One‐pot synthesis of a new high vinyl content hybrid silica monolith dedicated to nanoliquid chromatography

A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide,...

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Published inJournal of separation science Vol. 39; no. 5; pp. 842 - 850
Main Authors Racha, El‐Debs, Gay, Pauline, Dugas, Vincent, Demesmay, Claire
Format Journal Article
LanguageEnglish
Published Germany Wiley-VCH 01.03.2016
Blackwell Publishing Ltd
Wiley Subscription Services, Inc
Wiley-VCH Verlag
Subjects
Analytical chemistry
Capillarity
Catalysts
Chemical Sciences
Chemical synthesis
Chromatography
Density
Hybrid silica monoliths
Liquid chromatography
Nanostructure
Nitric acid
nitrogen
nuclear magnetic resonance spectroscopy
porous media
scanning electron microscopy
Silica
silicon
Silicon dioxide
surface area
Synthesis
Vinyl monoliths
Vinyl monoliths
Liquid chromatography
Hybrid silica monoliths
CAPILLARY LIQUID-CHROMATOGRAPHY
CEC
ENE CLICK CHEMISTRY
MESOPORES
STATIONARY-PHASE
ELECTROCHROMATOGRAPHY
COLUMNS
FABRICATION
STEP SYNTHESIS
SEPARATION
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Abstract A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, ²⁹Si nuclear magnetic resonance spectroscopy and N₂ adsorption–desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m²/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed‐phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed‐phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
AbstractList A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, 29Si nuclear magnetic resonance spectroscopy and N2 adsorption–desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m2/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed‐phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed‐phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, (29) Si nuclear magnetic resonance spectroscopy and N2 adsorption-desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m(2) /g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed-phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed-phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, 29 Si nuclear magnetic resonance spectroscopy and N 2 adsorption–desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m 2 /g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed‐phase mode. Plots of ln( k ) versus percentage of organic modifier were used to assess the reversed‐phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized ( N = 120 000).
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, super(29)Si nuclear magnetic resonance spectroscopy and N sub(2) adsorption-desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m super(2)/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed-phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed-phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, 29Si nuclear magnetic resonance spectroscopy and N2 adsorption-desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m2/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed-phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed-phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl hybridmacroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, Si-29 nuclear magnetic resonance spectroscopy and N-2 adsorption-desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m(2)/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed-phasemode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed-phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid macroporous monolith, by cocondensation of vinyltrimethoxysilane with tetramethoxysilane, was investigated using an unconventional (formamide, nitric acid) porogen/catalyst system. A macroporous hybrid silica monolith with 80% in mass of vinyltrimethoxysilane in the feeding silane solution was obtained and compared to a more conventional low vinyl content hybrid monolith with only of 20% vinyltrimethoxysilane. Monoliths were characterized by scanning electron microscopy, ²⁹Si nuclear magnetic resonance spectroscopy and N₂ adsorption–desorption. About 80% of the vinyl precursor was incorporated in the final materials, leading to 15.9 and 61.5% of Si atoms bonded to vinyl groups for 20% vinyltrimethoxysilane and 80% vinyltrimethoxysilane, respectively. The 80% vinyltrimethoxysilane monolith presents a lower surface area than 20% vinyltrimethoxysilane (159 versus 551 m²/g), which is nevertheless compensated by a higher vinyl surface density. Chromatographic properties were evaluated in reversed‐phase mode. Plots of ln(k) versus percentage of organic modifier were used to assess the reversed‐phase mechanism. Its high content of organic groups leads to high retention properties. Column efficiencies of 170 000 plates/m were measured for this 80% vinyltrimethoxysilane hybrid silica monolith. Long capillary monolithic columns (90 cm) were successfully synthesized (N = 120 000).
