Preparation and characterization of polylactide-block-poly(butylene adipate) polyurethane thermoplastic elastomer
Polylactide‐block‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide‐block‐poly(butylene adipate)‐block‐polylactide (PBLA) and hexamethylene diisocyanate (HDI). PBLA was previously prepared with L‐lactide and pol...
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| Published in | Polymer engineering and science Vol. 51; no. 5; pp. 908 - 916 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Hoboken
Wiley Subscription Services, Inc., A Wiley Company
01.05.2011
Wiley Society of Plastics Engineers, Inc Blackwell Publishing Ltd |
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| Abstract | Polylactide‐block‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide‐block‐poly(butylene adipate)‐block‐polylactide (PBLA) and hexamethylene diisocyanate (HDI). PBLA was previously prepared with L‐lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight (Mw) of PLAEU surpassed 105 g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature (Tm) of PLAEU decreased, whereas its glass transition (Tg) shifted to high temperature due to the “pseudoextension” structure of polylactide (PLA) block. Additionally, the crystallinity and Tm of PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. POLYM. ENG. SCI., 2011. © 2011 Society of Plastics Engineers |
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| AbstractList | Polylactide‐block‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide‐block‐poly(butylene adipate)‐block‐polylactide (PBLA) and hexamethylene diisocyanate (HDI). PBLA was previously prepared with L‐lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight (Mw) of PLAEU surpassed 105 g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature (Tm) of PLAEU decreased, whereas its glass transition (Tg) shifted to high temperature due to the “pseudoextension” structure of polylactide (PLA) block. Additionally, the crystallinity and Tm of PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. POLYM. ENG. SCI., 2011. © 2011 Society of Plastics Engineers Polylactide-block-poly(butylene adipate) poly(ester-urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactideto block-poly(butylene adipate)-block-polylactide (PBLA) and hexamethylene thisocyanate (HDI). PBLA was previously prepared with L-lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight (M^sub w^) of PLAEU surpassed 10^sup 5^ g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature (T^sub m^) of PLAEU decreased, whereas its glass transition (T^sub g^) shifted to high temperature due to the 'pseudoextension' structure of polylactide (PLA) block. Additionally, the crystallinity and T^sub m^ of PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. [PUBLICATION ABSTRACT] Polyiactide-block-poly(butylene adipate) poly(ester-urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide-block-poly(butylene adipate)-block-polylactide (PBLA) and hexamethylene diisocyanate (HD1), PBLA was previously prepared with L-lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight ([M.sub.w]) of PLAEU surpassed [10.sup.5] g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature ([T.sub.m]) of PLAEU decreased, whereas its glass transition ([T.sub.g]) shifted to high temperature due to the 'pseudoextension" structure of polylactide (PLA) block. Additionally, the crystallinity and [T.sub.m] of PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. POLYM. ENG. SCI., 51:908-916, 2011. [C]2011 Society of Plastics Engineers Polylactide‐ block ‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide‐ block ‐poly(butylene adipate)‐ block ‐polylactide (PBLA) and hexamethylene diisocyanate (HDI). PBLA was previously prepared with L ‐lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight ( M w ) of PLAEU surpassed 10 5 g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature ( T m ) of PLAEU decreased, whereas its glass transition ( T g ) shifted to high temperature due to the “pseudoextension” structure of polylactide (PLA) block. Additionally, the crystallinity and T m of PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. POLYM. ENG. SCI., 2011. © 2011 Society of Plastics Engineers Polylactide-block-poly(butylene adipate) poly(ester-urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactideto block-poly(butylene adipate)-block-polylactide (PBLA) and hexamethylene thisocyanate (HDI). PBLA was previously prepared with L-lactide and poly(butylene adipate) diol (PBA diol). Experimental parameters including feed ratio, polymerization temperature, and time were optimized. The weight average molecular weight (M sigma ub w] of PLAEU surpassed 10 sigma up 5g/mol. In contrast to corresponding PBLA, the crystallinity and melt temperature (T sigma ub m] of PLAEU decreased, whereas its glass transition (T sigma ub g] shifted to high temperature due to the 'pseudoextension' structure of polylactide (PLA) block. Additionally, the crystallinity and T sigma ub mof PLAEU were subject to crystallization method and molecular weight. The tensile strength of PLAEU varied from 6.61 to 24.41 MPa and elongation from 190% to 780%. Therefore, the mechanical properties of PLAEU can be regulated by altering the length ratio of PLA to PBA block. The high elasticity of PLAEU can be explained with phase separation mechanism. [PUBLICATION ABSTRACT] |
| Audience | Academic |
| Author | Ren, Jie Zhong, Qian Wang, Qinfeng |
| Author_xml | – sequence: 1 givenname: Qian surname: Zhong fullname: Zhong, Qian organization: Institute of Nano and Bio-Polymeric Materials, School of Materials Science and Engineering, Tongji University, Shanghai 200092, People's Republic of China – sequence: 2 givenname: Jie surname: Ren fullname: Ren, Jie email: renjie@tongji.edu.cn organization: Institute of Nano and Bio-Polymeric Materials, School of Materials Science and Engineering, Tongji University, Shanghai 200092, People's Republic of China – sequence: 3 givenname: Qinfeng surname: Wang fullname: Wang, Qinfeng organization: Institute of Nano and Bio-Polymeric Materials, School of Materials Science and Engineering, Tongji University, Shanghai 200092, People's Republic of China |
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| Keywords | Lactone copolymer Lactic acid copolymer Mechanical properties Thermoplastic rubber Crystallinity Experimental study Polyaddition Tensile strength Polyurethane elastomer Thermal properties Ester copolymer Esterurethane polymer Multiblock copolymer Preparation Property structure relationship Adipate copolymer |
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| Snippet | Polylactide‐block‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with... Polylactide‐ block ‐poly(butylene adipate) poly(ester‐urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactide‐... Polyiactide-block-poly(butylene adipate) poly(ester-urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with... Polylactide-block-poly(butylene adipate) poly(ester-urethane) (PLAEU) thermoplastic elastomer was obtained by melt chain extending reaction with polylactideto... |
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| SubjectTerms | Applied sciences Blocking Chemical properties Composition Crystallinity Diols Elastomers Exact sciences and technology High temperature Identification and classification Mechanical properties Molecular structure Molecular weight Organic polymers Phase separation Physicochemistry of polymers Polycondensation Polymerization Polyurethane Polyurethanes Preparation, kinetics, thermodynamics, mechanism and catalysts Production processes Thermoplastic elastomers Thermoplastics |
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| Title | Preparation and characterization of polylactide-block-poly(butylene adipate) polyurethane thermoplastic elastomer |
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