Unraveling of cocatalysts photodeposited selectively on facets of BiVO4 to boost solar water splitting
Bismuth vanadate (BiVO 4 ) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particu...
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| Published in | Nature communications Vol. 13; no. 1; pp. 484 - 9 |
|---|---|
| Main Authors | , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
25.01.2022
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Bismuth vanadate (BiVO
4
) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO
4
photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoO
x
), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoO
x
) on both interface charge separation and surface catalysis. Combined with the H
2
-evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN)
6
]
3−/4−
as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively.
Artificial photosynthesis offers an integrated means to convert light to fuel, but efficiencies are often low. Here, authors report a Z-scheme system utilizing Ir and FeCoO
x
co-catalysts to enhance charge separation on BiVO
4
facets that achieves high quantum efficiencies for overall water splitting. |
|---|---|
| AbstractList | Bismuth vanadate (BiVO4) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO4 photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoOx), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoOx) on both interface charge separation and surface catalysis. Combined with the H2-evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN)6]3−/4− as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively.Artificial photosynthesis offers an integrated means to convert light to fuel, but efficiencies are often low. Here, authors report a Z-scheme system utilizing Ir and FeCoOx co-catalysts to enhance charge separation on BiVO4 facets that achieves high quantum efficiencies for overall water splitting. Bismuth vanadate (BiVO4) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO4 photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoOx), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoOx) on both interface charge separation and surface catalysis. Combined with the H2-evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN)6]3-/4- as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively.Bismuth vanadate (BiVO4) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO4 photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoOx), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoOx) on both interface charge separation and surface catalysis. Combined with the H2-evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN)6]3-/4- as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively. Artificial photosynthesis offers an integrated means to convert light to fuel, but efficiencies are often low. Here, authors report a Z-scheme system utilizing Ir and FeCoOx co-catalysts to enhance charge separation on BiVO4 facets that achieves high quantum efficiencies for overall water splitting. Bismuth vanadate (BiVO 4 ) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO 4 photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoO x ), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoO x ) on both interface charge separation and surface catalysis. Combined with the H 2 -evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN) 6 ] 3−/4− as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively. Artificial photosynthesis offers an integrated means to convert light to fuel, but efficiencies are often low. Here, authors report a Z-scheme system utilizing Ir and FeCoO x co-catalysts to enhance charge separation on BiVO 4 facets that achieves high quantum efficiencies for overall water splitting. Bismuth vanadate (BiVO 4 ) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient cocatalysts and limited understanding of the underlying mechanism. Here we demonstrate significantly enhanced water oxidation on the particulate BiVO 4 photocatalyst via in situ facet-selective photodeposition of dual-cocatalysts that exist separately as metallic Ir nanoparticles and nanocomposite of FeOOH and CoOOH (denoted as FeCoO x ), as revealed by advanced techniques. The mechanism of water oxidation promoted by the dual-cocatalysts is experimentally and theoretically unraveled, and mainly ascribed to the synergistic effect of the spatially separated dual-cocatalysts (Ir, FeCoO x ) on both interface charge separation and surface catalysis. Combined with the H 2 -evolving photocatalysts, we finally construct a Z-scheme overall water splitting system using [Fe(CN) 6 ] 3−/4− as the redox mediator, whose apparent quantum efficiency at 420 nm and solar-to-hydrogen conversion efficiency are optimized to be 12.3% and 0.6%, respectively. |
| ArticleNumber | 484 |
| Author | Chen, Shanshan Liu, Wei Li, Deng Cui, Junyan Kong, Yuan Zhao, Yue Zhang, Jiangwei Domen, Kazunari Chen, Yifan Qi, Yu Xie, Tengfeng Li, Can Zhang, Fuxiang |
| Author_xml | – sequence: 1 givenname: Yu surname: Qi fullname: Qi, Yu organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 2 givenname: Jiangwei orcidid: 0000-0002-1221-3033 surname: Zhang fullname: Zhang, Jiangwei organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 3 givenname: Yuan surname: Kong fullname: Kong, Yuan organization: Hefei National Laboratory for Physical Sciences at the Microscale and Department of Chemical Physics, University of Science and Technology of China – sequence: 4 givenname: Yue surname: Zhao fullname: Zhao, Yue organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 5 givenname: Shanshan orcidid: 0000-0002-1801-8466 surname: Chen fullname: Chen, Shanshan organization: Research Initiative for Supra-Materials (RISM), Shinshu University – sequence: 6 givenname: Deng surname: Li fullname: Li, Deng organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 7 givenname: Wei surname: Liu fullname: Liu, Wei organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 8 givenname: Yifan surname: Chen fullname: Chen, Yifan organization: College of Chemistry, Jilin University – sequence: 9 givenname: Tengfeng surname: Xie fullname: Xie, Tengfeng organization: College of Chemistry, Jilin University – sequence: 10 givenname: Junyan surname: Cui fullname: Cui, Junyan organization: School of Material Science and Engineering, Zhengzhou University – sequence: 11 givenname: Can orcidid: 0000-0002-9301-7850 surname: Li fullname: Li, Can email: canli@dicp.ac.cn organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 12 givenname: Kazunari orcidid: 0000-0001-7995-4832 surname: Domen fullname: Domen, Kazunari organization: Research Initiative for Supra-Materials (RISM), Shinshu University, Office of University Professors, The University of Tokyo – sequence: 13 givenname: Fuxiang orcidid: 0000-0002-7859-0616 surname: Zhang fullname: Zhang, Fuxiang email: fxzhang@dicp.ac.cn organization: State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences |
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| Snippet | Bismuth vanadate (BiVO
4
) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient... Bismuth vanadate (BiVO4) has been widely investigated as a photocatalyst or photoanode for solar water splitting, but its activity is hindered by inefficient... Artificial photosynthesis offers an integrated means to convert light to fuel, but efficiencies are often low. Here, authors report a Z-scheme system utilizing... |
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| SubjectTerms | 119/118 147/135 147/143 639/638/224/909/4101/4050 639/638/439/890 639/925/357 Bismuth oxides Catalysis Catalysts Ferricyanide Humanities and Social Sciences multidisciplinary Nanocomposites Nanoparticles Oxidation Photocatalysts Photosynthesis Quantum efficiency Science Science (multidisciplinary) Separation Splitting Surface charge Synergistic effect Vanadate Vanadates Water splitting |
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| Title | Unraveling of cocatalysts photodeposited selectively on facets of BiVO4 to boost solar water splitting |
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