Rapid mass production of two-dimensional metal oxides and hydroxides via the molten salts method

Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be lo...

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Published in	Nature communications Vol. 8; no. 1; pp. 15630 - 9
Main Authors	Hu, Zhimi, Xiao, Xu, Jin, Huanyu, Li, Tianqi, Chen, Ming, Liang, Zhun, Guo, Zhengfeng, Li, Jia, Wan, Jun, Huang, Liang, Zhang, Yanrong, Feng, Guang, Zhou, Jun
Format	Journal Article
Language	English
Published	London Nature Publishing Group UK 30.05.2017 Nature Publishing Group Nature Portfolio
Subjects	140/146 639/925/357/1018 639/925/357/551 Chemical synthesis Electrochemistry Energy consumption Graphene Humanities and Social Sciences Hydroxides Manganese Manganese oxides Metal oxides Metals multidisciplinary Nitrates Scanning electron microscopy Science Science (multidisciplinary) Sedimentation & deposition Tungsten China
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Abstract	Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na 0.55 Mn 2 O 4 ·1.5H 2 O and K 0.27 MnO 2 ·0.54H 2 O), cation-intercalated tungsten oxides (Li 2 WO 4 and Na 2 W 4 O 13 ), and anion-intercalated metal hydroxides (Zn 5 (OH) 8 (NO 3 ) 2 ·2H 2 O and Cu 2 (OH) 3 NO 3 ), with a large lateral size and nanometre thickness in a short time. Using 2D Na 2 W 4 O 13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond. 2D materials with exotic electronic properties are increasingly important for the development of low-dimensional electronic devices. Here, Hu et al . have developed a fast and efficient method to synthesize 2D metal oxides and hydroxides, further enabling 2D electronics.
AbstractList	Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na 0.55 Mn 2 O 4 ·1.5H 2 O and K 0.27 MnO 2 ·0.54H 2 O), cation-intercalated tungsten oxides (Li 2 WO 4 and Na 2 W 4 O 13 ), and anion-intercalated metal hydroxides (Zn 5 (OH) 8 (NO 3 ) 2 ·2H 2 O and Cu 2 (OH) 3 NO 3 ), with a large lateral size and nanometre thickness in a short time. Using 2D Na 2 W 4 O 13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond. 2D materials with exotic electronic properties are increasingly important for the development of low-dimensional electronic devices. Here, Hu et al . have developed a fast and efficient method to synthesize 2D metal oxides and hydroxides, further enabling 2D electronics. Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na Mn O ·1.5H O and K MnO ·0.54H O), cation-intercalated tungsten oxides (Li WO and Na W O ), and anion-intercalated metal hydroxides (Zn (OH) (NO ) ·2H O and Cu (OH) NO ), with a large lateral size and nanometre thickness in a short time. Using 2D Na W O as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond. Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na 0.55 Mn 2 O 4 ·1.5H 2 O and K 0.27 MnO 2 ·0.54H 2 O), cation-intercalated tungsten oxides (Li 2 WO 4 and Na 2 W 4 O 13 ), and anion-intercalated metal hydroxides (Zn 5 (OH) 8 (NO 3 ) 2 ·2H 2 O and Cu 2 (OH) 3 NO 3 ), with a large lateral size and nanometre thickness in a short time. Using 2D Na 2 W 4 O 13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond. Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na0.55 Mn2 O4 ·1.5H2 O and K0.27 MnO2 ·0.54H2 O), cation-intercalated tungsten oxides (Li2 WO4 and Na2 W4 O13 ), and anion-intercalated metal hydroxides (Zn5 (OH)8 (NO3 )2 ·2H2 O and Cu2 (OH)3 NO3 ), with a large lateral size and nanometre thickness in a short time. Using 2D Na2 W4 O13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond. 2D materials with exotic electronic properties are increasingly important for the development of low-dimensional electronic devices. Here, Huet al. have developed a fast and efficient method to synthesize 2D metal oxides and hydroxides, further enabling 2D electronics. Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na0.55Mn2O4·1.5H2O and K0.27MnO2·0.54H2O), cation-intercalated tungsten oxides (Li2WO4 and Na2W4O13), and anion-intercalated metal hydroxides (Zn5(OH)8(NO3)2·2H2O and Cu2(OH)3NO3), with a large lateral size and nanometre thickness in a short time. Using 2D Na2W4O13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond.Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general synthesis methodology of 2D materials and advancing it from the laboratory to industry is of great importance. This type of method should be low cost, rapid and highly efficient. Here, we report the high-yield synthesis of 2D metal oxides and hydroxides via a molten salts method. We obtained a high-yield of 2D ion-intercalated metal oxides and hydroxides, such as cation-intercalated manganese oxides (Na0.55Mn2O4·1.5H2O and K0.27MnO2·0.54H2O), cation-intercalated tungsten oxides (Li2WO4 and Na2W4O13), and anion-intercalated metal hydroxides (Zn5(OH)8(NO3)2·2H2O and Cu2(OH)3NO3), with a large lateral size and nanometre thickness in a short time. Using 2D Na2W4O13 as an electrode, a high performance electrochemical supercapacitor is achieved. We anticipate that our method will enable new path to the high-yield synthesis of 2D materials for applications in energy-related fields and beyond.
ArticleNumber	15630
Author	Jin, Huanyu Liang, Zhun Huang, Liang Guo, Zhengfeng Zhou, Jun Hu, Zhimi Li, Tianqi Zhang, Yanrong Feng, Guang Chen, Ming Li, Jia Wan, Jun Xiao, Xu
Author_xml	– sequence: 1 givenname: Zhimi surname: Hu fullname: Hu, Zhimi organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 2 givenname: Xu orcidid: 0000-0001-6423-3039 surname: Xiao fullname: Xiao, Xu organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 3 givenname: Huanyu surname: Jin fullname: Jin, Huanyu organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 4 givenname: Tianqi surname: Li fullname: Li, Tianqi organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 5 givenname: Ming surname: Chen fullname: Chen, Ming organization: State Key Laboratory of Coal Combustion, School of Energy and Power Engineering, Huazhong University of Science and Technology – sequence: 6 givenname: Zhun surname: Liang fullname: Liang, Zhun organization: State Key Laboratory of Coal Combustion, School of Energy and Power Engineering, Huazhong University of Science and Technology – sequence: 7 givenname: Zhengfeng surname: Guo fullname: Guo, Zhengfeng organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 8 givenname: Jia surname: Li fullname: Li, Jia organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 9 givenname: Jun surname: Wan fullname: Wan, Jun organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 10 givenname: Liang surname: Huang fullname: Huang, Liang organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology – sequence: 11 givenname: Yanrong surname: Zhang fullname: Zhang, Yanrong organization: Environmental Science Research Institute, Huazhong University of Science and Technology – sequence: 12 givenname: Guang surname: Feng fullname: Feng, Guang organization: State Key Laboratory of Coal Combustion, School of Energy and Power Engineering, Huazhong University of Science and Technology – sequence: 13 givenname: Jun orcidid: 0000-0003-4799-8165 surname: Zhou fullname: Zhou, Jun email: jun.zhou@mail.hust.edu.cn organization: Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/28555669$$D View this record in MEDLINE/PubMed
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Snippet	Because of their exotic electronic properties and abundant active sites, two-dimensional (2D) materials have potential in various fields. Pursuing a general... 2D materials with exotic electronic properties are increasingly important for the development of low-dimensional electronic devices. Here, Huet al. have...
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SubjectTerms	140/146 639/925/357/1018 639/925/357/551 Chemical synthesis Electrochemistry Energy consumption Graphene Humanities and Social Sciences Hydroxides Manganese Manganese oxides Metal oxides Metals multidisciplinary Nitrates Scanning electron microscopy Science Science (multidisciplinary) Sedimentation & deposition Tungsten
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Title	Rapid mass production of two-dimensional metal oxides and hydroxides via the molten salts method
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