Thermally stable single atom Pt/m-Al2O3 for selective hydrogenation and CO oxidation

Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under...

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Published in	Nature communications Vol. 8; no. 1; p. 16100
Main Authors	Zhang, Zailei, Zhu, Yihan, Asakura, Hiroyuki, Zhang, Bin, Zhang, Jiaguang, Zhou, Maoxiang, Han, Yu, Tanaka, Tsunehiro, Wang, Aiqin, Zhang, Tao, Yan, Ning
Format	Journal Article
Language	English
Published	London Nature Publishing Group UK 27.07.2017 Nature Publishing Group Nature Portfolio
Subjects	1,3-Butadiene 140/131 140/146 639/638/224/685 639/638/77/887 Agglomeration Aluminum Aluminum oxide Butadiene Catalysts Chemical industry Clusters Cobalt Control stability Humanities and Social Sciences Hydrogenation Metals multidisciplinary n-Hexane Nanoparticles Oxidation Platinum Reforming Science Science (multidisciplinary) Single atom catalysts Structural integrity Thermal stability
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Abstract	Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under demanding conditions. The Pt atoms are firmly anchored in the internal surface of mesoporous Al 2 O 3 , likely stabilized by coordinatively unsaturated pentahedral Al 3+ centres. The catalyst keeps its structural integrity and excellent performance for the selective hydrogenation of 1,3-butadiene after exposure to a reductive atmosphere at 200 °C for 24 h. Compared to commercial Pt nanoparticle catalyst on Al 2 O 3 and control samples, this system exhibits significantly enhanced stability and performance for n -hexane hydro-reforming at 550 °C for 48 h, although agglomeration of Pt single-atoms into clusters is observed after reaction. In CO oxidation, the Pt single-atom identity was fully maintained after 60 cycles between 100 and 400 °C over a one-month period. Using precious noble elements as single atom metal catalysts is highly desirable and effective. Here the authors show the use of platinum atom catalysts anchored in mesoporous Al 2 O 3 for selective hydrogenation and CO oxidation that have better stability and performance compared to their nanoparticle counterparts.
AbstractList	Using precious noble elements as single atom metal catalysts is highly desirable and effective. Here the authors show the use of platinum atom catalysts anchored in mesoporous Al2O3for selective hydrogenation and CO oxidation that have better stability and performance compared to their nanoparticle counterparts. Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under demanding conditions. The Pt atoms are firmly anchored in the internal surface of mesoporous Al 2 O 3 , likely stabilized by coordinatively unsaturated pentahedral Al 3+ centres. The catalyst keeps its structural integrity and excellent performance for the selective hydrogenation of 1,3-butadiene after exposure to a reductive atmosphere at 200 °C for 24 h. Compared to commercial Pt nanoparticle catalyst on Al 2 O 3 and control samples, this system exhibits significantly enhanced stability and performance for n -hexane hydro-reforming at 550 °C for 48 h, although agglomeration of Pt single-atoms into clusters is observed after reaction. In CO oxidation, the Pt single-atom identity was fully maintained after 60 cycles between 100 and 400 °C over a one-month period. Using precious noble elements as single atom metal catalysts is highly desirable and effective. Here the authors show the use of platinum atom catalysts anchored in mesoporous Al 2 O 3 for selective hydrogenation and CO oxidation that have better stability and performance compared to their nanoparticle counterparts. Abstract Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under demanding conditions. The Pt atoms are firmly anchored in the internal surface of mesoporous Al 2 O 3 , likely stabilized by coordinatively unsaturated pentahedral Al 3+ centres. The catalyst keeps its structural integrity and excellent performance for the selective hydrogenation of 1,3-butadiene after exposure to a reductive atmosphere at 200 °C for 24 h. Compared to commercial Pt nanoparticle catalyst on Al 2 O 3 and control samples, this system exhibits significantly enhanced stability and performance for n -hexane hydro-reforming at 550 °C for 48 h, although agglomeration of Pt single-atoms into clusters is observed after reaction. In CO oxidation, the Pt single-atom identity was fully maintained after 60 cycles between 100 and 400 °C over a one-month period. Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under demanding conditions. The Pt atoms are firmly anchored in the internal surface of mesoporous Al2 O3 , likely stabilized by coordinatively unsaturated pentahedral Al3+ centres. The catalyst keeps its structural integrity and excellent performance for the selective hydrogenation of 1,3-butadiene after exposure to a reductive atmosphere at 200 °C for 24 h. Compared to commercial Pt nanoparticle catalyst on Al2 O3 and control samples, this system exhibits significantly enhanced stability and performance for n-hexane hydro-reforming at 550 °C for 48 h, although agglomeration of Pt single-atoms into clusters is observed after reaction. In CO oxidation, the Pt single-atom identity was fully maintained after 60 cycles between 100 and 400 °C over a one-month period. Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and sufficiently stable. Herein, we report a synthetic strategy for Pt single-atom catalysts with outstanding stability in several reactions under demanding conditions. The Pt atoms are firmly anchored in the internal surface of mesoporous Al2O3, likely stabilized by coordinatively unsaturated pentahedral Al3+ centres. The catalyst keeps its structural integrity and excellent performance for the selective hydrogenation of 1,3-butadiene after exposure to a reductive atmosphere at 200 °C for 24 h. Compared to commercial Pt nanoparticle catalyst on Al2O3 and control samples, this system exhibits significantly enhanced stability and performance for n-hexane hydro-reforming at 550 °C for 48 h, although agglomeration of Pt single-atoms into clusters is observed after reaction. In CO oxidation, the Pt single-atom identity was fully maintained after 60 cycles between 100 and 400 °C over a one-month period.
