengfei Zhang, Ji-Guang Gu, Meng Wang, Chong-Min Zheng, Jianming |
| Author_xml | – sequence: 1 givenname: Pengfei surname: Yan fullname: Yan, Pengfei organization: Environmental Molecular Sciences Laboratory, Pacific Northwest National Laboratory – sequence: 2 givenname: Jianming surname: Zheng fullname: Zheng, Jianming organization: Energy and Environment Directorate, Pacific Northwest National Laboratory – sequence: 3 givenname: Meng surname: Gu fullname: Gu, Meng organization: Environmental Molecular Sciences Laboratory, Pacific Northwest National Laboratory – sequence: 4 givenname: Jie surname: Xiao fullname: Xiao, Jie organization: Energy and Environment Directorate, Pacific Northwest National Laboratory – sequence: 5 givenname: Ji-Guang orcidid: 0000-0001-7343-4609 surname: Zhang fullname: Zhang, Ji-Guang email: Jiguang.zhang@pnnl.gov organization: Energy and Environment Directorate, Pacific Northwest National Laboratory – sequence: 6 givenname: Chong-Min surname: Wang fullname: Wang, Chong-Min email: Chongmin.wang@pnnl.gov organization: Environmental Molecular Sciences Laboratory, Pacific Northwest National Laboratory |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28091602$$D View this record in MEDLINE/PubMed https://www.osti.gov/servlets/purl/1339807$$D View this record in Osti.gov |
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| SSID | ssj0000391844 |
| Score | 2.6733918 |
| Snippet | LiNi
1/3
Mn
1/3
Co
1/3
O
2
-layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers... LiNi Mn Co O -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers advantages... LiNi1/3 Mn1/3 Co1/3 O2 -layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers... LiNi1/3Mn1/3Co1/3O2-layered cathode is often fabricated in the form of secondary particles, consisting of densely packed primary particles. This offers... LiNi1/3Mn1/3Co1/3O2 (NMC333) layered cathode is often fabricated as secondary particles of consisting of densely packed primary particles, which offers... Cycling-induced fracture can limit conditions for stable operation for various lithium-ion electrode materials. Here, the authors characterize fracture in... |
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| StartPage | 14101 |
| SubjectTerms | 639/301/299/161 639/4077/4079/891 batteries Cracks dislocation electrochemistry Electrodes Electrolytes Electrons ENERGY STORAGE Environmental Molecular Sciences Laboratory high voltage cycling Humanities and Social Sciences intragranular crack layered cathode Lithium lithium ion battery multidisciplinary Science Science (multidisciplinary) |
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| Title | Intragranular cracking as a critical barrier for high-voltage usage of layer-structured cathode for lithium-ion batteries |
| URI | https://link.springer.com/article/10.1038/ncomms14101 https://www.ncbi.nlm.nih.gov/pubmed/28091602 https://www.proquest.com/docview/1858736483 https://www.proquest.com/docview/1861514953 https://www.osti.gov/servlets/purl/1339807 https://pubmed.ncbi.nlm.nih.gov/PMC5241805 https://doaj.org/article/8af225752edc4fa092ba295ec870556a |
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