Author Racha, El‐Debs
Gay, Pauline
Demesmay, Claire
Dugas, Vincent
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Cites_doi 10.1039/C0CS00068J
10.1021/ac702343a
10.1021/cm990369r
10.1002/jssc.201300231
10.1021/ac9000749
10.1016/j.chroma.2014.09.017
10.1016/j.talanta.2012.01.009
10.1002/elps.200900627
10.1021/cm000451i
10.1016/j.chroma.2012.07.071
10.1023/A:1009627216939
10.1039/b207617a
10.1002/elps.201200354
10.1016/j.chroma.2008.08.119
10.1002/jssc.200401816
10.1039/b502870a
10.1007/s00216-013-7026-7
10.1002/jssc.201401264
10.1016/j.chroma.2011.05.090
10.1039/b508415f
10.1002/elps.201400316
10.1002/jssc.200700359
10.1002/jssc.200700304
10.1002/1521-4095(200010)12:19<1403::AID-ADMA1403>3.0.CO;2-X
10.1016/j.chroma.2009.11.019
10.1021/ja00521a016
10.1016/j.chroma.2011.07.048
10.1021/ja025573l
10.1002/jssc.200900147
10.1002/elps.201200344
10.1039/c2cc37974k
10.1039/b903444g
10.1021/cm052776a
10.1002/chem.201403982
10.1351/pac198557040603
10.1016/j.chroma.2014.06.023
10.1002/jssc.201400773
10.1016/j.talanta.2014.11.044
10.1016/j.chroma.2014.06.031
10.1016/j.chroma.2014.12.031
10.1002/jssc.201200084
10.1016/j.chroma.2015.05.073
10.1039/b501833c
10.1023/A:1020770209234
10.1016/j.chroma.2008.03.064
10.1016/j.chroma.2013.02.008
ContentType Journal Article
Copyright 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim
2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Distributed under a Creative Commons Attribution 4.0 International License
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– notice: 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
– notice: 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
– notice: Distributed under a Creative Commons Attribution 4.0 International License
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Issue 5
Keywords Vinyl monoliths
Liquid chromatography
Hybrid silica monoliths
CAPILLARY LIQUID-CHROMATOGRAPHY
CEC
ENE CLICK CHEMISTRY
MESOPORES
STATIONARY-PHASE
ELECTROCHROMATOGRAPHY
COLUMNS
FABRICATION
STEP SYNTHESIS
SEPARATION
Language English
License 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Distributed under a Creative Commons Attribution 4.0 International License: http://creativecommons.org/licenses/by/4.0
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References Zhang, Z., Wang, F., Xu, B., Qin, H., Ye, M., Zou, H., J. Chromatogr. A 2012, 1256, 136-143.
Roux, R., Puy, G., Demesmay, C., Rocca, J.-L., J. Sep. Sci. 2007, 30, 3035-3042.
Marechal, A., Jarrosson, F., Randon, J., Dugas, V., Demesmay, C., J. Chromatogr. A 2015, 1406, 109-117.
Nakanishi, K., J. Porous Mater. 1997, 4, 67-112.
Kanamori, K., Yonezawa, H., Nakanishi, K., Hirao, K., Jinnai, H., J. Sep. Sci. 2004, 27, 874-886.
Sagiv, J., J. Am. Chem. Soc. 1980, 102, 92-98.
Nakanishi, K., Kanamori, K., J. Mater. Chem. 2005, 15, 3776-3786.
Popp, M., Sulyok, M., Rosenberg, E., J. Sep. Sci. 2007, 30, 2888-2899.
Marechal, A., El-Debs, R., Dugas, V., Demesmay, C., J. Sep. Sci. 2013, 36, 2049-2062.
Qin, W., Lu, H., Xie, Z., J. Sep. Sci. 2014, 37, 3722-3728.
Yang, F., Mao, J., He, X. W., Chen, L. X., Zhang, Y. K., Anal. Bioanal. Chem. 2013, 405, 6639-6648.
Wu, M., Wu, R.a., Wang, F., Ren, L., Dong, J., Liu, Z., Zou, H., Anal. Chem. 2009, 81, 3529-3536.
Zhu, T., Row, K. H., J. Sep. Sci. 2012, 35, 1294-1302.
Bruns, S., Hara, T., Smarsly, B. M., Tallarek, U., J. Chromatogr. A 2011, 1218, 5187-5194.
