Ultrahigh Density of Atomic CoFe-Electron Synergy in Noncontinuous Carbon Matrix for Highly Efficient Magnetic Wave Adsorption
Highlights A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm. The ultrahigh-density distribution of the nanoscale polarized charges (+ / −) along the edges of the pores resulted in nanoscale variable c...
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| Published in | Nano-micro letters Vol. 14; no. 1; pp. 96 - 14 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Singapore
Springer Nature Singapore
01.12.2022
Springer Nature B.V Springer Singapore SpringerOpen |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Highlights
A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm.
The ultrahigh-density distribution of the nanoscale polarized charges (+ / −) along the edges of the pores resulted in nanoscale variable capacitors.
The high density of Co–Fe electromagnetic coupling on the carbon matrix, showing the enhanced electromagnetic wave attenuation.
Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg
−1
mm
−1
at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. |
|---|---|
| AbstractList | Highlights
A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm.
The ultrahigh-density distribution of the nanoscale polarized charges (+ / −) along the edges of the pores resulted in nanoscale variable capacitors.
The high density of Co–Fe electromagnetic coupling on the carbon matrix, showing the enhanced electromagnetic wave attenuation.
Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg
−1
mm
−1
at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. HighlightsA typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm.The ultrahigh-density distribution of the nanoscale polarized charges (+ / −) along the edges of the pores resulted in nanoscale variable capacitors.The high density of Co–Fe electromagnetic coupling on the carbon matrix, showing the enhanced electromagnetic wave attenuation.Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg−1 mm−1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. Improving the atom utilization of metals and clarifying the M-M' interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co-Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of - 57.7 dB and a specific RL value of - 192 dB mg-1 mm-1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption.Improving the atom utilization of metals and clarifying the M-M' interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co-Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of - 57.7 dB and a specific RL value of - 192 dB mg-1 mm-1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg −1 mm −1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. Improving the atom utilization of metals and clarifying the M-M' interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co-Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of - 57.7 dB and a specific RL value of - 192 dB mg mm at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm. The ultrahigh-density distribution of the nanoscale polarized charges (+ / −) along the edges of the pores resulted in nanoscale variable capacitors. The high density of Co–Fe electromagnetic coupling on the carbon matrix, showing the enhanced electromagnetic wave attenuation. Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg −1 mm −1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. Abstract Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light electromagnetic wave-absorbing materials. Herein, a high-temperature explosion strategy has been successfully applied to assemble the hierarchical porous carbon sponge with Co–Fe decoration via the pyrolysis of the energetic metal organic framework. The as-constructed hybrid displays a superior reflection loss (RL) value of − 57.7 dB and a specific RL value of − 192 dB mg−1 mm−1 at 12.08 GHz with a layer thickness of 2.0 mm (loading of 15 wt%). The off-axis electron hologram characterizes the highly distributed numerous polarized nanodomain variable capacitors, demonstrating the dipole and interfacial polarization along the edges of the nanopores. More importantly, the X-ray absorption spectroscopy analysis verifies the mutual interaction between the metal cluster and carbon matrix and the electronic coupling responsible for the greatly improved electromagnetic wave absorption. |
| ArticleNumber | 96 |
| Author | Zuo, Shouwei Zhang, Huabin Che, Renchao Bai, Jianan Huang, Wenhuan Qiu, Qiang Pei, Ke Yang, Xiufang |
| Author_xml | – sequence: 1 givenname: Wenhuan surname: Huang fullname: Huang, Wenhuan email: huangwenhuan@sust.edu.cn organization: Key Laboratory of Chemical Additives for China National Light Industry, College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology – sequence: 2 givenname: Qiang surname: Qiu fullname: Qiu, Qiang organization: Key Laboratory of Chemical Additives for China National Light Industry, College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology – sequence: 3 givenname: Xiufang surname: Yang fullname: Yang, Xiufang organization: Key Laboratory of Chemical Additives for China National Light Industry, College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology – sequence: 4 givenname: Shouwei surname: Zuo fullname: Zuo, Shouwei organization: Key Laboratory of Chemical Additives for China National Light Industry, College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology – sequence: 5 givenname: Jianan surname: Bai fullname: Bai, Jianan organization: Key Laboratory of Chemical Additives for China National Light Industry, College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology – sequence: 6 givenname: Huabin surname: Zhang fullname: Zhang, Huabin email: huabin.zhang@kaust.edu.sa organization: KAUST Catalysis Center, King Abdullah University of Science and Technology – sequence: 7 givenname: Ke surname: Pei fullname: Pei, Ke organization: Laboratory of Advanced Materials, Shanghai Key Lab of Molecular Catalysis and Innovative Materials, Fudan University – sequence: 8 givenname: Renchao surname: Che fullname: Che, Renchao email: rcche@fudan.edu.cn organization: Laboratory of Advanced Materials, Shanghai Key Lab of Molecular Catalysis and Innovative Materials, Fudan University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/35384519$$D View this record in MEDLINE/PubMed |
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| Keywords | Off-axis electron hologram Electromagnetic wave-absorbing materials Energetic metal organic framework Hierarchical porous structure M–M’ interaction |
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| PublicationTitleAbbrev | Nano-Micro Lett |
| PublicationTitleAlternate | Nanomicro Lett |
| PublicationYear | 2022 |
| Publisher | Springer Nature Singapore Springer Nature B.V Springer Singapore SpringerOpen |
| Publisher_xml | – name: Springer Nature Singapore – name: Springer Nature B.V – name: Springer Singapore – name: SpringerOpen |
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A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of... Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light... Improving the atom utilization of metals and clarifying the M-M' interaction is both greatly significant in assembling high-performance ultra-light... HighlightsA typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15... A typical 3D porous carbon sponge of CoFe@PCS exhibited the continuous distribution of nano-meso-micro-hierarchical pores in the range of 1 nm–15 μm. The... Abstract Improving the atom utilization of metals and clarifying the M–M’ interaction is both greatly significant in assembling high-performance ultra-light... |
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| SubjectTerms | Capacitors Carbon Cobalt Density distribution Dipoles Electromagnetic coupling Electromagnetic radiation Electromagnetic wave-absorbing materials Energetic metal organic framework Engineering Hierarchical porous structure High temperature Iron Metal clusters Metal-organic frameworks Microwave absorption and EMI shielding M–M’ interaction Nanoscale Science and Technology Nanotechnology Nanotechnology and Microengineering Off-axis electron hologram Pyrolysis Thickness Wave attenuation X ray absorption |
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| Title | Ultrahigh Density of Atomic CoFe-Electron Synergy in Noncontinuous Carbon Matrix for Highly Efficient Magnetic Wave Adsorption |
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