Spontaneously separated intermetallic Co3Mo from nanoporous copper as versatile electrocatalysts for highly efficient water splitting
Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co 3 Mo spontaneously separated from hierarchical nanoporous copper skeleton shows ge...
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| Published in | Nature communications Vol. 11; no. 1; pp. 2940 - 10 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
10.06.2020
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co
3
Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co
3
Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co
3
Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec
−1
) in 1 M KOH, realizing current density of −400 mA cm
−2
at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts.
Electrochemical water splitting is an attractive energy conversion technology, but it usually suffers from low efficiency. Here, the authors report intermetallic Co
3
Mo integrated on porous Cu as highly efficient electrocatalysts for alkaline HER/OER due to in-situ hydroxylation and electro-oxidation. |
|---|---|
| AbstractList | Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co
3
Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co
3
Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co
3
Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec
−1
) in 1 M KOH, realizing current density of −400 mA cm
−2
at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts. Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co3Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co3Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co3Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec-1) in 1 M KOH, realizing current density of -400 mA cm-2 at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts.Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co3Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co3Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co3Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec-1) in 1 M KOH, realizing current density of -400 mA cm-2 at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts. Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co 3 Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co 3 Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co 3 Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec −1 ) in 1 M KOH, realizing current density of −400 mA cm −2 at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts. Electrochemical water splitting is an attractive energy conversion technology, but it usually suffers from low efficiency. Here, the authors report intermetallic Co 3 Mo integrated on porous Cu as highly efficient electrocatalysts for alkaline HER/OER due to in-situ hydroxylation and electro-oxidation. Electrochemical water splitting is an attractive energy conversion technology, but it usually suffers from low efficiency. Here, the authors report intermetallic Co3Mo integrated on porous Cu as highly efficient electrocatalysts for alkaline HER/OER due to in-situ hydroxylation and electro-oxidation. Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in hydrogen production. Here, we report that intermetallic Co3Mo spontaneously separated from hierarchical nanoporous copper skeleton shows genuine potential as highly efficient electrocatalysts for alkaline hydrogen/oxygen evolution reactions in virtue of in-situ hydroxylation and electro-oxidation, respectively. The hydroxylated intermetallic Co3Mo has an optimal hydrogen-binding energy to facilitate adsorption/desorption of hydrogen intermediates for hydrogen molecules. Associated with high electron/ion transport of bicontinuous nanoporous skeleton, nanoporous copper supported Co3Mo electrodes exhibit impressive hydrogen evolution reaction catalysis, with negligible onset overpotential and low Tafel slope (~40 mV dec−1) in 1 M KOH, realizing current density of −400 mA cm−2 at overpotential of as low as 96 mV. When coupled to its electro-oxidized derivative that mediates efficiently oxygen evolution reaction, their alkaline electrolyzer operates with a superior overall water-splitting output, outperforming the one assembled with noble-metal-based catalysts.Electrochemical water splitting is an attractive energy conversion technology, but it usually suffers from low efficiency. Here, the authors report intermetallic Co3Mo integrated on porous Cu as highly efficient electrocatalysts for alkaline HER/OER due to in-situ hydroxylation and electro-oxidation. |
| ArticleNumber | 2940 |
| Author | Yao, Rui-Qi Lang, Xing-You Ge, Xin Zheng, Wei-Tao Zhang, Wei Shi, Hang Wen, Zi Jiang, Qing Wan, Wu-Bin Zhou, Yi-Tong |
| Author_xml | – sequence: 1 givenname: Hang orcidid: 0000-0002-7327-3582 surname: Shi fullname: Shi, Hang organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 2 givenname: Yi-Tong orcidid: 0000-0002-1094-7826 surname: Zhou fullname: Zhou, Yi-Tong organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 3 givenname: Rui-Qi orcidid: 0000-0002-9910-1463 surname: Yao fullname: Yao, Rui-Qi organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 4 givenname: Wu-Bin orcidid: 0000-0002-1995-7887 surname: Wan fullname: Wan, Wu-Bin organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 5 givenname: Xin surname: Ge fullname: Ge, Xin organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 6 givenname: Wei orcidid: 0000-0002-6414-7015 surname: Zhang fullname: Zhang, Wei organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 7 givenname: Zi orcidid: 0000-0002-6515-441X surname: Wen fullname: Wen, Zi organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 8 givenname: Xing-You orcidid: 0000-0002-8227-9695 surname: Lang fullname: Lang, Xing-You email: xylang@jlu.edu.cn organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 9 givenname: Wei-Tao surname: Zheng fullname: Zheng, Wei-Tao organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University – sequence: 10 givenname: Qing orcidid: 0000-0003-0660-596X surname: Jiang fullname: Jiang, Qing email: jiangq@jlu.edu.cn organization: Key Laboratory of Automobile Materials (Jilin University), Ministry of Education, School of Materials Science and Engineering, and Electron Microscopy Center, Jilin University |
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| Snippet | Developing robust nonprecious electrocatalysts towards hydrogen/oxygen evolution reactions is crucial for widespread use of electrochemical water splitting in... Electrochemical water splitting is an attractive energy conversion technology, but it usually suffers from low efficiency. Here, the authors report... |
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| SubjectTerms | 140/133 140/146 147/135 147/137 147/143 639/301/299/886 639/4077/909 639/638/77/884 Catalysis Catalysts Copper Electrocatalysts Electrochemistry Energy conversion Energy conversion efficiency Evolution Humanities and Social Sciences Hydrogen Hydrogen evolution reactions Hydrogen production Hydrogen-based energy Hydroxylation Intermediates Ion transport multidisciplinary Noble metals Oxidation Oxygen Oxygen evolution reactions Science Science (multidisciplinary) Splitting Water splitting |
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| Title | Spontaneously separated intermetallic Co3Mo from nanoporous copper as versatile electrocatalysts for highly efficient water splitting |
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