Ou, J., Liu, Z., Wang, H., Lin, H., Dong, J., Zou, H., Electrophoresis 2015, 36, 62-75.
Laaniste, A., Marechal, A., El-Debs, R., Randon, J., Dugas, V., Demesmay, C., J. Chromatogr. A 2014, 1355, 296-300.
Hara, T., Makino, S., Watanabe, Y., Ikegami, T., Cabrera, K., Smarsly, B., Tanaka, N., J. Chromatogr. A 2010, 1217, 89-98.
Rozga-Wijas, K., Chojnowski, J., Scibiorek, M., Fortuniak, W., J. Mater. Chem. 2005, 15, 2383-2392.
Ou, J., Lin, H., Zhang, Z., Huang, G., Dong, J., Zou, H., Electrophoresis 2013, 34, 126-140.
Chen, M.-L., Zhang, J., Zhang, Z., Yuan, B.-F., Yu, Q.-W., Feng, Y.-Q., J. Chromatogr. A 2013, 1284, 118-125.
Göbel, R., Hesemann, P., Friedrich, A., Rothe, R., Schlaad, H., Taubert, A., Chem. Eur. J. 2014, 20, 17579-17589.
Stein, A., Melde, B. J., Schroden, R. C., Adv. Mater. 2000, 12, 1403-1419.
Kanamori, K., Nakanishi, K., Chem. Soc. Rev. 2011, 40, 754-770.
Rahayu, A., Lim, L.W., Takeuchi, T., J. Sep. Sci. 2015, 38, 1109-1116.
Marechal, A., Laaniste, A., El-Debs, R., Dugas, V., Demesmay, C., J. Chromatogr. A 2014, 1365, 140-147.
Alekseev, S. A., Zaitsev, V. N., Fraissard, J.Chem. Mater. 2006, 18, 1981-1987.
Li, L., Colón, L. A., J. Sep. Sci. 2009, 32, 2737-2746.
Loy, D. A., Baugher, B. M., Baugher, C. R., Schneider, D. A., Rahimian, K., Chem. Mater. 2000, 12, 3624-3632.
Laschober, S., Rosenberg, E., J. Chromatogr. A 2008, 1191, 282-291.
Yang, H., Chen, Y., Liu, Y., Nie, L., Yao, S., Electrophoresis 2013, 34, 510-517.
Wang, K., Chen, Y., Yang, H., Li, Y., Nie, L., Yao, S., Talanta 2012, 91, 52-59.
Lim, M. H., Stein, A., Chem. Mater. 1999, 11, 3285-3295.
Roux, R., Jaoudé, M. A., Demesmay, C., Rocca, J. L., J. Chromatogr. A 2008, 1209, 120-127.
Xie, Y., Zhang, X., Han, Q., Wan, W., Ding, M., Talanta 2015, 134, 425-434.
Igarashi, N., Hashimoto, K., Tatsumi, T., J. Mater. Chem. 2002, 12, 3631-3636.
Wu, M., Zhang, H., Wang, Z., Shen, S., Le, X.C., Li, X.-F., Chem. Commun. 2013, 49, 1407-1409.
Itagaki, A., Nakanishi, K., Hirao, K., J. Solgel Sci. Technol. 2003, 26, 153-156.
Ma, J., Liang, Z., Qiao, X., Deng, Q., Tao, D., Zhang, L., Zhang, Y., Anal. Chem. 2008, 80, 2949-2956.
Lin, Z., Tan, X., Yu, R., Lin, J., Yin, X., Zhang, L., Yang, H., J. Chromatogr. A 2014, 1355, 228-237.
Feng, R., Tian, Y., Chen, H., Huang, Z., Zeng, Z., Electrophoresis 2010, 31, 1975-1982.
Zhang, Z., Lin, H., Ou, J., Qin, H., Wu, R.a., Dong, J., Zou, H., J. Chromatogr. A 2012, 1228, 263-269.
Kanamori, K., Nakanishi, K., Hanada, T., Soft Matter 2009, 5, 3106-3113.
