山核桃蒲壳化学成分定性鉴定及总生物碱提取工艺研究

O657; 采用试管法、纸层析法(PPC)和薄层层析法(TLC),初步鉴定了山核桃蒲壳中的氨基酸、多糖、黄酮、皂苷、挥发油、强心苷、生物碱组分.采用正交实验法,考察提取温度、乙醇浓度、液料比、提取时间对总生物碱提取率的影响.研究结果表明,提取温度与乙醇浓度对总生物碱提取率的影响显著(P<0.05),较佳提取条件为:50%乙醇,60 ℃水浴提取2次,每次1.5 h,液料比5∶1....

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Published in浙江大学学报（理学版） Vol. 36; no. 4; pp. 442 - 449
Main Authors 姜著英, 宣贵达, 李林林
Format Journal Article
LanguageChinese
Published 浙江大学 药学院,浙江 杭州,310058%浙江大学 城市学院,浙江 杭州,310015 2009
Subjects
总生物碱
化学成分
山核桃蒲壳
Online AccessGet full text
ISSN1008-9497
DOI10.3785/j.issn.1008-9497.2009.04.018

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Abstract O657; 采用试管法、纸层析法(PPC)和薄层层析法(TLC),初步鉴定了山核桃蒲壳中的氨基酸、多糖、黄酮、皂苷、挥发油、强心苷、生物碱组分.采用正交实验法,考察提取温度、乙醇浓度、液料比、提取时间对总生物碱提取率的影响.研究结果表明,提取温度与乙醇浓度对总生物碱提取率的影响显著(P<0.05),较佳提取条件为:50%乙醇,60 ℃水浴提取2次,每次1.5 h,液料比5∶1.
AbstractList O657; 采用试管法、纸层析法(PPC)和薄层层析法(TLC),初步鉴定了山核桃蒲壳中的氨基酸、多糖、黄酮、皂苷、挥发油、强心苷、生物碱组分.采用正交实验法,考察提取温度、乙醇浓度、液料比、提取时间对总生物碱提取率的影响.研究结果表明,提取温度与乙醇浓度对总生物碱提取率的影响显著(P<0.05),较佳提取条件为:50%乙醇,60 ℃水浴提取2次,每次1.5 h,液料比5∶1.
Author 宣贵达
李林林
姜著英
AuthorAffiliation 浙江大学 药学院,浙江 杭州,310058%浙江大学 城市学院,浙江 杭州,310015
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JIANG Zhu-ying
LI Lin-lin
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Title 山核桃蒲壳化学成分定性鉴定及总生物碱提取工艺研究
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