Effect of ultrasound irradiation on asphaltene aggregation and implications to rheological behavior of bitumen
•The contribution of asphaltene aggregation to bitumen viscosity is studied.•The ultrasound waves reduce the viscosity of the bitumen.•The applied frequency and the gas environment influence the bitumen viscosity reduction.•A positive correlation between the asphaltene yield and the viscosity is est...
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| Published in | Ultrasonics sonochemistry Vol. 80; p. 105811 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Netherlands
Elsevier B.V
01.12.2021
Elsevier |
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| Online Access | Get full text |
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| Abstract | •The contribution of asphaltene aggregation to bitumen viscosity is studied.•The ultrasound waves reduce the viscosity of the bitumen.•The applied frequency and the gas environment influence the bitumen viscosity reduction.•A positive correlation between the asphaltene yield and the viscosity is established.
The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N2) and carbon dioxide (CO2). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N2 environment could lower the bitumen viscosity up to 3274cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). |
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| AbstractList | The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N
) and carbon dioxide (CO
). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N
environment could lower the bitumen viscosity up to 3274cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N2) and carbon dioxide (CO2). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N2 environment could lower the bitumen viscosity up to 3274cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency).The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N2) and carbon dioxide (CO2). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N2 environment could lower the bitumen viscosity up to 3274cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). • The contribution of asphaltene aggregation to bitumen viscosity is studied. • The ultrasound waves reduce the viscosity of the bitumen. • The applied frequency and the gas environment influence the bitumen viscosity reduction. • A positive correlation between the asphaltene yield and the viscosity is established. The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043 cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N 2 ) and carbon dioxide (CO 2 ). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079 cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N 2 environment could lower the bitumen viscosity up to 3274 cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043 cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N2) and carbon dioxide (CO2). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079 cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N2 environment could lower the bitumen viscosity up to 3274 cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). •The contribution of asphaltene aggregation to bitumen viscosity is studied.•The ultrasound waves reduce the viscosity of the bitumen.•The applied frequency and the gas environment influence the bitumen viscosity reduction.•A positive correlation between the asphaltene yield and the viscosity is established. The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a viscosity of 12043cP at room temperature was sonicated at low (38 kHz) and mild frequency (200 kHz) under controlled gas environment including air, nitrogen (N2) and carbon dioxide (CO2). The rheology of the bitumen, asphaltene content analyses as well as spectral studies were conducted. Herein was found that sonicating the bitumen at 200 kHz under air-environment reduces the initial viscosity up to 2079cP, which was twice larger than that obtained when a low frequency was used. In respect of the gas environment, it was shown that ultrasound irradiation under N2 environment could lower the bitumen viscosity up to 3274cP. A positive correlation between the asphaltene content and the viscosity reduction was established. The results from the spectral analyses including Fast Fourier Infrared and the observations from Scanned Electron Microscope were consistent with the rheological studies and led to the argument that the viscosity reduction results from either the scission of long chain molecules attached to the aromatic rings (when the applied frequency was altered under fixed gas environment) or the self-aggregation of asphaltene monomers (when gas environment was changed at fixed frequency). |
| ArticleNumber | 105811 |
| Author | Okawa, Hirokazu Nguele, Ronald |
| Author_xml | – sequence: 1 givenname: Ronald orcidid: 0000-0002-0364-0017 surname: Nguele fullname: Nguele, Ronald email: nguele@mine.kyushu-u.ac.jp organization: Resource Production & Safety Engineering Laboratory, Kyushu University, Fukuoka 819-0395, Japan – sequence: 2 givenname: Hirokazu surname: Okawa fullname: Okawa, Hirokazu organization: Graduate School of Engineering Science, Akita University, Akita 010-8502, Japan |
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| CitedBy_id | crossref_primary_10_1021_acs_iecr_3c03126 crossref_primary_10_1080_10916466_2022_2049817 crossref_primary_10_1021_acs_energyfuels_2c01541 crossref_primary_10_1061_JMCEE7_MTENG_16461 crossref_primary_10_2118_209476_PA crossref_primary_10_1016_j_cep_2023_109619 crossref_primary_10_1016_j_ultsonch_2023_106542 crossref_primary_10_1021_acs_iecr_4c00182 crossref_primary_10_1016_j_fuel_2022_123372 |
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| Keywords | Asphaltene Sonication Bitumen viscosity Ultrasound Bitumen |
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| Snippet | •The contribution of asphaltene aggregation to bitumen viscosity is studied.•The ultrasound waves reduce the viscosity of the bitumen.•The applied frequency... The present work investigates the contribution of asphaltene aggregation to bitumen viscosity subject to ultrasound irradiation. A West-African bitumen with a... • The contribution of asphaltene aggregation to bitumen viscosity is studied. • The ultrasound waves reduce the viscosity of the bitumen. • The applied... |
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| SubjectTerms | Asphaltene Bitumen Bitumen viscosity Original Sonication Ultrasound |
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| Title | Effect of ultrasound irradiation on asphaltene aggregation and implications to rheological behavior of bitumen |
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