Colon, H., Zhang, X., Murphy, J. K., Rivera, J. G., Colon, L. A., Chem. Commun. 2005, 22, 2826-2828.
Kruk, M., Asefa, T., Jaroniec, M., Ozin, G. A., J. Am. Chem. Soc. 2002, 124, 6383-6392.
Sing, K. S. W., Everett, D. H., R.A.W, H. L. M., Pierotti, J., Rouquerol, J., Siemienwska, T., Pure Appl. Chem. 1985, 57, 603-619.
Lin, H., Ou, J., Liu, Z., Wang, H., Dong, J., Zou, H., J. Chromatogr. A 2015, 1379, 34-42.
2015; 36
2010; 31
2015; 38
2013; 49
2009; 81
2008; 1191
2013; 405
2004; 27
2002; 12
2011; 40
2012; 1228
2010; 1217
2006; 18
2015; 1379
2014; 1365
2007; 30
2012; 35
1997; 4
2005; 22
2014; 20
2012; 91
2012; 1256
2013; 36
2009; 32
2015; 1406
2000; 12
2013; 34
2002; 124
2015; 134
2013; 1284
2014; 37
1999; 11
2003; 26
2011; 1218
2009; 5
2005; 15
2014; 1355
2008; 80
1980; 102
1985; 57
2008; 1209
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References_xml – volume: 1217
  start-page: 89
  year: 2010
  end-page: 98
  publication-title: J. Chromatogr. A
– volume: 35
  start-page: 1294
  year: 2012
  end-page: 1302
  publication-title: J. Sep. Sci.
– volume: 12
  start-page: 1403
  year: 2000
  end-page: 1419
  publication-title: Adv. Mater.
– volume: 1365
  start-page: 140
  year: 2014
  end-page: 147
  publication-title: J. Chromatogr. A
– volume: 37
  start-page: 3722
  year: 2014
  end-page: 3728
  publication-title: J. Sep. Sci.
– volume: 27
  start-page: 874
  year: 2004
  end-page: 886
  publication-title: J. Sep. Sci.
– volume: 57
  start-page: 603
  year: 1985
  end-page: 619
  publication-title: Pure Appl. Chem.
– volume: 405
  start-page: 6639
  year: 2013
  end-page: 6648
  publication-title: Anal. Bioanal. Chem.
– volume: 1191
  start-page: 282
  year: 2008
  end-page: 291
  publication-title: J. Chromatogr. A
– volume: 1284
  start-page: 118
  year: 2013
  end-page: 125
  publication-title: J. Chromatogr. A
– volume: 1406
  start-page: 109
  year: 2015
  end-page: 117
  publication-title: J. Chromatogr. A
– volume: 15
  start-page: 3776
  year: 2005
  end-page: 3786
  publication-title: J. Mater. Chem.
– volume: 1218
  start-page: 5187
  year: 2011
  end-page: 5194
  publication-title: J. Chromatogr. A
– volume: 102
  start-page: 92
  year: 1980
  end-page: 98
  publication-title: J. Am. Chem. Soc.
– volume: 34
  start-page: 510
  year: 2013
  end-page: 517
  publication-title: Electrophoresis
– volume: 134
  start-page: 425
  year: 2015
  end-page: 434
  publication-title: Talanta
– volume: 15
  start-page: 2383
  year: 2005
  end-page: 2392
  publication-title: J. Mater. Chem.
– volume: 1256
  start-page: 136
  year: 2012
  end-page: 143
  publication-title: J. Chromatogr. A
– volume: 4
  start-page: 67
  year: 1997
  end-page: 112
  publication-title: J. Porous Mater.
– volume: 91
  start-page: 52
  year: 2012
  end-page: 59
  publication-title: Talanta
– volume: 32
  start-page: 2737
  year: 2009
  end-page: 2746
  publication-title: J. Sep. Sci.
– volume: 1379
  start-page: 34
  year: 2015
  end-page: 42
  publication-title: J. Chromatogr. A
– volume: 30
  start-page: 2888
  year: 2007
  end-page: 2899
  publication-title: J. Sep. Sci
– volume: 80
  start-page: 2949
  year: 2008
  end-page: 2956
  publication-title: Anal. Chem.
