Specific and Selective Determination Method for Halide Anions by a Flow Injection Technique
A flow-injection analysis system is described for the determination of halide (chloride, bromide and iodide) anions. This method could be used as a post column detection method for these anions in water samples. The system is based on the specific and selective reaction between halide anion and fluo...
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| Published in | Chemical & pharmaceutical bulletin Vol. 32; no. 9; pp. 3702 - 3705 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Tokyo
The Pharmaceutical Society of Japan
01.01.1984
Maruzen Japan Science and Technology Agency |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A flow-injection analysis system is described for the determination of halide (chloride, bromide and iodide) anions. This method could be used as a post column detection method for these anions in water samples. The system is based on the specific and selective reaction between halide anion and fluorescein with an oxidant in an acidic flow. The product is detected at 530 nm in an alkaline flow. The detection limits of the three anions under the conditions tentatively established for the determination of bromide anion were as follows ; Cl-, 1×10-8mol ; Br-, 1×10-10mol ; I-, 1×10-10mol. |
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| AbstractList | A flow-injection analysis system is described for the determination of halide (chloride, bromide and iodide) anions. This method could be used as a post column detection method for these anions in water samples. The system is based on the specific and selective reaction between halide anion and fluorescein with an oxidant in an acidic flow. The product is detected at 530 nm in an alkaline flow. The detection limits of the three anions under the conditions tentatively established for the determination of bromide anion were as follows ; Cl-, 1×10-8mol ; Br-, 1×10-10mol ; I-, 1×10-10mol. |
| Author | MIYAZAKI, MOTOICHI HAYAKAWA, KAZUICHI UMEDA, TOSHIHIKO OKUBO, NOBORU |
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| Copyright | The Pharmaceutical Society of Japan 1985 INIST-CNRS Copyright Japan Science and Technology Agency 1984 |
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| Discipline | Pharmacy, Therapeutics, & Pharmacology Chemistry |
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| Issue | 9 |
| Keywords | Water Absorption spectrometry Chemical analysis Iodides Analytical reagent Flow(fluid) Chlorides Detection limit Bromides Visible spectrometry Injection |
| Language | English |
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| References | 5) "Standard Methods of Chemical Analysis in Poisoning With Commentary-" authorized by the Pharmaceutical Society of Japan, Tokyo, 1974, p. 89. 1) Parts of this work were presented at the 102nd Annual Meeting of the Pharmaceutical Society of Japan, Osaka, April 1982, and at the 3rd Liquid Chromatography Forum, Tokyo, October 1982. 3) a) F. Feigl, "Spot Tests; Inorganic Applications," Vol. I, Elsevier Publishing Co., Amsterdam, 1954, p. 245 d) K. Kawanabe, S. Takitani, M. Miyazaki and Z. Tamura, Jpn. Analyst, 13, 976 (1964). b) Z. Tamura and M. Miyazaki, Jpn. Analyst, 5, 566 (1956 4) J. Ruzicka and E. H. Hansen, Anal. Chim. Acta, 78, 145 (1975). 2) H. Small, T. S. Stevens and W. C. Bauman, Anal. Chem., 47, 1081 (1975). c) F. A. Pohl, Z. Anal. Chem., 149, 68 (1956 |
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| Snippet | A flow-injection analysis system is described for the determination of halide (chloride, bromide and iodide) anions. This method could be used as a post column... |
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| SubjectTerms | Analytical chemistry bromovalerylurea Chemistry Exact sciences and technology Spectrometric and optical methods |
| Title | Specific and Selective Determination Method for Halide Anions by a Flow Injection Technique |
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