ArticleNumber	16100
Author	Asakura, Hiroyuki Zhu, Yihan Wang, Aiqin Yan, Ning Zhang, Bin Zhang, Zailei Zhang, Jiaguang Zhou, Maoxiang Han, Yu Tanaka, Tsunehiro Zhang, Tao
Author_xml	– sequence: 1 givenname: Zailei surname: Zhang fullname: Zhang, Zailei organization: Department of Chemical and Biomolecular Engineering, National University of Singapore – sequence: 2 givenname: Yihan surname: Zhu fullname: Zhu, Yihan organization: Physical Sciences and Engineering Division, Advanced Membranes and Porous Materials Center, King Abdullah University of Science and Technology – sequence: 3 givenname: Hiroyuki surname: Asakura fullname: Asakura, Hiroyuki organization: Department of Molecular Engineering, Graduate School of Engineering, Kyoto University, Elements Strategy Initiative for Catalysts & Batteries (ESICB), Kyoto University – sequence: 4 givenname: Bin surname: Zhang fullname: Zhang, Bin organization: Department of Chemical and Biomolecular Engineering, National University of Singapore – sequence: 5 givenname: Jiaguang orcidid: 0000-0001-7238-4021 surname: Zhang fullname: Zhang, Jiaguang organization: Department of Chemical and Biomolecular Engineering, National University of Singapore – sequence: 6 givenname: Maoxiang surname: Zhou fullname: Zhou, Maoxiang organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 7 givenname: Yu orcidid: 0000-0003-1462-1118 surname: Han fullname: Han, Yu organization: Physical Sciences and Engineering Division, Advanced Membranes and Porous Materials Center, King Abdullah University of Science and Technology, Physical Sciences and Engineering Division, KAUST Catalysis Center, King Abdullah University of Science and Technology – sequence: 8 givenname: Tsunehiro surname: Tanaka fullname: Tanaka, Tsunehiro organization: Department of Molecular Engineering, Graduate School of Engineering, Kyoto University, Elements Strategy Initiative for Catalysts & Batteries (ESICB), Kyoto University – sequence: 9 givenname: Aiqin surname: Wang fullname: Wang, Aiqin organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 10 givenname: Tao surname: Zhang fullname: Zhang, Tao organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 11 givenname: Ning orcidid: 0000-0002-1877-9206 surname: Yan fullname: Yan, Ning email: ning.yan@nus.edu.sg organization: Department of Chemical and Biomolecular Engineering, National University of Singapore
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Snippet	Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically active and... Abstract Single-atom metal catalysts offer a promising way to utilize precious noble metal elements more effectively, provided that they are catalytically... Using precious noble elements as single atom metal catalysts is highly desirable and effective. Here the authors show the use of platinum atom catalysts...
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StartPage	16100
SubjectTerms	1,3-Butadiene 140/131 140/146 639/638/224/685 639/638/77/887 Agglomeration Aluminum Aluminum oxide Butadiene Catalysts Chemical industry Clusters Cobalt Control stability Humanities and Social Sciences Hydrogenation Metals multidisciplinary n-Hexane Nanoparticles Oxidation Platinum Reforming Science Science (multidisciplinary) Single atom catalysts Structural integrity Thermal stability
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Title	Thermally stable single atom Pt/m-Al2O3 for selective hydrogenation and CO oxidation
URI	https://link.springer.com/article/10.1038/ncomms16100 https://www.proquest.com/docview/1923719876 https://search.proquest.com/docview/1924600875 https://pubmed.ncbi.nlm.nih.gov/PMC5537564 https://doaj.org/article/3662c2cb15524bb68c20f36b5e384153
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