– volume: 38
  start-page: 1109
  year: 2015
  end-page: 1116
  publication-title: J. Sep. Sci.
– volume: 1228
  start-page: 263
  year: 2012
  end-page: 269
  publication-title: J. Chromatogr. A
– volume: 36
  start-page: 2049
  year: 2013
  end-page: 2062
  publication-title: J. Sep. Sci.
– volume: 26
  start-page: 153
  year: 2003
  end-page: 156
  publication-title: J. Solgel Sci. Technol.
– volume: 31
  start-page: 1975
  year: 2010
  end-page: 1982
  publication-title: Electrophoresis
– volume: 11
  start-page: 3285
  year: 1999
  end-page: 3295
  publication-title: Chem. Mater.
– volume: 12
  start-page: 3631
  year: 2002
  end-page: 3636
  publication-title: J. Mater. Chem.
– volume: 34
  start-page: 126
  year: 2013
  end-page: 140
  publication-title: Electrophoresis
– volume: 36
  start-page: 62
  year: 2015
  end-page: 75
  publication-title: Electrophoresis
– volume: 1355
  start-page: 296
  year: 2014
  end-page: 300
  publication-title: J. Chromatogr. A
– volume: 81
  start-page: 3529
  year: 2009
  end-page: 3536
  publication-title: Anal. Chem.
– volume: 30
  start-page: 3035
  year: 2007
  end-page: 3042
  publication-title: J. Sep. Sci.
– volume: 5
  start-page: 3106
  year: 2009
  end-page: 3113
  publication-title: Soft Matter
– volume: 20
  start-page: 17579
  year: 2014
  end-page: 17589
  publication-title: Chem. Eur. J.
– volume: 124
  start-page: 6383
  year: 2002
  end-page: 6392
  publication-title: J. Am. Chem. Soc.
– volume: 40
  start-page: 754
  year: 2011
  end-page: 770
  publication-title: Chem. Soc. Rev.
– volume: 1209
  start-page: 120
  year: 2008
  end-page: 127
  publication-title: J. Chromatogr. A
– volume: 18
  start-page: 1981
  year: 2006
  end-page: 1987
  publication-title: J.Chem. Mater.
– volume: 12
  start-page: 3624
  year: 2000
  end-page: 3632
  publication-title: Chem. Mater.
– volume: 1355
  start-page: 228
  year: 2014
  end-page: 237
  publication-title: J. Chromatogr. A
– volume: 49
  start-page: 1407
  year: 2013
  end-page: 1409
  publication-title: Chem. Commun.
– volume: 22
  start-page: 2826
  year: 2005
  end-page: 2828
  publication-title: Chem. Commun.
– ident: e_1_2_6_10_1
  doi: 10.1039/C0CS00068J
– ident: e_1_2_6_16_1
  doi: 10.1021/ac702343a
– ident: e_1_2_6_13_1
  doi: 10.1021/cm990369r
– ident: e_1_2_6_29_1
  doi: 10.1002/jssc.201300231
– ident: e_1_2_6_35_1
  doi: 10.1021/ac9000749
– ident: e_1_2_6_30_1
  doi: 10.1016/j.chroma.2014.09.017
– ident: e_1_2_6_22_1
  doi: 10.1016/j.talanta.2012.01.009
– ident: e_1_2_6_45_1
  doi: 10.1002/elps.200900627
– ident: e_1_2_6_7_1
  doi: 10.1021/cm000451i
– ident: e_1_2_6_36_1
  doi: 10.1016/j.chroma.2012.07.071
– ident: e_1_2_6_5_1
  doi: 10.1023/A:1009627216939
– ident: e_1_2_6_15_1
  doi: 10.1039/b207617a
– ident: e_1_2_6_38_1
  doi: 10.1002/elps.201200354
– ident: e_1_2_6_21_1
  doi: 10.1016/j.chroma.2008.08.119
– ident: e_1_2_6_6_1
  doi: 10.1002/jssc.200401816
– ident: e_1_2_6_19_1
  doi: 10.1039/b502870a
– ident: e_1_2_6_37_1
