Ordered Hybrids from Template-Free Organosilane Self-Assembly
Despite considerable achievements over the last two decades, nonporous organic–inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self‐assembly approach is one of the few opportunities for creating a regular assembly of organic and...
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| Published in | Chemistry : a European journal Vol. 20; no. 7; pp. 1790 - 1806 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
10.02.2014
WILEY‐VCH Verlag Wiley Subscription Services, Inc Wiley-VCH Verlag |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0947-6539 1521-3765 1521-3765 |
| DOI | 10.1002/chem.201303070 |
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| Abstract | Despite considerable achievements over the last two decades, nonporous organic–inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self‐assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well‐established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono‐, bis‐, or multisilylated organosilane building blocks self‐assembling into hybrid mesostructures or superstructures, subsequently cross‐linked by siloxane Si‐O‐Si condensation. The general synthesis procedure is template‐free and one‐step. However, three concurrent processes underlie the generation of self‐organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self‐assembly, and kinetically controlled sol–gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long‐range order. Since the first developments in the mid‐1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research.
A successful marriage: Periodically ordered hybrids represent the successful marriage of organosilane sol–gel polymerization and supramolecular chemistry. Their template‐free and single‐step synthesis procedure has no equivalent in polymer chemistry (see scheme) |
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| AbstractList | Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three concurrent processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. A successful marriage: Periodically ordered hybrids represent the successful marriage of organosilane sol-gel polymerization and supramolecular chemistry. Their template-free and single-step synthesis procedure has no equivalent in polymer chemistry (see scheme) Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three concurrent processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three concurrent processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research.Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three concurrent processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. Despite considerable achievements over the last two decades, nonporous organic–inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self‐assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well‐established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono‐, bis‐, or multisilylated organosilane building blocks self‐assembling into hybrid mesostructures or superstructures, subsequently cross‐linked by siloxane Si‐O‐Si condensation. The general synthesis procedure is template‐free and one‐step. However, three concurrent processes underlie the generation of self‐organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self‐assembly, and kinetically controlled sol–gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long‐range order. Since the first developments in the mid‐1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. A successful marriage: Periodically ordered hybrids represent the successful marriage of organosilane sol–gel polymerization and supramolecular chemistry. Their template‐free and single‐step synthesis procedure has no equivalent in polymer chemistry (see scheme) Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three con-current processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of solvothermal processes. The organosilane self-assembly approach is one of the few opportunities for creating a regular assembly of organic and inorganic moieties. Additionally, well-established organosilicon chemistry enables the introduction of numerous organic functionalities. The synthesis of periodically ordered hybrids relies on mono-, bis-, or multisilylated organosilane building blocks self-assembling into hybrid mesostructures or superstructures, subsequently cross-linked by siloxane Si-O-Si condensation. The general synthesis procedure is template-free and one-step. However, three concurrent processes underlie the generation of self-organized hybrid networks: thermodynamics of amphiphilic aggregation, dynamic self-assembly, and kinetically controlled sol-gel chemistry. Hence, the set of experimental conditions and the precursor structure are of paramount importance in achieving long-range order. Since the first developments in the mid-1990s, the subject has seen considerable progress leading to many innovative advanced nanomaterials providing promising applications in membranes, pollutant remediation, catalysis, conductive coatings, and optoelectronics. This work reviews, comprehensively, the primary evolution of this expanding field of research. [PUBLICATION ABSTRACT] |
| Author | Boury, Bruno Ni, Lingli Chemtob, Abraham Croutxé-Barghorn, Céline |
| Author_xml | – sequence: 1 givenname: Abraham surname: Chemtob fullname: Chemtob, Abraham email: abraham.chemtob@uha.fr organization: Laboratory of Photochemistry and Macromolecular Engineering, ENSCMu, University of Haute-Alsace, 3 rue Alfred Werner 68093 Mulhouse Cedex (France), Fax: (+33) 389335014 – sequence: 2 givenname: Lingli surname: Ni fullname: Ni, Lingli organization: Laboratory of Photochemistry and Macromolecular Engineering, ENSCMu, University of Haute-Alsace, 3 rue Alfred Werner 68093 Mulhouse Cedex (France), Fax: (+33) 389335014 – sequence: 3 givenname: Céline surname: Croutxé-Barghorn fullname: Croutxé-Barghorn, Céline organization: Laboratory of Photochemistry and Macromolecular Engineering, ENSCMu, University of Haute-Alsace, 3 rue Alfred Werner 68093 Mulhouse Cedex (France), Fax: (+33) 389335014 – sequence: 4 givenname: Bruno surname: Boury fullname: Boury, Bruno organization: Institut Charles Gerhardt Montpellier, UMR5253 CNRS-UM2-ENSCM-UM1, Université Montpellier 2, Montpellier (France) |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/24449381$$D View this record in MEDLINE/PubMed https://hal.science/hal-04383919$$DView record in HAL |
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| Copyright | Copyright © 2014 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim Distributed under a Creative Commons Attribution 4.0 International License |
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| Keywords | self-assembly hybrid materials organosilane nanostructures sol-gel processes Ordered hybrids |
| Language | English |
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(e_1_2_7_3_2) 2006 e_1_2_7_148_2 e_1_2_7_114_2 e_1_2_7_50_2 e_1_2_7_73_2 e_1_2_7_96_2 e_1_2_7_21_2 e_1_2_7_35_2 e_1_2_7_58_2 e_1_2_7_152_2 e_1_2_7_175_2 e_1_2_7_198_2 e_1_2_7_212_2 e_1_2_7_175_3 e_1_2_7_137_2 e_1_2_7_103_2 e_1_2_7_126_2 e_1_2_7_6_2 e_1_2_7_18_2 e_1_2_7_61_2 e_1_2_7_190_2 e_1_2_7_209_2 e_1_2_7_84_2 e_1_2_7_10_2 e_1_2_7_46_2 e_1_2_7_69_2 e_1_2_7_141_2 e_1_2_7_164_2 e_1_2_7_187_2 e_1_2_7_201_2 e_1_2_7_224_2 e_1_2_7_149_2 e_1_2_7_115_2 e_1_2_7_72_2 e_1_2_7_22_2 e_1_2_7_95_2 e_1_2_7_34_2 e_1_2_7_57_2 e_1_2_7_130_2 e_1_2_7_153_2 e_1_2_7_199_2 e_1_2_7_176_2 e_1_2_7_213_2 e_1_2_7_138_2 |
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| Snippet | Despite considerable achievements over the last two decades, nonporous organic–inorganic hybrid materials are mostly amorphous, especially in the absence of... Despite considerable achievements over the last two decades, nonporous organic-inorganic hybrid materials are mostly amorphous, especially in the absence of... |
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| SubjectTerms | Amorphous materials Catalysis Chemical Sciences Chemistry Crosslinking hybrid materials Hybrids Long range order nanostructures Nanotechnology organosilane Other Polymerization Self assembly Sol gel process sol-gel processes Synthesis Synthesis (chemistry) |
| Title | Ordered Hybrids from Template-Free Organosilane Self-Assembly |
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