Solar photocatalytic mineralization of commercial pesticides: acrinathrin
A comparative study of the degradation of commerical acrinathrin spiked in water using TiO 2 photocatalysis and photolysis under sunlight was performed. Samples were analysed by liquid chromatography-diode array detector (HPLC–DAD) and gas chromatography-ion trap-mass spectrometric detector (GC–ITMS...
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Published in | Chemosphere (Oxford) Vol. 40; no. 4; pp. 403 - 409 |
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Format | Journal Article |
Language | English |
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01.02.2000
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Abstract | A comparative study of the degradation of commerical acrinathrin spiked in water using TiO
2 photocatalysis and photolysis under sunlight was performed. Samples were analysed by liquid chromatography-diode array detector (HPLC–DAD) and gas chromatography-ion trap-mass spectrometric detector (GC–ITMS). Additional total organic carbon (TOC) analyses were carried out to evaluate the mineralisation rates. One photoproduct, 2-phenoxy benzaldehyde, was unequivocally identified and evaluated by GC–ITMS during the processes. Although acrinathrin is almost destroyed when exposed to irradiation for more than 400 h, photocatalysis with TiO
2 noticeably reduced degradation to a few hours. In this case, with the additional presence of peroxydisulphate, in less than 2 h acrinathrin is completely destroyed. Mineralisation of acrinathrin, without catalyst, was only around 50% after 400 h of irradiation. |
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AbstractList | A comparative study of the degradation of commerical acrinathrin spiked in water using TiO
2 photocatalysis and photolysis under sunlight was performed. Samples were analysed by liquid chromatography-diode array detector (HPLC–DAD) and gas chromatography-ion trap-mass spectrometric detector (GC–ITMS). Additional total organic carbon (TOC) analyses were carried out to evaluate the mineralisation rates. One photoproduct, 2-phenoxy benzaldehyde, was unequivocally identified and evaluated by GC–ITMS during the processes. Although acrinathrin is almost destroyed when exposed to irradiation for more than 400 h, photocatalysis with TiO
2 noticeably reduced degradation to a few hours. In this case, with the additional presence of peroxydisulphate, in less than 2 h acrinathrin is completely destroyed. Mineralisation of acrinathrin, without catalyst, was only around 50% after 400 h of irradiation. A comparative study of the degradation of commercial acrinathrin spiked in water using TiO2 photocatalysis and photolysis under sunlight was performed. Samples were analysed by liquid chromatography-diode array detector (HPLC-DAD) and gas chromatography-ion trap-mass spectrometric detector (GC-ITMS). Additional total organic carbon (TOC) analyses were carried out to evaluate the mineralisation rates. One photoproduct, 2-phenoxy benzaldehyde, was unequivocally identified and evaluated by GC-ITMS during the processes. Although acrinathrin is almost destroyed when exposed to irradiation for more than 400 h, photocatalysis with TiO2 noticeably reduced degradation to a few hours. In this case, with the additional presence of peroxydisulphate, in less than 2 h acrinathrin is completely destroyed. Mineralisation of acrinathrin, without catalyst, was only around 50% after 400 h of irradiation. Acrinathrin is a new contact systemic insecticide introduced recently in Europe for use on fruits and vegetables. The photodegradation of acrinathrin was studied in aqueous solution in the presence of titanium dioxide as the photocatalyst with and without peroxydisulfate as an additional oxidant. The transformation products were identified subsequently. Results showed that, in the presence of TiO sub(2), the degradation rate of the insecticide was increased approximately 22-fold compared to the use of solar radiation alone. The presence of peroxydisulfate accelerated the degradation rate by more than 200 times compared with photolysis alone. Although several transformation products were formed, only 2-phenoxy benzaldehyde was identified. A comparative study of the degradation of commercial acrinathrin spiked in water using TiO sub(2) photocatalysis and photolysis under sunlight was performed. Samples were analysed by liquid chromatography-diode array detector (HPLC-DAD) and gas chromatography-ion trap-mass spectrometric detector (GC-ITMS). Additional total organic carbon (TOC) analyses were carried out to evaluate the mineralisation rates. One photoproduct, 2-phenoxy benzaldehyde, was unequivocally identified and evaluated by GC-ITMS during the processes. Although