Challenges in the size analysis of a silica nanoparticle mixture as candidate certified reference material
A new certified reference material for quality control of nanoparticle size analysis methods has been developed and produced by the Institute for Reference Materials and Measurements of the European Commission’s Joint Research Centre. The material, ERM-FD102, consists of an aqueous suspension of a m...
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Published in | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology Vol. 18; no. 6; p. 171 |
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Main Authors | , , , , , , , , , , , , |
Format | Journal Article |
Language | English |
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Dordrecht
Springer Netherlands
2016
Springer Nature B.V |
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Abstract | A new certified reference material for quality control of nanoparticle size analysis methods has been developed and produced by the Institute for Reference Materials and Measurements of the European Commission’s Joint Research Centre. The material, ERM-FD102, consists of an aqueous suspension of a mixture of silica nanoparticle populations of distinct particle size and origin. The characterisation relied on an interlaboratory comparison study in which 30 laboratories of demonstrated competence participated with a variety of techniques for particle size analysis. After scrutinising the received datasets, certified and indicative values for different method-defined equivalent diameters that are specific for dynamic light scattering (DLS), centrifugal liquid sedimentation (CLS), scanning and transmission electron microscopy (SEM and TEM), atomic force microscopy (AFM), particle tracking analysis (PTA) and asymmetrical-flow field-flow fractionation (AF4) were assigned. The value assignment was a particular challenge because metrological concepts were not always interpreted uniformly across all participating laboratories. This paper presents the main elements and results of the ERM-FD102 characterisation study and discusses in particular the key issues of measurand definition and the estimation of measurement uncertainty. |
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AbstractList | A new certified reference material for quality control of nanoparticle size analysis methods has been developed and produced by the Institute for Reference Materials and Measurements of the European Commission's Joint Research Centre. The material, ERM-FD102, consists of an aqueous suspension of a mixture of silica nanoparticle populations of distinct particle size and origin. The characterisation relied on an interlaboratory comparison study in which 30 laboratories of demonstrated competence participated with a variety of techniques for particle size analysis. After scrutinising the received datasets, certified and indicative values for different method-defined equivalent diameters that are specific for dynamic light scattering (DLS), centrifugal liquid sedimentation (CLS), scanning and transmission electron microscopy (SEM and TEM), atomic force microscopy (AFM), particle tracking analysis (PTA) and asymmetrical-flow field-flow fractionation (AF4) were assigned. The value assignment was a particular challenge because metrological concepts were not always interpreted uniformly across all participating laboratories. This paper presents the main elements and results of the ERM-FD102 characterisation study and discusses in particular the key issues of measurand definition and the estimation of measurement uncertainty. A new certified reference material for quality control of nanoparticle size analysis methods has been developed and produced by the Institute for Reference Materials and Measurements of the European Commission’s Joint Research Centre. The material, ERM-FD102, consists of an aqueous suspension of a mixture of silica nanoparticle populations of distinct particle size and origin. The characterisation relied on an interlaboratory comparison study in which 30 laboratories of demonstrated competence participated with a variety of techniques for particle size analysis. After scrutinising the received datasets, certified and indicative values for different method-defined equivalent diameters that are specific for dynamic light scattering (DLS), centrifugal liquid sedimentation (CLS), scanning and transmission electron microscopy (SEM and TEM), atomic force microscopy (AFM), particle tracking analysis (PTA) and asymmetrical-flow field-flow fractionation (AF4) were assigned. The value assignment was a particular challenge because metrological concepts were not always interpreted uniformly across all participating laboratories. This paper presents the main elements and results of the ERM-FD102 characterisation study and discusses in particular the key issues of measurand definition and the estimation of measurement uncertainty. |