  doi: 10.1007/s00216-013-7026-7
– ident: e_1_2_6_25_1
  doi: 10.1002/jssc.201401264
– ident: e_1_2_6_9_1
  doi: 10.1016/j.chroma.2011.05.090
– ident: e_1_2_6_14_1
  doi: 10.1039/b508415f
– ident: e_1_2_6_4_1
  doi: 10.1002/elps.201400316
– ident: e_1_2_6_12_1
  doi: 10.1002/jssc.200700359
– ident: e_1_2_6_20_1
  doi: 10.1002/jssc.200700304
– ident: e_1_2_6_26_1
  doi: 10.1002/1521-4095(200010)12:19<1403::AID-ADMA1403>3.0.CO;2-X
– ident: e_1_2_6_42_1
  doi: 10.1016/j.chroma.2009.11.019
– ident: e_1_2_6_33_1
  doi: 10.1021/ja00521a016
– ident: e_1_2_6_46_1
  doi: 10.1016/j.chroma.2011.07.048
– ident: e_1_2_6_44_1
  doi: 10.1021/ja025573l
– ident: e_1_2_6_41_1
  doi: 10.1002/jssc.200900147
– ident: e_1_2_6_3_1
  doi: 10.1002/elps.201200344
– ident: e_1_2_6_39_1
  doi: 10.1039/c2cc37974k
– ident: e_1_2_6_8_1
  doi: 10.1039/b903444g
– ident: e_1_2_6_34_1
  doi: 10.1021/cm052776a
– ident: e_1_2_6_23_1
  doi: 10.1002/chem.201403982
– ident: e_1_2_6_43_1
  doi: 10.1351/pac198557040603
– ident: e_1_2_6_18_1
  doi: 10.1016/j.chroma.2014.06.023
– ident: e_1_2_6_24_1
  doi: 10.1002/jssc.201400773
– ident: e_1_2_6_27_1
  doi: 10.1016/j.talanta.2014.11.044
– ident: e_1_2_6_31_1
  doi: 10.1016/j.chroma.2014.06.031
– ident: e_1_2_6_47_1
  doi: 10.1016/j.chroma.2014.12.031
– ident: e_1_2_6_2_1
  doi: 10.1002/jssc.201200084
– ident: e_1_2_6_32_1
  doi: 10.1016/j.chroma.2015.05.073
– ident: e_1_2_6_28_1
  doi: 10.1039/b501833c
– ident: e_1_2_6_40_1
  doi: 10.1023/A:1020770209234
– ident: e_1_2_6_11_1
  doi: 10.1016/j.chroma.2008.03.064
– ident: e_1_2_6_17_1
  doi: 10.1016/j.chroma.2013.02.008
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Snippet A new vinyltrimethoxysilane‐based hybrid silica monolith was developed and used as a reversed‐phase capillary column. The synthesis of this rich vinyl hybrid...
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl hybrid...
A new vinyltrimethoxysilane-based hybrid silica monolith was developed and used as a reversed-phase capillary column. The synthesis of this rich vinyl...
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SubjectTerms Analytical chemistry
Capillarity
Catalysts
Chemical Sciences
Chemical synthesis
Chromatography
Density
Hybrid silica monoliths
Liquid chromatography
Nanostructure
Nitric acid
nitrogen
nuclear magnetic resonance spectroscopy
porous media
scanning electron microscopy
Silica
silicon
Silicon dioxide
surface area
Synthesis
Vinyl monoliths
Title One‐pot synthesis of a new high vinyl content hybrid silica monolith dedicated to nanoliquid chromatography
URI https://api.istex.fr/ark:/67375/WNG-2WH7X0S3-5/fulltext.pdf
https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fjssc.201501076
https://www.ncbi.nlm.nih.gov/pubmed/26719150
https://www.proquest.com/docview/1770021055
https://search.proquest.com/docview/1770883588
https://search.proquest.com/docview/1800495500
https://hal.science/hal-01356863
Volume 39
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