acrinathrin is almost destroyed when exposed to irradiation for more than 400 h, photocatalysis with TiO sub(2) noticeably reduced degradation to a few hours. In this case, with the additional presence of peroxydisulphate, in less than 2 h acrinathrin is completely destroyed. Mineralisation of acrinathrin, without catalyst, was only around 50% after 400 h of irradiation. The degradation the commercial pesticide acrinathrin, spiked in water by photocatalytic mineralization, was investigated. Photocatalysis with titanium oxide reduced degradation to 2 h compared to 400 h in the absence of a catalyst. The degradation rate was further increased by the additional presence of peroxydisulphate. In the absence of a catalyst, mineralization was only 50 per cent after 400 h. |
Author | Blanco, J Fernández-Alba, A.R Agüera, A Malato, S |
Author_xml | – sequence: 1 givenname: S surname: Malato fullname: Malato, S email: SIXTO.MALATO@PSA.ES organization: PSA (Plataforma Solar de Almerı́a). Crta Senés s/n, Tabernas, Almerı́a 04200, Spain – sequence: 2 givenname: J surname: Blanco fullname: Blanco, J organization: PSA (Plataforma Solar de Almerı́a). Crta Senés s/n, Tabernas, Almerı́a 04200, Spain – sequence: 3 givenname: A.R surname: Fernández-Alba fullname: Fernández-Alba, A.R organization: Pesticide Residue Research Group. Faculty of Sciences. University of Almeria, Almeria 04071, Spain – sequence: 4 givenname: A surname: Agüera fullname: Agüera, A organization: Pesticide Residue Research Group. Faculty of Sciences. University of Almeria, Almeria 04071, Spain |
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Keywords | Acrinathrin Photolysis Photocatalysis Solar energy Chemical analysis Insecticide Pesticides Pyrethroids Peroxodisulfates Heterogeneous catalysis Decontamination Mineralization Qualitative analysis Water pollution Solar radiation Titanium oxide Degradation product Comparative study Quantitative analysis Photochemical degradation |
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Cat. doi: 10.1016/0304-5102(90)85260-O contributor: fullname: Grätzel – volume: 28 start-page: 1159 year: 1994 ident: 10.1016/S0045-6535(99)00267-2_BIB5 article-title: Rapid degradation of fenitrotion in estuarine waters publication-title: Environ. Sci. Technol. doi: 10.1021/es00055a029 contributor: fullname: Lacorte – ident: 10.1016/S0045-6535(99)00267-2_BIB18 – volume: 93 start-page: 671 year: 1993 ident: 10.1016/S0045-6535(99)00267-2_BIB7 article-title: Photochemical processes for water treatment publication-title: Chem. Rev. doi: 10.1021/cr00018a003 contributor: fullname: Legrini |
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Snippet | A comparative study of the degradation of commerical acrinathrin spiked in water using TiO
2 photocatalysis and photolysis under sunlight was performed.... A comparative study of the degradation of commercial acrinathrin spiked in water using TiO2 photocatalysis and photolysis under sunlight was performed. Samples... Acrinathrin is a new contact systemic insecticide introduced recently in Europe for use on fruits and vegetables. The photodegradation of acrinathrin was... The degradation the commercial pesticide acrinathrin, spiked in water by photocatalytic mineralization, was investigated. Photocatalysis with titanium oxide... A comparative study of the degradation of commercial acrinathrin spiked in water using TiO sub(2) photocatalysis and photolysis under sunlight was performed.... |
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SubjectTerms | Acrinathrin Agronomy. Soil science and plant productions Applied sciences Biological and medical sciences Biological and physicochemical phenomena Catalysis Chromatography, High Pressure Liquid - methods Earth sciences Earth, ocean, space Engineering and environment geology. Geothermics Exact sciences and technology Fundamental and applied biological sciences. Psychology Gas Chromatography-Mass Spectrometry - methods Insecticides - chemistry Insecticides - radiation effects mineralization Natural water pollution Photocatalysis Photolysis Pilot Projects Pollution Pollution, environment geology Pyrethrins - chemistry Pyrethrins - radiation effects pyrethroid insecticides Soil and water pollution Soil science Solar energy solar radiation Sunlight Titanium titanium dioxide Ultraviolet Rays Water Water treatment and pollution |
Title | Solar photocatalytic mineralization of commercial pesticides: acrinathrin |
URI | https://dx.doi.org/10.1016/S0045-6535(99)00267-2 https://www.ncbi.nlm.nih.gov/pubmed/10665406 https://search.proquest.com/docview/14541864 https://search.proquest.com/docview/17682603 https://search.proquest.com/docview/18016543 |
Volume | 40 |
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