ArticleNumber | 171 |
Author | Roebben, Gert Clifford, Charles Coleman, Victoria Jämting, Åsa Babick, Frank Cölfen, Helmut Kestens, Vikram Minelli, Caterina Mast, Jan De Temmerman, Pieter-Jan Junjie, Liu Emons, Hendrik Herrmann, Jan |
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Keywords | Quality assurance Measurement uncertainty Silica nanoparticles Interlaboratory comparison study Measurand Particle size analysis Certified reference material Nanotechnology |
Language | English |
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publication-title: J Microcolumn Sep doi: 10.1002/(SICI)1520-667X(1997)9:3<151::AID-MCS3>3.0.CO;2-0 contributor: fullname: MN Myers – start-page: 867 volume-title: Physical methods of chemistry year: 1989 ident: 3474_CR17 contributor: fullname: JC Giddings – volume: 8 start-page: 187 year: 1991 ident: 3474_CR14 publication-title: Part Part Syst Charact doi: 10.1002/ppsc.19910080135 contributor: fullname: R Finsy – volume: 272 start-page: 1 year: 1993 ident: 3474_CR57 publication-title: Anal Chim Acta doi: 10.1016/0003-2670(93)80373-S contributor: fullname: PJ Wyatt – ident: 3474_CR48 – volume: 27 start-page: 229 year: 1982 ident: 3474_CR53 publication-title: Comput Phys Commun doi: 10.1016/0010-4655(82)90174-6 contributor: fullname: SW Provencher – volume: 13 start-page: 7317 year: 2011 ident: 3474_CR42 publication-title: J Nanopart Res doi: 10.1007/s11051-011-0624-4 contributor: fullname: A Lamberty – volume-title: Small angle X-ray scattering year: 1982 ident: 3474_CR20 contributor: fullname: O Glatter – volume-title: ISO 9276-2, representation of results of particle size analysis—part 2: calculation of average particle sizes/diameters and moments from particle size distributions year: 2014 ident: 3474_CR35 contributor: fullname: ISO (International Organization for Standardization) – volume-title: ISO 13318-2, determination of particle size distribution by centrifugal liquid sedimentation methods—part 2: photocentrifuge method year: 2007 ident: 3474_CR29 contributor: fullname: ISO (International Organization for Standardization) – volume-title: Particle size measurements: fundamentals, practice, quality year: 2009 ident: 3474_CR49 contributor: fullname: HG Merkus – volume-title: Certification of equivalent spherical diameters of silica nanoparticles in water, certified reference material ERM-FD100, EUR 24620 EN, ISBN 978-92-79-18676-9 year: 2011 ident: 3474_CR5 contributor: fullname: A Braun – volume-title: Small angle scattering from X-rays year: 1955 ident: 3474_CR21 contributor: fullname: A Guinier – volume: 57 start-page: 4814 year: 1972 ident: 3474_CR40 publication-title: J Chem Phys doi: 10.1063/1.1678153 contributor: fullname: DE Koppel – volume-title: Solving least squares problems year: 1974 ident: 3474_CR43 contributor: fullname: L Lawson – ident: 3474_CR12 – volume: 10 start-page: 415 year: 1977 ident: 3474_CR19 publication-title: J Appl Crystallogr doi: 10.1107/S0021889877013879 contributor: fullname: O Glatter – volume-title: ISO 13322-1, particle size analysis—part 1: static image analysis methods year: 2004 ident: 3474_CR26 contributor: fullname: ISO (International Organization for Standardization) – volume-title: ISO 17867, particle size analysis—small-angle X-ray scattering year: 2015 ident: 3474_CR37 contributor: fullname: ISO (International Organization for Standardization) |
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SubjectTerms | Characterization and Evaluation of Materials Chemistry and Materials Science Fractionation Inorganic Chemistry Lasers Light scattering Materials Science Nanoparticles Nanotechnology Optical Devices Optics Particle size Photonics Physical Chemistry Quality control Research Paper Silica |
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Title | Challenges in the size analysis of a silica nanoparticle mixture as candidate certified reference material |
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